Lady Jewellyn G.Diola*‚ Jennika Joy L. Casin‚ Andrian R. De Leon‚ Jan Rotsen Kyle A. Delos Santos Department of Chemistry‚ College of Science *Lady Jewellyn G. Diola; ladyjewellyndiola@yahoo.com Abstract Synthesis of 3‚4-dihydro-3-(p-methylphenyl)-1‚2-(2h)-benzoxazine involves the nucleophillic addition of the 1 °amine group upon the carbonyly group of the salicylaldehyde‚ the reduction of imine to amine and the addition of paraformaldehyde to proceed ring closure. The
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Inorganica Chimica Acta 357 (2004) 3825–3835 www.elsevier.com/locate/ica Synthesis‚ crystal structures‚ and molecular hyperpolarizabilities of a new Schiff base ligand‚ and its copper(II)‚ nickel(II)‚ and cobalt(II) metal complexes Pascal G. Lacroix a b a‚* ‚ Frdric Averseng a‚ Isabelle Malfant a‚ Keitaro Nakatani e e b Laboratoire de Chimie de Coordination du CNRS‚ 205 route de Narbonne‚ 31077 Toulouse‚ France PPSM‚ Ecole Normale Suprieure de Cachan‚ URA 1906‚ Avenue du Pdt Wilson
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Monica Perez Experiment 8: Acetylsalicylic Acid Experiment 01/25/2013 CHM Lab- 2211 Sec 0016 Instructor: Jennifer Reed Introduction: Commonly used as Aspirin‚ acetylsalicylic acid is an analgesic (pain reliever)‚ which is one of the products of the esterification reaction between salicylic acid and acetic anhydride. This esterification occurs since the hydroxyl group from the salicylic acid reacts with acetic anhydride to form an ester. In this experiment‚ we will be able to recreate
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LABORATORY REPORT 4 PREPARATION OF ALUM FROM ALUMINUM METAL Huy Nguyen October 2nd‚ 2012 The objective of the laboratory is to synthesize alum (KAl(SO4)2.xH2O) from aluminum powder and to determine the proportion of water in the alum crystals. Alum is a product from the reaction between potassium hydroxide and sulfuric acid. The reaction include several steps‚ as followed: Aluminum powder reacts with potassium hydroxide to generate Al(OH)4- ions and release hydrogen. 2 Al(s) + 2 KOH(aq)
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Organic Chemistry II Laboratory (ABCT357/ABCT3757) Lab Manual 2014-2015 Lee Hang Wai‚ Alston (alston.lee@polyu.edu.hk) Dr. Lee Cheng Hao‚ Samuel (chenghao.lee@polyu.edu.hk) Organic Chemistry II Laboratory (ABCT357‚ ABCT3757) (Group one) Contact: Alston Lee (alston.lee@polyu.edu.hk) Tuesday 8:30-11:30 ‚ Laboratory: Y1315 Lab supporting staffs: YK Au / Kan Chan/Arnold Demonstrators: Dr. Samuel Lee‚ Alston Lee‚ Fu Wai Chung‚ Guo Shuai‚ Yuen On Ying‚ Sep 16 Tue Acetylation of α-D-glucopyranose (Expt
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SYNTHESIS OF 1-PHENYLAZO-2-NAPHTHOL ABSTRACT Amines are compounds composed of nitrogen atoms bearing alkyl or aromatic compounds. Amines undergo interesting reactions‚ one of which is with the reaction with nitrous acid producing an azo dye. In this study‚ the experiment focused on synthesizing an observing the physical properties of Sudan-1. Sudan-1 is of the most common dyes found in waxes‚ oils and in some food ingredients specifically curry and chilli powder. Furthermore‚ this study aimed to
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the synthesis of a compound or in the isolation of a compound from a natural source‚ acid-base extractions are used to either directly isolate a desired acidic or basic compound or to remove acidic or basic impurities. Extraction‚ along with recrystallization and distillation‚ is one of the most important separation and purification techniques in organic chemistry. The Experiment. then the drop will mix with the solution. If the solvent is the mistaken organic layer‚ then the water
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Synthesis‚ Recrystallization of β-D-Glucose Pentaacetate from its Original D-Glucose and it comparison with literature though Melting point‚ TLC‚ IR‚ 1H and 13C NMR Abstract: The synthesis of the product: β-D-glucose pentaacetate is done though the acetylation using acetic anhydride with D-glucose with the help of sodium acetate. The recrystallization of the product is done though a polar solvent like water. The Result of this experiment has a percentage yield of 61% and analytical methods
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2-(2‚4-Dinitrobenzyl) pyridine Peter Defnet and Cody Krepps Department of Chemstry Juniata College Huntingdon‚ PA September 18‚ 2012 Abstract: Nitration of 2-benzylpyridine is supposed to yield 2-(2‚4-Dinitrobenzyl) pyridine‚ when electrophilic aromatic substitution is the mechanism. Experiencing many pitfalls‚ however‚ has lead to the actual product obtained to contain the expected product‚ as well as many impurities. This report examines the supposed mechanism for the electrophilic substitution
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EXPERIMENT 1: REACTIONS OF ENOLATE IONS WITH CARBONYL GROUPS Aims In this experiment we used two techniques for the reactions of enolate ions with carbonyl groups. One technique used was Doebner reaction and the other technique used was Claisen-Schmidt reaction. Therefore the aim of this experiment is to synthesize trans p-methoxycinnamic acid and to synthesize dibenzalacetone via an aldol condensation reaction between acetone and benzaldehyde. The products would be recrystallized using ethanol
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