Name: Bhumiben Shah Date: 31st Jan ‘13 EXPERIMENT # 2 RECRYSTALLIZATION; FILTRATION OBJECTIVES: 1. To perform recrystallization and filtration of given impure organic compound. 2. To purify impure acetanilide using reflux condenser apparatus and Hirsch funnel filtration. 3. To determine percentage recovery of pure material (which is)‚ purified by recrystallization and filtration. SAFETY PRECAUTIONS: 1. Operate the aspirator with the maximum water-flow using a stop cock to
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Analytes with lower boiling points would boil first and elute before analytes with higher boiling points. The two factors affect retention time‚ which is used to determine the identity of eluted compounds. For the experiment‚ the internal standard anisole was eluted before limonene because it was more polar and had a lower boiling
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2):  During this experiment‚ we used recrystallization methods in order to help in the purification of the unknown solid‚ as well as drying and vacuum filtration. We then ground the unknown and combined it with different chemicals (such as acetanilide or phenacetin) and used the melting point ranges to determine the identity. We used the Mel-Temp method in order to measure the melting points. (It is important to remember that if a chemical is mixed with a differing chemical‚ the melting point
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SYLLABUS CHEMISTRY (043) CLASS-XII – (2012-13) Annexure - ‘ I ’ S.No. 1. 2. 3. 4. Type of Question Long Answers (LA) Short Answers-II (SA II) Short Answers-I (SA-I) Very Short Answer (VSA) Total Marks for No. of Total Marks each Question Questions 5 3 2 1 3 9 10 08 30 15 27 20 08 70 Weightage 4 5 5 5 4 3 8 5 3 4 4 6 4 4 3 3 70 Total: S.No. UNIT 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. Solid State Solutions Electrochemistry Chemical Kinetics Surface Chemistry General Principles
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SOLVENT EXTRACTION Solvent extraction‚ also known as liquid extraction and partitioning‚ is a method to separate compounds based on their relative solubility in two different immiscible liquid‚ usually water and organic solvent. It is an extraction from one liquid phase to another liquid phrase. Liquid extraction is a basic technique in chemical laboratories‚ where it is performed using a separator funnel. This type of process is commonly performed after a chemical reaction as part of the work-up
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Kate Kirby June 6‚ 2013 Title: Extraction of an Unknown Compound Purpose: The purpose of this experiment was to separate a mixture of two or more unknown compounds and identify them based on their melting point and reactivity with an acid or a base. Compound studied/Reactions: The organic solvent used in this experiment was methyl t-butyl ether (MTBE‚ 2-methoxy-2-methylpropane). The unknown that dissolved in the MTBE‚ but was insoluble in water. MBTE is very volatile and flammable. It was
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gum arabic powder and icing sugar. For a specifically black polish‚ 280 g (10 oz) of charcoal powder from the chemist may be added at this stage. In recent history the black colour comes from an aniline dye. The next recipe indicates that nigrosene (generically‚ a black dye made from oxidised aniline) was domestically procurable in the 1940s. Note that the above recipe uses potassium carbonate (potash) whereas the following recipe uses potassium bicarbonate‚ which is not potash. Imperial Measures
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their possible result. Analyze and state the observation based on the result of experiment. Methodology Materials and Apparatus The chemicals used in the experiment are as follows: benzoic acid‚ sugar‚ denatured alcohol‚ chloroform‚ acetanilide‚ copper sulfate‚ activated charcoal‚ distilled water‚ acetone‚ toluene‚ glutamic acid and glycine. The apparatus used include funnel‚ Erlenmeyer flask‚ separatory funnel‚ beakers‚ evaporating dish‚ water bath‚ graduated cylinder‚ stirring rod‚ watch
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corrosive‚ harmful if inhaled‚ flammable and can cause burns (handle in fume hood) Gloves are recommended to avoid chemical contact with skin Reaction Scheme: Conversion of acetanilide to p-bromoacetanilide Procedure: To a 125 mL Erlenmeyer flask containing a mixture of 95% ethanol (6 mL) and acetic acid (5 mL)‚ dissolve acetanilide (7.4 mmol) and sodium bromide (1.8 g). Place the reaction flask in an ice bath (at least 5oC) for 5 minutes (keep this reaction in the hood). Add sodium hypochlorite (8
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evidence will show that the red solid collected after recrystallization from the nucleophilic aromatic substitution of 2‚ 4-dinitrobromobenzene and aniline has the characteristics of 2‚ 4-dinitrodiphenylamine. Evidence: The procedure was carried out as described by Ault1 and the lab manual2. 2‚4-dinitrobromobenzene (0.92g‚ 3.75mmol‚ pale yellow solid) and aniline (0.7mL‚ 0.7g‚ 7.5 mmol) were boiled in ethanol (10mL) under reflux until all solid dissolved. After the mixture cooled to room temperature‚ short
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