Name: Bhumiben Shah Date: 31st Jan ‘13 EXPERIMENT # 2 RECRYSTALLIZATION; FILTRATION OBJECTIVES: 1. To perform recrystallization and filtration of given impure organic compound. 2. To purify impure acetanilide using reflux condenser apparatus and Hirsch funnel filtration. 3. To determine percentage recovery of pure material (which is)‚ purified by recrystallization and filtration. SAFETY PRECAUTIONS: 1. Operate the aspirator with the maximum water-flow using a stop cock to
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The Iodine Clock Investigation Introduction This is an investigation into the rate of a reaction and the factors that contribute to how fast a reaction will take place. Through the recording and analysis of raw data‚ this investigation also allows us to apply generally accepted scientific rules and to test them against results gained from accurate experimental procedures. Aim The aim of this experiment is to investigate the rate at which iodine is formed when the concentration
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Preparation of t-Butyl-Chloride March 8 & 15‚ 2012 Theory: Alkyl halides can be synthesized when alcohols react with hydrogen halides. An alkyl halide is a halogen-substituted alkane‚ and a hydrogen halide is a compound consisting of a hydrogen bonded to a halogen (H-X). Alkyl halides are classified as primary‚ secondary‚ or tertiary depending on the number of alkyl substituents directly attached to the carbon bearing the halogen atom. The purpose of this laboratory experiment was to prepare
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SODIUM DISORDERS * Identify specific types of hyponatremia and hypernatremia using diagnostic criteria and assessment questions * Hyponatremia * Mild: 125-130 * Nausea‚ Malaise * Moderate: 115-125 * HA‚ Lethargy‚ Restlessness‚ Disorientation * Severe: <115 * Seizures‚ Coma‚ Resp/Brainstem damage * Hypernatremia * Mild: 145-160 * Asymptomatic * Moderate: 160-180
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Lithium‚Sodium‚Potassium‚Rubidium‚Caesium and Francium are all part of group 1.They are metals that can be easily cut.After being cut‚it is shiny but it quickly tarnishes due to the fact that the metal reacts quickly with oxygen or water.The shiny surfaces of Sodium quickly tarnishes more quickly than Lithium and Potassium more tarnishes more quickly than Lithium.This shows that the reactivity increases as we move down the group. Figure 1 Elements Melting point Boiling point Thermal
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this experiment was to use Iodine‚ Benedict and Biuret to test the reaction of the following 12 samples: 1% glucose‚ 0.3% glucose-1-phosphate‚ 1% maltose‚ honey‚ 1% sucrose‚ 1%lactose‚ 1% glycogen‚ 1% starch‚ protein‚ beer‚ distilled water and an unknown solution (test tube: 300). The iodine test for starch was to test how would starch reacted if we put iodine in it. The color of starch before the test was clear. The color of the iodine was brown. When you added iodine into starch‚ the result was
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The halides in unknown solution were identified as iodide and chloride based on their experimental E°(Ag/AgX) values‚ -0.16 ±0.01V and 0.22 ±0.02V respectively. These results were both accurate with percent error of 5.96% for iodine and 0.9% for chloride. The literature value of E°(Ag/AgI) and E°(Ag/AgCl) were -0.151V and 0.222V respectively (1). In addition‚ the literature vales lay within the 95% confidence interval for both halides therefore the results were accurate. These results were precise
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Title: Separating the components of “Panacetin” Name: Ip‚ Wing Chung (Vincent) Lab Partner: Ma‚ Siyin Date: 2/3/2013 Introduction: The purpose of this experiment is to investigate the composition of compounds in Panacetin. Generally‚ it is made up of sucrose‚ aspirin and an unknown component‚ either acetanilide or phenacetin. SinceBy using different techniques‚ such as filtration‚ extraction‚ and evaporation‚ those three components have been isolated out‚ which is based on varies solubility
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Separating a Mixture Aim: To separate the components of a mixture of sand and salt. To carry out a gravimetric analysis to calculate the percentage of both components. Equipment: * Electronic Scale | * Evaporating Basin | * Beaker | * Bunsen Burner | * Glass Stirring Rod | * Filter Funnel | * Wire Gauze Mat | * Filter Paper | * Heat Resistant Mat | * Conical Flask | * Safety Glasses | * Tripod | * Matches | Tongs | Risk Assessment:
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SCHOOL OF FOOD SCIENCE & NUTRITION LABORATORY REPORT NT20903 FOOD CHEMISTRY AND BIOCHEMISTRY Determination of free fatty acid(FFA) and iodine value (IV)in oil LECTURER NAME : MOHD NAZRI BIN ABDUL RAHMAN LAB SESSION : 3 OCTOBER 2011 (GROUP 4‚ MONDAY) Group Member Title: Determination of free fatty acid (FFA) in oil and determination of iodine value (IV) in oil Introduction Acid value or free fatty acid content is an important characteristic commonly used in quality control of fat
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