ANALYTICAL AND ORGANIC CHEMISTRY LECTURER’S NAME : DR.RAPIDAH OTHMAN COD SUBJECT : NKB 10103 NAME : NUR NADIRAH BINTI BAHARUDEAN ID NUMBER : 55220114255 CHAPTER : ORGANIC CHEMISTRY CONTENTS 1‚4-BENZENEDICARBOXYLIC ACID Introduction The organic compound’s group that I’ve chosen in this assignment is 1‚4-benzenedicarboxylic acid. 1‚4-benzenedicarboxylic acid and also called as Terephthalic acid containing the carboxyl group and benzene group. Sometimes it simply referred to as a acid group
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Separation of the Components of a Mixture Purpose: To become familiar with the methods of separating substances from one another using decantation‚ extraction‚ and sublimation techniques. Apparatis and Chemicals: balance‚ Bunsen burner‚ rubber hose‚ tongs‚ 2 evaporating dishes‚ 2 watch glasses‚ 100-mL graduated cylinder‚ clay triangles‚ 2 ring stands‚ 2 iron rings‚ 2 glass stirring rods‚ unknown mixture of NaCl‚ NH4Cl‚ SiO2. Discussion: Mixtures are composed of two or more substances
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Experiment B2 Chromatography for Protein Purification Name Matric No. Group : : : Date of Expt. : GRADE : A. Learning objectives 1. 2. 3. 4. Establish chromatographic assay to determine protein concentrations in a mixture. Appreciate the importance of resolution in protein chromatography. Understand the tension between purity and yield in protein chromatography. Understand the importance of mass balance closure in protein purification. B. Introduction I. Fast Protein Liquid Chromatography
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EXTRACTION OF METALS SUMMARY Most metals exist in compounds in rocks in the Earth’s crust. Many of these ores contain oxides or sulphides of the metals. The compounds need to be reduced to produce the metals as elements. Metals are very useful to us because of their special properties. Reduction means removal of oxygen or gain of electrons. Carbon is a good chemical reducing agent because it readily combines with oxygen‚ but it is only useful for the metals below it in the Reactivity
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acid-alkaline extraction. 2. To determine the percentage recovery and melting point of benzoic acid and p-diclorobenzene. Apparatus:Separatory funnel(250mL)‚Buchner funnel‚beaker. Materials:Benzoic acid‚p-dichlorobenzene‚ether‚10% NaOH‚conc.HCl‚distilled water‚ anhydrous CaCl2. Introduction: Organic compounds in an aqueous mixture can be separated by shaking the aqueous solution with a solvent which is immiscible with water. Extraction involves dissolving either a compound or compounds from
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experiment is to practice common organic laboratory techniques inside the lab to get one oriented to the basic methods of procedure that can be used for later experiments. This experiment involves the separation of benzoic acid from a more crude form‚ consisting of benzoic acid‚ methyl orange‚ a common acid/base indicator‚ and cellulose‚ a natural polymer of glucose (Huston‚ and Liu 17-24). The technique that is used to perform this separation is called extraction. Extraction is a systematic process of
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Introduction Extraction is a purification technique used in organic chemistry to separate compounds from a mixture of two or more compounds. There are three different extraction techniques: liquid-liquid extraction‚ solid-liquid extraction and chemically active extraction. All three types of extraction follow the same principle. Organic molecules dissolve in organic solvents and polar molecules dissolve in aqueous solvents. This phenomenon is observed because of the intermolecular forces between
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Purification of Infliximab[3] begins at Stage 1 with the filtration of the harvest material using a spin filter. The harvest is then clarified and undergoes 3 main chromatographic steps. Firstly‚ at Stage 2‚ the direct protein capture by Protein A affinity chromatography helps to remove a large majority of the impurities whicn include viruses and media components. At Stage 3‚ prior to cation exchange chromatography‚ the purified material in the eluted stream is then subjected to freezing‚ thawing
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mummion assignment Task 1 – purification Aim We were given a sample of mummion in the form of dried mud from a lake; the aim of the practical was to purify the sample and separate it from the insoluble impurities into the form of mummion salt. Context A long time ago mummion was used to preserve the bodies of ‘mummies’ in ancient Egypt‚ mummion along with other naturally occurring preservatives was used to treat the organs before the bodies were wrapped. This purification practical happens very often
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the melting points of crude and recrystallized acetanilide. Introduction : The most common method of purifying solid organic compounds is by recrystallization. In this technique‚ an impure solid compound is dissolved in a solvent and then allowed to slowly crystallize out as the solution cools. As the compound crystallizes from the solution‚ the molecules of the other compounds dissolved in solution are excluded from the growing crystal lattice‚ giving a pure solid.The first consideration in purifying
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