tert-butyl chloride via an SN1 reaction. t-Butyl Chloride was synthesized from t-Butyl Alcohol using hydrochloric acid in separatory funnel; isolation of t-Butyl Chloride was done under distillation conditions. The experiment resulted in 8.29grams of purified compound‚ which is a 66.27 percent yield. Procedure: As per handout with changes Equation: Mechanism: Results: (Scan IR spectrum) Compounds t-Butyl Chloride(Experimental) t-Butyl Chloride(Book Value) Molecular Weight (g/mol) 92.5681
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Abstract This work describes the extraction of caffeine from tea leaves to determine its % caffeine. The extraction process selectively dissolves one or more compounds in a mixture into an appropriate solvent. In this experiment‚ it was visible in the process wherein the components of the tea leaves were dissolved in two solvents‚ water and dichloromethane (DCM)‚ with DCM used for multiple extractions. The organic layer was evaporated and the determined % caffeine was 0.12%. Furthermore‚ the purified
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Mohamed Hatab‚Ibraheem Sattour‚Rahim Fazil‚Tarik Ahroui Simple sentences‚compound sentences‚complex sentences‚compound complex sentences Simple sentence:Contains a subject a predicate‚and expresses a complete thought Ex.Some students like to study in the morning Identify the subject and predicate in these simple sentences Ex.1 1.Bill and Bob auditioned for the lead role in the play. 2.The kittens were adopted by the family. 3.Peanut butter
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Extraction of Caffeine from Thea sinensis Abstract Extraction of Caffeine from Thea sinensis main objective is to isolate‚ purify characterized caffeine from tea leaves. Sublimation technique was used to get the % yield which is 0.07%. The melting point of the standard caffeine with the sublimate is 229°C. Introduction The active ingredient that makes tea and coffee valuable to humans is caffeine. Caffeine is an alkaloid; a class of naturally occurring compounds containing nitrogen and
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then separate a component (acetyleugenol) from the oil by liquid-liquid extraction. Finally‚ you will isolate the acetyleugenol by using a rotovap for reduced pressure distillation‚ which will remove the organic solvent (dichloromethane). Background Whole cloves contain between 14% and 20% by weight of essential oils‚ but only half of that can be isolated as acetyleugenol. Clove oil contains two basic compounds: eugenol and acetyleugenol. As a result of Dalton’s Law and Raoult’s
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#2 and #3 Extraction and Evaporation Recrystallization and Melting Point Measurement PURPOSE: 1. To the components of a simulated pharmaceutical preparation‚ Panacetin‚ and identifying the unknown component of the mixture through extraction and separation methods. 2. To learn how to purify by recrystallization‚ how to dry them and how to obtain a melting point. PRECAUTION: ACETANILIDE AND PHENACETIN ARE EYE AND SKIN IRRITANTS. Minimize contact with your unknown compound. THEORY:
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Lab 3 – Separation of a Mixture of Solids Cathy Lab Partners: Chelsea Brooke Sept 4‚ 2012 Chemistry 131A Dr. Vicki H Audia Pelab Questions: Proposed procedure for separation of a mixture: Use physical properties of the 4 substances to separate. 1. Remove iron with magnet 2. Add water to the mixture to melt the benzoic acid and NaCl then filter out sand. 3. Chill the solution and scoop the acid out leaving a salt solution. 4. Boil water away leaving salt. Purpose: The
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Continuously Compounded Interest Mathematics: MATH650 section 02 Wendy Forbes April 27‚ 2010 We often hear people say that we should let our money work for us. Using money or capital for income or profit is called an investment. An accountant manages a company’s money. Then‚ managers or company investors review their reports to find out the financial status. The demand for accountants increases as more private companies are established. In addition‚ there are always new and changing
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EXPERIMENT 1 IDENTIFICATION OF UNKNOWN COMPOUNDS Date of experiment : 7th August 2012 Venue: ME204 INTRODUCTION Chemical reactions are regularly categorized into 3 types: oxidation-reduction (redox reaction)‚ precipitation (double displacement) and acid-base reaction (double displacement) Type 1: Oxidation-Reduction Reactions Oxidation-reduction processes include the movements of electrons form oxidants to reductants‚ which lead to increases in oxidation
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of a mixture and purifying them through sublimation and recrystiliation‚ changes in the substances physical properties can be shown. A salicylic acid-naphthalene mixture was mixed together with diethyl ether and saturated sodium bicarbonate. Two layers separated and were extracted after acidifying with HCl. This precipitated the crude salicylic acid. The left over mixture was combined with water and the two layers separated where crude naphthalene was recovered. Sublimation was used to purify
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