Melting point 1. What two effects do impurities have on the melting point of an organic compound? Soluble impurities affect the melting point of a solid in the following manner. a. The presence of an impurity in the molten compound reduces its vapor pressure thus lowering the melting point of the compound. b. Broaden the melting point range. 2. For what tow purpose are melting points routinely used a. To determine the identity of an organic solid. b. To determine the purity of an organic solid
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Contents 1. Introduction 2 2. Concrete attacks 2 3. Alkali-Silica Reaction – ASR 3 4. Sulphate Attack 5 5. Reference List 8 1. Introduction This report was issued in order to provide an in depth understanding of how a surveyor can differentiate between Alkali-Silica Reaction and Sulphate attacks in concrete when inspecting a building. In order to satisfy the requirements for this report‚ the author will give a detailed description of both kind of attacks‚ different study areas
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Chromatography refers to a set of laboratory methods used in separating as well as purifying biomolecules. A variety of chromatography techniques exist‚ and all depend on the interaction between a stationary and a mobile state. Two types of chromatography methods were examined in this investigation. First‚ ion-exchange chromatography was used. This method separates ions and polar molecules based on their affinity to the ion exchanger [2]. Specifically‚ cation-exchange chromatography was performed
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SYNT m o d u l a r · l a b o r a t o r y · p r o g r a m · i n · publisher: H. A. Neidig c h e m i s t r y 738 organic editor: Joe Jeffers Copper-Catalyzed Oxidation of Benzoin to Benzil prepared by Carl T. Wigal‚ Lebanon Valley College PURPOSE OF THE EXPERIMENT Oxidize benzoin to benzil using ammonium nitrate and copper(II) ion as a catalyst‚ monitoring the reaction by thin-layer chromatography. Characterize the product using melting point measurement and infrared spectroscopy. EXPERIMENTAL
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Column and thin layer chromatography of plant pigments CHEMISTRY 201L EXPT 04 PAGE 01 - 12 Noel Angelo P. Kalacas*‚ Hanna Mae Laluces‚ Ina Bianca Lanuza Department of Chemistry‚ College of Science *Corresponding author; e-mail: knight_BeNcH66@yahoo.com Abstract Chromatography is a powerful technique for separating and/or identifying the components in a mixture. There are different types of chromatography and each has its own strengths and weaknesses. In this experiment‚ pigments of the
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compound. Intodection. In this experiment the thin-layer chromatography the (TLC) will be used to determine the composition of various over-the-counter analgesic. We will be given two commercially prepared TLC plates with a flexible backing and a silica-gel coating with a fluorescent indicator. On the first TLC plate‚ a reference plate‚ we will spot five standard compounds . In addition‚ a standard reference mixture containing four of these same compounds will be spotted. In this experiment we will
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Column Chromatography of Plant Pigments Paul Ibarbia‚ Gene Paolo Jasmin‚ Gianpaolo Jimenez and Lorenzo Labicane* Department of Biology‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Column chromatography of plant pigments is the separation of plant pigments extracted from Capsicum frutescens (siling labuyo). No slurry is prepared of the eluent; eluent with the stationary phase is set and then carefully poured into the column. The eluent are the solvents which are responsible for the
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Sulfate (ZTS) is a Semi Organic Nonlinear Optical (NLO) material which finds applications in the area of laser technology‚ optical communication‚ data storage technology‚ and optical computing etc. The author has successfully grown ZTS crystal by gel method. Gel technique has been adopted at ambient temperature to attain better result. The grown crystals were transparent and colourless. The crystal size has been obtained the range about 5mm X 3mm X 2mm. Thermal study of ZTS crystal from Thermo-Gravimetric
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Chromatography 43 A simple and sensitive high-performance thin-layer chromatography method has been developed for the quantitative estimation of gatifloxacin and ornidazole in its combined dosage forms. Gatifloxacin and ornidazole were chromatographed on silica Gel 60 F254 TLC plate using n-butanol: methanol: ammonia (6 M) (8:1:1.5 v/v) as the mobile phase and scanned at 302 nm using a Camag TLC Scanner 3. The linearity of gatifloxacin and ornidazole were in the range of 100-500 ng/spot and 250-1250 ng/spot
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separate test tubes containing 2.5mL of dichloromethane. I noticed that my unknown was a coated tablet. Each test tube was swirled until the greatest amount of each solid was dissolved. Each solution was spotted along a labeled starting line on the silica gel TLC plate. The TLC plate was put into a developing chamber containing 200:1 acetic acid and allowed to developed until the solvent reached almost to the top of the TLC plate‚ which took about 10 minutes. When the TLC plate finished developing
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