CHEM 3152-003 Experiment 2: Fractional Distillation and Gas Chromatography Introduction: The purpose of this experiment was to separate a mixture of ethyl acetate (EtOAc) and toluene by using the method of fractional distillation and to analyze the fractions using gas chromatography (GC). ethyl acetate toluene Distillation is a method known as separating or purifying a liquid or mixture by vaporization and condensation. In a simple distillation‚ the liquids being separated boil below 150 0C
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DESIGN CONSIDERATIONS * System: Ethanol – water * Feed rate: 225kmol/h * Feed composition: 28 mol% ethanol * Feed condition: 50% saturated liquid & 50% saturated vapor * 97% of ethanol recovery is required * Operating pressure: 1bar * Distillate composition: 81 mol% ethanol * Column type: Sieve tray column * Operating condition: 70% of flooding Applying material balance to the rectifying section (Eqn 01); V=L+D Applying material balance for the more volatile
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ranged from about 77 degrees in fraction 1 to about 89 degrees in the fraction 10. Next‚ the toluene stayed relatively the same temperature throughout the first 6 fractions at around 69 degrees and then drastically shot up to 100 degrees by the end of fraction 10. This is due to hexane having a lower boiling point and being able to steadily increase through each fraction evenly as temperature rises while the toluene‚ because of its higher boiling component‚ needed the higher temperature in order for higher
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1 Section 2 – 12:30 to 2:20 Distillation and Fractional Distillation Distillation and Fraction Distillations Purpose: The purpose of distillation is to purify a liquid. Distillations are use to purify contaminates out of water to obtain clean pure water‚ as well as‚ to separate mixtures of liquids into their individual components; e.g. methanol and water. Objective: Distill methanol from water using a simple distillation apparatus and fractional distillation apparatus to determine which
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Sodium chloride‚ also known as salt‚ common salt‚ table salt‚ or halite‚ is an ionic compound with the formula NaCl. Sodium chloride is the salt most responsible for the salinity of the ocean and of the extracellular fluid of many multicellular organisms. As the major ingredient in edible salt‚ it is commonly used as a condiment and food preservative. [edit] Properties Thermal conductivity of pure NaCl as a function of temperature has a maximum of 2.03 W/(cm K) at 8 K and decreases to 0.069 at 314
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purpose of this experiment was to isolate the aromatic hydroxyl compound‚ eugenol from crushed cloves using steam distillation. After conducting the distillation‚ the expected two layers were not visible in the centrifuge tube. Subsequently‚ the extraction and evaporation did not produce the expected oil. This result is probably due to the collection of only water vapor during distillation. From another group’s data‚ 3.80% of the oil was recovered from the cloves in which the major component is eugenol
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Principles of Distillation What is distillation? Simply‚ distillation is the process in which a liquid is vaporized (turned to steam)‚ recondensed (turned back into a liquid) and collected in a container. Nature uses a form of distillation to turn salt water (seawater) into fresh water (rain). Why do you use distillation to recycle waste solvents? Solvent-based waste contains volatile material (solvents) and non-volatile material (contaminants like paint‚ ink‚ grease‚ fiberglass‚ etc.). Many of the
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Purpose: The purpose of this experiment is to determine the number of moles of water molecules of crystallization of a sample of hydrated Barium Chloride. This can be calculated using Gravimetric Analysis and to indirectly determine the percent composition of a hydrate by taking advantage of its chemical properties. Introduction: Gravimetric procedures are analytical methods in which the results are determined from the masses of starting materials and products. These methods
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Fractional Distillation of GSM Blue Pamela Trix Lanaja‚ Jonathan M. Librojo‚ Shaun Therence Mabunay and Carissa Mae Magdaleno 3Bio3‚ Department of Biology‚College of Science‚ University of Santo Tomas‚ Manila‚ Philippines Abstract G.S.M. Blue is composed primarily of water‚ sugar cane alcohol with essences of juniper berries and other botanicals with traces of impurities and flavourings and it has 32.5 percent alcohol by volume (65 proof). The experiment aimed to separate its
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Results | 9-11 | 6) Discussion | 12 | 7) Conclusion | 13-14 | 8) References | 15 | ABSTRACT This experiment is about steam distillation by using Dalton’s Law. The objectives of this experiment are to demonstrate a separation of a mixture by using steam distillation and next to prove that Dalton’ Law and ideal gas law are applicable in steam distillation. Dalton’s Law; While Ideal Gas Law; This experiment is conducted by placing 2mL of Turpentine and 15mL of water into
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