Fractional Distillation Name: Pinaki Das Partner’s Name: Alice Kim Course: Advance Science Grade 9 Slot: B Date: November 6th 2013 Fractional distillation separates a mixture of liquids based on differences in the boiling points of the liquid. The purpose of this experiment was to identify
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Acetyl chloride‚ CH3COCl‚ also known as ethanoyl chloride or acyl chloride‚ is an acid chloride derived from acetic acid. It belongs to the class of organic compounds called acyl halides. It is a colorless liquid. Acetyl chloride does not exist in nature‚ because contact with water would hydrolyze it into acetic acid and hydrogen chloride. In fact‚ if handled in open air it gives off white smoke owing to the hydrolysis from the moisture in the air. The "smoke" is actually small droplets of hydrochloric
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eugenol in the basic aqueous layer‚ and acetyleugenol in the organic layer. The basic aqueous layer can be acidified to re-extract eugenol from it. And the organic layer can be dried and concentrated to yield acetyleugenol The principle of steam distillation is based on the fact that two immiscible liquids will boil at a lower temperature than the boiling points of either pure component‚ because the total vapor pressure of the heterogeneous mixture is simply the sum of the vapor pressures of the individual
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100 5 50 100 For A compound = 78-82oC For B compound = 100oC 4. What is the mole fraction of each component if 3.9g of benzene(C6H6) is dissolved in 4.6g of toluene (C7H8) Mole of benzene=3.9g\(6*12+6)g\mol = 0.05 mol Moles of toluene=4.6g\(7*12+8)g\mol =0.05 mol Mole fraction of benzene=mole fraction of toluene = 0.05\(0.05+0.05)
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3.3 Results and Discussion 3.3.1 Particle Size of Asphaltenes. DLS was utilized to obtain the hydrodynamic radius of asphaltenes in toluene‚ which could help understand the behaviors of asphaltenes in the bulk solutions and oil/water interfaces. Figure 1 shows the particle size distribution of asphaltenes under different concentrations at 23 ℃ and under 2000 mg/L at different temperatures. A summary of the average particle size under different concentration and temperature conditions is shown in
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We reached our goals through our experimentation. We tested the solubility of each of the starting and ending materials in water‚ HCl‚ NaOH‚ toluene‚ and acetone. We discovered that the starting materials would only dissolve in toluene. To make the soap‚ we obtained about 10 mL of vegetable oil and 10 g of lard and we placed them both in separate 250 mL beakers. While we were stirring the compounds‚ we also added 15 mL of 6 M NaOH drop by drop and 1 mL of glycerol. We then heated our solutions
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MEMORANDUM From: To: Subject: Calcium Chloride Best Purchase for Deicing Enclosures: (1) Data Record (2) Data Treatment (3) Environment Impact Research After hours of vigorous examination‚ we have come to the conclusion that calcium chloride (CaCl2) would be the best deicer to use on a naval base over sodium chloride (NaCl) and ethylene glycol (C2H6O2). In order to melt ice‚ deicers lower the freezing point so that the ice melts at lower temperatures. CaCl2 has
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Title: Distillation of an Ethanol Using Fractional Distillation Lab Report Abstract: This experiment aimed to separate the components of a mixture using Fractional Distillation. A volume of 28.0mL of a mixture including ethanol was heated until the temperature reached 78.0 C. Approximately 1.0mL of distillate was collected between 78.0 – 84.0 C. Percent composition by weight of the 1.0mL sample was determined to be 95% ethanol. By careful and accurate techniques‚ a high percent composition
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Distillation Column In the the Chemical Enginneering Lab at CSULB there is a total reflux eight-stage glass binary distillation column at atmospheric pressure. The components that need to be separated are 1-propanol and 2-propanol. These two compounds are isomers with fairly close boiling points. They are separated based on their physical propertis. With the
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Steam Distillation Purpose: To use steam distillation to purify heat sensitive‚ natural products‚ like essential oils. Procedure Please refer to: Williamson‚ Macroscale &Microscale Organic Experiments 4th Ed.‚ pgs.98-109 Results Table 1.1: Steam distillation Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water 1 100.3 Water added 2 100.5 3 100.5 Water added 4 100.6 Water added 5 100.6 6 100.6 Water added 7 100.6 8 100.6 Water added 9 100.3 10 100.6
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