laboratory techniques including proper mixing in an oxidation reaction‚ extraction‚ infrared spectroscopy‚ and gas chromatography. Reactants cyclohexanol and sodium hypochlorite (NaOCl) undergo a redox reaction and when combined with the catalyst acetic acid (HOAc) and solvent water (H2O)‚ form the product cyclohexanone along with sodium chloride (NaCl) and water. In the overall Figure 1: Cyclohexanol Reaction oxidation-reduction reaction‚ the secondary alcohol of cyclohexanol is oxidized to form
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Experiment 8 Chemical Kinetics Abstract This experiment was done to determine the effects of the nature of the reactants‚ concentration‚ temperature‚ surface area and catalyst on the rate of chemical reactions. The nature of the reactants implies a difference if the reactants are aqueous or organic‚ acidic or basic or if they occur in the same phase or not. Acid-base reactions‚ formation of salts‚ and exchange of ions are fast reactions while reactions in which large molecules are formed
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Abstract The purpose of this experiment was to perform a liquid-liquid extraction method to extract the caffeine from the tea bags that were provided‚ and then recrystallize the caffeine. The solvents used in the experiment were an aqueous sodium carbonate and dichloromethane (DCM). Anhydrous calcium chloride pellets were used to dry the solution and emulsion layer and the DCM was then decanted. After washing the anhydrous calcium chloride pellets with more DCM‚ the solvent was evaporated‚ leaving
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put it into the 100mL beaker‚ add your 25mL of distilled water and stir to form the calcium chloride solution. Next‚ use stoichiometry to determine how much Na2CO3 and put it into a small paper cup. Then add the 25mL of distilled water to make the sodium carbonate solution. Mix the two solutions in the beaker and a precipitate of calcium carbonate will form instantly. Next‚ set up your filtration assembly. After the filtration assembly is ready‚ swirl the contents of the beaker to dislodge any precipitate
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particularly in the determination of silica in iron and steel and in cement and other silicate materials. It is also used as a solvent for sulfide ores for the determination of copper and other metals‚ in the separation and determination of the alkali metals sodium and potassium. In the manufacture of anhydrous magnesium perchlorate‚ the best of the absorbents for water in analytical work. It is also a strong standard acid for the titration of bases. A chemical reaction that takes place is actually in the
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results in the confirmatory tests and (3) point out suitable conditions necessary for the detection process and the reasons for such conditions. II. Methodology A. Materials and Apparatus The chemical used in the experiment are as follows: HCl‚ sodium ions‚ ammonium carbonate‚ barium nitrate‚ acetic acid‚ potassium chromate‚ ammonium hydroxide and potassium oxalate. The apparatus used include spot plates/watch glass‚ nichrome wire‚ alcohol lamp‚ salt‚ water and stirring rod. B. Procedure We obtain
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General Chemistry Laboratory 151 Chemiluminescence Introduction: The objective of tis experiment was to carry out systematic series of experiments in order to determine which chemicals and which ratios of chemicals produce the brightest light. Also‚ this experiment will determine which chemical produces the longest light. Chemiluminescence is the emission of light (luminescence)‚ as the result of a chemical reaction. There may also be limited emission of heat. This occurs because the
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Lab: 5 Experiment:13 Pre-Lab The purpose of this experiment is to observe an equilibrium reaction counteracting changes to it’s system all in accordance to Le Chatelier’s principle. An equilibrium reaction can be pushed toward products or reactant based on changes in temperature or concentration. The reversibility of reaction will also be looked at. Pre-Lab questions 1. The concentrations of products and concentrations of reactants remain constant but both reactions
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evaporation when forming crystals. Phenolic compounds will undergo salt formation with sodium hydroxide solution‚ NaOH.Therefore‚sodium hydroxide solution is allow to use to extract a carboxylic acid or phenolic compound from its solution in an organic solvent.An organic solvent can be used to remove organic impurities from a carboxylic acid or phenol dissolved in aqueous sodium hydroxide.Aqueous solution of Sodium
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Muscle and Nerve Preparation Preparation of Ringer ’s solution Dissolve 6.5 g of sodium chloride (NaCl)‚ 0.14 g of potassium chloride (KCl)‚ and 0.20 g of sodium bicarbonate (NaHCO3) in 800 mL of distilled water. Also‚ dissolve 0.16 g of hydrated calcium chloride (CaCl2.2H2O) and 0.39 g of hydrated magnesium sulfate (MgSO4.7H2O) in 100 mL of distilled water. Add the 100 mL cautiously to the 800 mL‚ stirring vigorously. Then make the final volume equal to 1 liter by adding more distilled water
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