John Heger CMY 211 Lab Section 13 11-30-2011 Borohydride Reduction of Vanillin to Vanillyl Alcohol Introduction: The purpose of this lab was to reduce vanillin to vanillyl alcohol. This lab report recaps the procedure and results of the lab. The chemical process studied in this lab was reduction‚ the process of reducing the number of bonds to oxygen and increasing the number of bonds to hydrogen. Other chemical processes included in the lab were recrystallization‚ melting point‚ and extraction
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Title: Preparation and Standardization of a Sodium Hydroxide Solution Objective/Purpose: The objective of this experiment will be the standardization of sodium hydroxide using potassium hydrogen phthalate by the titration method. Introduction: The concentration of solutions can be reported in terms of molarity and normality. Molarity is equal to: HCL‚ HBR‚ H2SO4‚ HNO3 M = mol Solute (mol) (Monoprotic) (Diprotic) _______________ V(L)g solutions (L)
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covalent compound because both hydrogen and iodine are nonmetals. 6) Why would the bulb light up when placed in an aqueous solution of sodium chloride but not in a solid sample of sodium chloride? In a solid sample of sodium chloride‚ sodium and chloride are bonded together ionic and so there aren’t any free electrons to support the flow of electricity. When sodium
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Experiment 7 Investigating Stoichiometry with Sodium Salts of Carbonic Acid Introduction: The student will perform the experiment in order to find the percent yield by using the theoretical value found using the balanced equation for sodium carbonate as well as sodium bicarbonate. The objective is to stabilize the substances by titrations and finding the percent yield when all the data is collected. The purpose of this procedure is so that the student will get better understanding of stoichiometry
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Preparation of Sodium Chloride through titration Abstract: acid-base titration is a technique commonly used to determine the moles of acid in a sample by adding a known volume of strong base of a known concentration. The strong base provides the hydroxide ion‚ to react quantitatively with the acid. The point at which the acid is completely and exactly consumed the known quantity of base is called the equivalence end point and is signalled by a colour change in the solution (end point). This colour
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The chemical equation for Thiopental Sodium is C11H17N2NaO2S. First synthesized in 1935‚ the proper name for the drug is Thiopental Sodium it also goes by Sodium Pentothal but that is actually a trademark of the drug ’s manufacturer‚ Abbott Laboratories. A yellow water-soluble crystal‚ it is classified as an ultra-short acting barbiturate‚ a type of drug that depresses the central nervous system‚ slowing the heart rate and lowering blood pressure. Widely used in medicine as an anesthetic during surgery
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FormulaMolecular Weight (g/mol)Density(g/cm3)Melting Point(oC)Boiling Point(oC)HazardO-vanillinC8H8O3152.15-42.5265-266Harmful andIrritantFor all 3vanillinC8H8O3152.151.05680-81285isovanillinC8H8O3152.15-113-115179Vanillyl alcohol*C8H10O3154.17-113-115--Sodium hydroxide**NaOH39.992.13181390CorrosiveHydrochloric acidHCl36.461.18-26110CorrosiveSodium borohydrideNaBH437.831.074505400IrritantCorrosive*Vanillyl alcohol is soluble in cold organic solvents such as ether/alcohol and hot water‚ but insoluble in
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PurposeIn this experiment‚ sodium hypochlorite (NaOCl) in acetic acid mixture was used to oxidize emdo-borneol (an alcohol) to camphor (a ketone). The product would then be purified by sublimation and then be analyzed by Infrared spectroscopy and melting point test. Procedure and ObservationsPlease refer to the lab manual and the carbon copy attached. Data and CalculationsWeight of endo-borneol = 0.2013gNo of moles of endo-borneol = 0.2013g/154.25g mol-1 = 1. 305mmolSince one mole of endo-borneol
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this goal by creating five reactions containing Sodium Sulfate that would confirm our compound and show its chemical properties. In each reaction‚ we replaced the presence of Sodium Sulfate with our unknown. Our first reaction was the reaction from the sulfate anion test between Sodium Sulfate and Barium Chloride. If the compound was in fact Sodium Sulfate it would produce a white precipitate and it did. The second reaction was first between Sodium Sulfate and Hydrochloric Acid‚ and then Silver Nitrate
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that were added from the burette is 0.00327 moles (1 tablet of Gaviscon). However‚ for Quick-eze‚ the number of moles is 0.00216 moles (1 tablet). This means the average volume of the NaOH have affected the number of moles as the concentration of the sodium hydroxide is 0.1M. This means that if less NaOH was required to neutralise the acid‚ the number of moles of HCl neutralized by the ant-acid would be greater. For example; by using mole ratio‚ the number of moles of HCl reacted with the NaOH is 0.00216
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