Experiment 5B: Ketone Reduction Objective: Using sodium borohydride as a reducing agent‚ the ketone 4-tert-butylcyclohexane is reduced to its corresponding alcohol. It is purified through extraction techniques to give the cis and trans diasteromer products. Procedure: The procedure was followed as outlined in Mayo’s book for Experiment 5B with the following modifications: 1. Reagents and Equipment – The reaction will be on a scale of 2X what is described in the text. 2. Reagents and Equipment
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12-STANDARDIZATION OF SODIUM HYDROXIDE Standard solutions for titrations are especially pure mixtures with exactly known concentrations. Primary standards are very pure solids. They have the advantage that they can be weighed (the analytical balance is normally the most accurate instrument in the laboratory) and they are stable under laboratory conditions. In this experiment‚ the primary standard is oxalic acid dihydrate‚ H2C2O4 ( 2H2O. It will be used to standardize a solution of sodium hydroxide
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believe that if the amount of sodium citrate is too low or too high‚ the sodium alginate solution would not form into a ball. The recommended amount of sodium citrate to be added to the sodium alginate solution was ⅛ teaspoon‚ or 0.5 grams. We supposed that if we exceeded this measurement‚ the sodium citrate would unbalance the whole solution‚ making the balls deform. If we added too little of the sodium citrate‚ we thought that there would be too little for the sodium citrate to fully do its job of
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Lab 4. Volumetric Determination of Impure Sodium Carbonate (Na2CO3) Introduction: To determine the total amount of carbonate in unrefined sodium carbonate‚ soda ash‚ a titration is done using a standardized solution of HCl. Aqueous HCl is a strong acid and therefore almost completely disassociates into H+ and CL-. Therefore‚ when HCl is used in a titration‚ the H+ is the titrant. Carbonate in aqueous solution is able to accept a proton‚ i.e. it acts as a base. When carbonate accepts the H+ a bicarbonate
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2. An aqueous solution of KCl is colorless‚ KMnO4 is purple‚ and K2Cr2O7 is orange. What color would you expect of an aqueous solution of Na2Cr2O7? Explain. Orange. 3. Explain why hexane will dissolve benzene but will not dissolve sodium chloride. Sodium chloride is an ionic compound. 4. Some drinks like tea are consumed hot or cold‚ whereas others like Coca-Cola are consumed only cold. Why? For taste reasons‚ these drinks can be drunk if the user likes It but having coca cola like tea
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eLearning 2009 Publication No. 91860 Rate of Reaction of Sodium Thiosulfate and Hydrochloric Acid Rate Laws Introduction The purpose of this demonstration is to investigate the effect of sodium thiosulfate concentration on the rate of reaction of sodium thiosulfate with hydrochloric acid. The reaction‚ which produces solid sulfur‚ will be followed by measuring the time needed for the reaction mixture to become opaque. The results will be analyzed graphically to determine the order of
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Analysis of Soda Ash and Volumetric Analysis of a Carbonate-Bicarbonate Mixture Buti‚ Mary Daphne A. Department of Chemical Engineering‚ Faculty of Engineering University of Santo Tomas España‚ Manila Abstract Sodium carbonate (Na2CO3)‚ commonly known by trade name soda ash‚ is a white‚ anhydrous‚ powdered or granular material that is an essential raw material used in the manufacturing of glass‚ detergents‚ chemicals‚ and other industrial products. In this experiment‚ the percent alkalinity
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Review of Related Literature Calamondin or Clamansi‚ Citrofornella microcarpa‚ belong to the fruit tree family Rutaceae. The fruit of the Calamansi is a small‚ round lime‚ a little bigger than the size of a thumbnail‚ about 30 mm (an inch) in diameter. Similar to other citrus fruits‚ the calamansi is high in vitamin C‚ and the juice can be an excellent vitamin basis. The lively ingredient D-limonene destroys the wax coating of the insects’ respiratory system
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liquid soaps‚ shampoos and soft soaps because it produces soap of soft consistency and higher solubility in water. Other raw materials: * Builders These are essentially used to build up soaps. Examples of alkali builders are sodium carbonate‚ sodium silicate and sodium sulfate.
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Chemical Reactions- Sodium Hydroxide A chemical reaction is a change where two or more substances are changed into a new substance. You can identify a chemical reaction by colour change‚ effervescence (bubbles)‚ when light or heat given off‚ and the change is usually irreversible. There are 6 main types of chemical reactions- combustion (often called burning)‚ synthesis‚ decomposition‚ neutralization‚ single replacement and double replacement. A combustion reaction is a reaction with oxygen‚ and
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