Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method used for the
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The Purity and Purification of Solids Recrystallization ABSTRACT In this experiment‚ impure adipic acid is purified though recrystallization. The impure adipic acid is dissolved in a solvent. After cooling it is ran through a vacuum filter to separate any moisture. The dry crystals are then weight for percent yield and the melting point range is taken to test the purity. There were two different trials ran in this experiment. The difference between the two was the addition of charcoal in
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Lab #5 Questions and Answers 1. Which tool is better at performing protocol captures and which tool is better at performing protocol analysis? Wireshark is better for performing protocol analysis and Netwitness Investigator is best at performing protocol captures. Wireshark does well at both aspects‚ which makes it a little better. 2. What is promiscuous mode and how does this allow tcpdump‚ Wireshark‚ and NetWitness Investigator to perform protocol capture off a live network? Promiscuous
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Lab 5 Assessment Questions 1. What are the three major categories used to provide authentication of an individual? a. Password b. Token c. Shared Secret 2. What is Authorization and how is this concept aligned with Identification and Authentication? Authorization is a set of rights defined for a subject and an object; this concept is aligned with Identification and Authentication because these are the 3 steps to the access control process 3. Provide at least 3 examples of Network Architecture
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Abstract The objective of this lab was to determine the convective heat transfer coefficient of a heated sphere in an quiescent environment. In the experiment a hot brass sphere was put into water and cooled. The temperature of the sphere was recorded over a time of 600 seconds to see how it cooled and given temperature was recorded every 20 seconds. Results were then calculated at both of the time values 300 and 600 seconds. For the experimental results at time 300 seconds‚ the Rayleigh number
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Title: Lab #3 Separation of a Mixture of Solids Purpose: To understand the different separation methods and techniques that depend on the chemical properties of a specific substance. Also to become more comfortable with performing those actions of separation so I have them in the future. For this experiment‚ I will separate a mixture of four distinct substances: sodium chloride‚ benzoic acid‚ silicon dioxide‚ and iron fillings into pure beings. Procedure: Materials: distilled water coffee
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Experiment 3 Liquid-Liquid Extraction Discussion The success of extracting each compound out of the solution can be seen in the IR graphs for each substance. For ethyl 4-aminobenzoate‚ the N-H‚ C=O and C-O are distinguishable in their proper wavenumber positions. The amino N-H stretch was found between 3224 cm-1 and 3423 cm-1. The C=O was found at 1681 cm-1 and the C-O was at 1280 cm-1. The IR for benzoic acid also displays its significant bonds‚ O-H and C=O. The O-H was between 2566 and
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LAB 02: Measuring and Dispensing Liquids Introduction Pipetting is one of the most important and basic skills when it comes to experimental science. Good pipetting skills allow an individual to put trust in his or her results‚ prevent waste of materials‚ and assure reproducibility of results. In order to correctly pipette liquids‚ the volume range must be first determined. p1000 micropipettes have a volume range of 200 - 1000 uL‚ p200 micropipettes have a volume range of 20 - 200 uL‚ and p20 micropipettes
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Post-Lab Report for Experiment 2: Cooperative Identification of an organic Solid October 6‚ 2013 Introduction: This experiment was focused on the cooperative identification of organic compound by its chemical properties such as: slow melting point‚ mixed melting point‚ Rf values in TLC experiment‚ IR spectrum analysis‚ and H NMR spectra. Such data can provide the the identity of functional groups and the identity of the compound itself. In this experiment
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Lab 2 “Separation of a Mixture of Solids Lab Report Assistant (10 points) Data Table 1: Experimental Data Grams Percent of mixture Iron (Fe) fillings 0.9 g 20 % Sand 1.2 g 25 % Table salt 1.6 g 25 % Benzoic acid .8 g 16 % Total 4.5 g 86 & Questions A. How did your proposed Procedures or flow charts at the beginning of this experiment compare to the actual Procedures of this lab exercise? (2 points) I proposed a magnet would be the used to remove the iron from
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