MIXTURE INTO ITS COMPONENTS BY FRACTIONAL CRYSTALLIZATION Introduction: Fractional crystallization is one of the experimental techniques used to separate or purify mixture. Fractional crystallization makes use of the differences of solubility to separate the components of a mixture. Goals: Applying fractional crystallization to separate a mixture of salicylic acid and copper sulfate pentahydrate into its components. Calculate the percent of salicylic acid and copper sulfate pentahy-
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Name: Allison Bynum Date:6/17/14 Exp 8: Ionic Reactions Lab Section: 75426 Data Table: Record your observations in the following table Na3PO4 NaI Na2SO4 NaCl NaHCO3 Na2CO3 NaOH Co(NO3)2 Created a musty looking cloud that later turned dye to a purple shade No change‚ brought out pink very slightly No change No change Created a cream looking liquid‚ did not mix with pink substance Darkened color‚ changing to more of a purple tint as time passes on. Immediately turned
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Crystal making lab Purpose: To better understand saturated solutions‚ solubility . Analysis: 2. Why was it necessary to heat the water? Be specific. Heating the water allows it to hold much more borax in solution than it could at room temperature. So after the water cooled‚ the ability of the solution to hold the solute inside decreases‚this causes the excess borax in the solution to precipitate in crystal form on the string.When the water at a high temperature‚ water molecules have more kinetic
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This is where you can find the following instruction for this experiment. In the pre-lab notebook the experiment is explained in full details which will specify that there were no changes made to the experiment. Calculations: Theoretical Yields: 1.094g benzophenone * (1 mol benzophenone/ 182.22 g benzophenone) = 0.006003732 mol benzophenone 0.006003732 mol benzophenone * (1 mol triphenylmethanol/1 mol benzophenone) * (260.33 g triphenylmethanol/ 1 mol triphenylmethanol) = 1.562951552 g triphenylmethanol
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esterification reaction that was carried out in this lab is shown in figure 1. It worth mentioning that the by-product of such reaction is water. In organic chemistry‚ the reaction in which water molecule is released is known as condensation reaction (Hornback‚ 2006). Figure1 is drawn using Chem Sketch software. a) b) Figure 1: Typical Fischer esterification reaction (a) in comparison to the specific esterification reaction used in this lab (b) The reaction can also be categorized in terms of
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Lab Report Name: _____ Date: ______ Ionic Reactions List all of the cations used: Cobalt‚ Copper‚ Iron‚ Barium‚ Nickel List all of the anions used: Phosphate‚ Iodide‚ Sulfate‚ Chloride‚ Bicarbonate‚ Carbonate‚ Hydroxide Compare your results with the solubility rules and/or solubility table in your chemistry text. QUESTIONS: A - Do your results agree with your expectations
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The Mass of Acetylsalicylic Acid in Aspirin ------------------------------------------------- Purpose The purpose of the lab is to determine the mass of the ‘active ingredient’ in a commercial ASA tablet. ------------------------------------------------- ------------------------------------------------- Introduction There are three main theories surrounding acids and bases including the Arrhenius‚ Bronsted-Lowry‚ and Lewis theories. The Arrhenius theory of acids and bases states that
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| Reactions of Grignard Reagents with Carbonyls | | | Tuesday 1:30 | 2/28/2012 | | Introduction This experiment explores the reactivity pattern for the addition of Grignard reagents to three different carbonyl groups: a ketone‚ an ester‚ and a carbonate. Grignard reagents are organometallic compounds that have a carbon-metal bond‚ such as carbon-magnesium. Grignard reagents are formed from the reaction of an alkyl‚ cycloalkyl‚ or aryl halide and magnesium metal in dry ether
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depending on the number of alkyl substituents directly attached to the carbon attached to the halogen atom. The purpose of this lab was to properly prepare t-butyl chloride from t-butyl-alcohol in a concentrated hydrochloric acid. The reaction occurs through a nucleophilic substitution‚ which is when a nucleophile replaces the leaving group in the substrate. In this lab‚ the hydroxyl group of t-butyl alcohol is replaced by a chlorine atom. The reaction proceeds through an SN1 mechanism (Weldegirma
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Purpose: To find out the densities and to find out the name of the unknown metals. (Based on the extensive and intensive properties) Check up the words mass‚ volume‚ density‚ extensive properties‚ and intensive properties. Where do the units for mass and volume) come from and what do they mean? What is the density of distilled water? What is Archimedes principle? Does temperature affect the density of a solid? Liquid? Gas? Materials: Safety glasses‚ 10‚ 25 or 50 mL graduated cylinders
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