EXPERIMENT 13： Extraction: Extraction with acid and alkali Objective 1. To recover the benzoic acid and p-dichlorobenzene from its mixture from its mixture by using acid-alkali extraction. 2. To determine the percentage recovery and melting point of the recovered benzoic acid and p-dichlorobenzene. Introduction Acid-base extraction is a process which purifying the acids and bases from mixtures based on their chemical properties. Acid-base extraction is performed to isolate the compounds and natural
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Experiment 1: Observations of Chemical Changes Lab Partners: None Date of Experiment: February 25‚ 2015 Location: My House Abstract: The experiment intended to provide observations of chemical changes as the primary objective. The experiment was divided into two parts‚ first‚ mixing two aqueous solutions of ionic compounds. The second part involved the observance of heating and combustion reactions‚ using the supplied solid elements and compounds. Experiment and Observations: The first part of
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Abstract-Timur Solid phase extraction is a sample preparation technique that overperform liquid /liquid extraction in its efficiency‚ labor intensity and waste disposal. The purpose of this lab is to learn how SPE can be used to identify trace amounts of Vanillin. Stock solution of vanillin in water with concentration of 50 ppm was prepared. Four solutions with concentration of 5 ppm‚ 1 ppm‚ 0.5 ppm and 0.1 ppm were made from stock solution. UV-Vis spectra of standard solution was recorded at 229
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To calculate the yield of acetylferrocene and the percent recovery of unreacted ferrocene. Table of Quantity showing various physical properties Type of substance Molecular Formula Molecular Weight (g/mol) Density(g/cm3) M.P.(oC) B.P.(oC) Solubility Ferrocene C10H10Fe 186.03 1.49 172 oC-174 oC 249oC Insoluble in water‚ soluble in organic solvent Acetyl-ferrocene C12H12FeO 228.08 - 81 oC -83 oC 161 oC - 163 oC (at 4 mm) Very slightly soluble in water‚ soluble in organic solvent Ethyl Acetate
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Student Number Mark / 39 Chemistry Preliminary Course Final Examination • 2006 General Instructions • • • • • • • Reading time – 5 minutes Working time – 45 minutes Write using black or blue pen Draw diagrams using pencil Board-approved calculators may be used A Data Sheet and a Periodic Table are provided Write your Student Number at the top of this page Total Marks – 39 Part A – 10 marks • Attempt Questions 1 – 10 • Allow about 10 minutes for this part Part B – 29 marks • Attempt
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material and at the same time you will be exposed to several techniques and procedures which are fundamental for survival in an organic chemistry lab. You have been exposed to most of them during your CHEM 250 laboratory session. Please refer to the Laboratory Techniques TECH 1 to 7 and familiarize yourself with the content. For example during this lab you will be doing extraction and TECH 6 describes the theory behind it and how to handle separatory funnel. using a drying agent and in TECH 6-5
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Much can be learned from studying an organisms DNA. The first step to doing this is extracting DNA from cells. In this experiment‚ you will isolate DNA from the cells of fruit. Materials (1) 10 mL Graduated Cylinder(2) 100 mL Beakers15 cm Cheesecloth1 Resealable Bag1 Rubber Band (Large. Contains latex pleasewear gloves when handling if you have a latex allergy).Standing Test TubeWooden Stir StickFresh‚ Soft Fruit (e.g.‚ Grapes‚ Strawberries‚ Banana‚ etc.) ScissorsDNA Extraction SolutionIce Cold EthanolYou
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for thinking. It also relaxes blood vessels and increases urination. Other than tea leaves‚ caffeine can also be found in coffee‚ cocoa beans and kola nuts. Tea leaves consist mostly of cellulose‚ caffeine‚ and a small amount of chlorophyll. The solubility of caffeine in water is 22 mg/ml at 25·C‚ 180 mg/ml at 80·C‚ and 670 mg/ml at 100·C. [1] There have been several concerns about the health risks of caffeine‚ although scientists have already said that normal consumption
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ANIONS: CO32- ‚ S2- ‚ SO32- ‚ SO42- ‚ NO2- ‚ NO3- ‚ Cl- ‚ Br2- ‚ PO43- ‚ CH3COO- _______________________________________________________________ PRELIMINARY TESTS 1. Note the state (amorphous or crystalline) and colour of salt. 2. Test the solubility of the salt in the following solutions: i. Water (cold and hot) ii. Dilute HCl (cold and hot) iii. Dilute HNO3 (cold and hot) _______________________________________________________________ IDENTIFICATION OF ACID RADICALS (ANIONS) This part
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10. The gravimetric determination of nickel in alloys Gravimetric analyses belong to the most precise‚ because contemporary analytical balances make possible determination of the mass of a sample with great accuracy. In these analyses one should obtain high purity compound of the analyzed element or a compound directly obtained from the analyzed substance). This reaction has to be exactly stoichiometric. It is also important that the weighed compound was non-hydroscopic and stable in air‚ it also
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