| Discussion: Recrystallization is a widely-used technique to purify a solid mixture. The desired product is isolated from its impurities by differences in solubility. Insoluble impurities and colored impurities can be removed from hot solvent through the use of activated carbon and filtration. Soluble impurities remain in the cold solvent after recrystallization. The desired product should be as soluble as
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Experiment 1: Study of Solubility Equilibrium Data Treatment and Analysis Section 1: Solubility Product Constant Temperature (˚C) | Volume of NaOH used (mL) | | | | Titration 1 | Titration 2 | Average | 28 | 12.7 | 12.8 | 12.75 | 9 | 10.5 | 10.5 | 10.5 | 19 | 11.3 | 11.2 | 11.25 | 40 | 16.2 | 16.2 | 16.2 | 50 | 22.8 | 22.9 | 22.85 | Table 1: The volume of NaOH used in the titration at various temperatures. No. of moles of KHC4H4O6 = 1.45 g ÷ 188.177g/mol = 7.71 x 10-3mol
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impurities have on the melting point of an organic compound? Soluble impurities affect the melting point of a solid in the following manner. a. The presence of an impurity in the molten compound reduces its vapor pressure thus lowering the melting point of the compound. b. Broaden the melting point range. 2. For what tow purpose are melting points routinely used a. To determine the identity of an organic solid. b. To determine the purity of an organic solid. 3. What effects on the measured melting
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Modeling Effective Dose: Salt Tasting lab Purpose The purpose of this lab is to see at what measurements (of salt) can the salt be detected by taste. Abstract The science of toxicology is based on the principle that there is a relationship between a toxic reaction (the response) and the amount of poison received (the dose). An important assumption in this relationship is that there is almost always a dose below which no response occurs or can be measured. A second assumption is that once a maximum
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equal each other. At this point‚ the concentrations do not change with time. These reactions are said to be in equilibrium. Equilibrium is depended on a particular temperature‚ and the concentrations of reactants and products have to follow a rule demonstrated by the equilibrium constant Kc. The equilibrium concentrations that will be studied is the reaction between iron (III) ion and thiocyanate ion: The mixture of Fe3+ and SCN- react to form a compound that produces a dark brown/red color. Since
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Acids There are relatively few suitable tests for carboxylic acids. Classification is based mostly upon solubility tests. If the compound is water soluble‚ test the aqueous solution of your compound with pH paper (also check the pH of the original water). If the compound is water-insoluble and it dissolves in 5% (1.5M) sodium hydroxide and 5% NaHCO3 solutions as performed in your solubility tests‚ it can be classified as a carboxylic acid. Establish an equivalence value for the unknown to estimate
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The Effect of Temperature on Solubility By Aviraj Singh Rogers 2 Background: The solubility of most solid substances is generally said to increase as the temperature of the solvent increases. However‚ some substances‚ such as ytterbium sulfate‚ do the opposite. This can be explained through the Second Law of Thermodynamics which states that “in all energy exchanges‚ if no energy enters or leaves the system‚ the potential energy of the state will always be less than that of the initial state”
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The spring constant Manuel Cereijido Fernández – UO237242 PL-4 -----------------------------------------------------------------------------------1. Objectives The main objective of this experiment was to determine the spring constant using the dynamic method. 2. Theoretical fundamentals On the one hand‚ when a spring oscillates‚ the movement which describes can be classify as a simple harmonic motion. Therefore‚ its position‚ velocity and acceleration equations respect the time will
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The Equilibrium Constant of an Ester Hydrolysis Reaction CHM 152LL Section 33263 March 28‚ 2014 John Weide Abstract: The purpose if this experiment is to determine the equilibrium constant of an unknown alcohol. In this experiment unknown alcohol number three and unknown ester number three were used. The equilibrium constant was found by titrating a series of reactions containing H2O‚ HCl‚ and the unknown ester with only the last solution containing the unknown alcohol
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NOTES - SALT ANALYSIS S.No. | EXPERIMENT | OBSERVATION | INFERENCE | 1(a) | Noted the colour of the salt | BluePale greenGreenPale pinkColourless | May be Cu2+May be Fe2+May be Ni2+‚ Cu2+May be Mn2+Absence of Cu2+‚ Fe2+‚ Ni2+‚ Cu2+‚ Mn2+ | (b) | Noted the physical state of the salt | (i)Amorphous(ii)crystalline | May be CO32-May be Cl-‚ Br-‚ SO42-‚ NO3- | 2 | Action of heat:The given salt is heated in a dry test tube. | (i)Reddish brown vapours(ii)Crackling sound(iii)Yellow when salt and white
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