Lab #5: Grignard Reaction – Synthesis of Triphenylmethanol John Kang Chem 152L Performed: 7/20/04 Date submitted: ________________ Lab Partners: Sang Lee‚ Vicky Lai TA: John Stanko Abstract: This experiment explored the synthesis of triphenylmethanol through the use of Grignard reagents. The percent yield of the product was 10% on a relatively humid day. The melting point was calculate to be 127.2oC with a literature value of 162oC. An IR spectrum of the product was taken and used
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Separating the components of Panacetin Umar Hussaini Sneha Ray 9/30/14 Abstract In this lab we separated components of a simulated preparation‚ panacetin and making use of its acid base properties. To obtain such a pure compound‚ the compound we want must be separated from its other natural components‚ which can be done by manipulating physical and chemical properties. Panacetin contains sucrose‚ aspirin and an unknown which can be acetanilide or phenacetin in which phenacetin
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The objective of this experiment was to synthesize 3-nitrochalcone from 3- nitrobenzaldehyde. This was accomplished with a Diels-Alder reaction that utilized 3-nitrobenzaldehyde and acetophenone. After the reaction was completed‚ purification of the product was conducted using semi-microscale recrystallization. The melting point of the product was 136-141 oC‚ which is in the close vicinity of the literature melting point of 146 oC. The theoretical yield of 3-nitrochalcone was 0.253g and the
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Bromination Solo Experiment 3 – Individual Lab Report (Save as pdf and submit‚ due by 12:00 NOON one week after experiment) Last Name: First Name: TA Name: Date Lab Performed: Date Lab Submitted: Group A‚ B‚ or C: Comments for Grading TA: (Please indicate if you performed the lab on a day other than your regularly scheduled day and/or with a TA other than your regular TA). Page Limit: report must not exceed FIVE pages (including this page) LIMIT DOES NOT INCLUDE ANY GRAPHS‚ SPECTRA
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In part 1 the results of the solubility do not agree with the with rules of solubility most likely because we put too much solid in the test tubes and not enough water to dissolve it. They should have dissolved because the anything with nitrate should be soluble. With the pH‚ when the mixture where compared with the chart all of them except NaCl where a shade of blue which means that they have a pH of 8-14‚ depending on the darkness of the shade‚ meaning that they are a basic solution. When reacting
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EXPERIMENT 1: TITLE: ISOMERISM AND KINETICS IN COORDINATION CHEMISTRY OBJECTIVE: 1. To prepare and study the kinetics of the interconversion of some of the isomers of a typical coordination compound. INTRODUCTION: Isomerism played a central role to establish the basic concept in coordination chemistry while reaction kinetics of coordination compound is known as the area of continuing intense research activity. The mechanism of the reactions of coordination compounds relevance
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CHEMICAL PROCESS PRINCIPLES (CEN 1022) Tutorial 3 : Process Variables 1. The specific gravity of gasoline is approximately 0.70. a) Determine the mass (kg) of 50.0 liters of gasoline. b) The mass flowrate of gasoline exiting a refinery tank is 1150kg/min. Estimate the volumetric flow rate in litres/s. 3. How many of the following are found in 15.0kmol of benzene(C6H6)? a) kg C6H6 b) mol C6H6 c) Ib-mol C6H6 d) mol (g-atom) C e) mol H f) g C g) g H h) molecules
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C. partellus gut protease and protease inhibitor activity assays. C. partellus gut protease activity was estimated using chromogenic substrate BApNA [Manasi A et al.‚ 2005]. It was dissolved in the DMSO and a final concentration was made to 1mM in 1.0ml‚ Glycine-NaOH buffer (pH 9)‚ assays were carried at 38°C for 30min [Manasi A et al.‚ 2005]. The reaction was terminated by adding of acetic acid (30%) of 200µl [8‚ 9‚ Manasi A et al.‚ 2005 ]. Supernatant (0.5ml) was added to 1M NaOH (0.5ml) and the
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According to Stability testing of new drug substances and products‚ a guideline of ICH desires that to clarify the inherent stability characteristics of the active component stress testing was implemented. The aim of this work was to carry out the stress degradation studies on the Lamivudine‚ Abacavir and Dolutegravir using the proposed method. Formulation drug products were exposed to thermal stress‚ oxidative stress‚ photolytic‚ hydrolytic stress under acidic medium and basic medium. An ideal
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Materials and methods Chemicals Triton X-100‚ abscisic acid‚ sodium nitroprusside‚ methyl jasmonate (95%) and phenylalanine were purchased from Sigma Aldrich (Mumbai‚ India)‚ sodium hypochlorite and salicylic acid from Hi-media (Mumbai‚ India). The other chemicals were of analytical grade and obtained commercially. Plant material and callus induction Carrot seeds (var. Atomic red) were collected from Denmark (plantfro). Seeds were surface- sterilized with 75% ethanol for 1 min‚ and then soaked in
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