Abstract: The optical and photocatalytic properties of Nb2O5 sculptured thin films (STF) are investigated. Films are synthesized via sol- gel route using spin coating technique. The sol is prepared from niobium ethoxide. The films are prepared at different rpm to tailor the thickness. The structures of the films are investigated through XRD measurements. Refractive index‚ extinction coefficient and thickness of the films are determined from Variable Angle Spectroscopic Ellipsometery. The absorbance
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References: (1 pt): ACS style guidelines (http://library.williams.edu/citing/styles/acs.php) General quality (3 pts): Grammaer‚ formatting‚ quality of writing‚ etc. Lab practice (2 pts)
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According to the experimental IR spectroscopy for the E isomer of phenylcinnamic acid the peaks of the wavenumber were at 2952‚ 2518 1672 and 1426 cm-1. The peak at 2952 presents the double bond CH stretch for the alkene carbon. The peak at 2518 presents the carboxylic acid –OH peak. The peak at 1672 could present the carbonyl group. The aromatic ring peaks are around 1600 and 1426-1492. Different values could be seen for the z isomer. The wavenumbers for the IR spectroscopy are 3412‚ 3247‚ 1687 and 1552
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Chem-102 Lab Dr. Sobhi Experiment #3: Spectrophotometric Determination of Tartrazine Purpose The objectives of this lab include- illustrating the use of the spectrophotometer in chemical analysis‚ and generating a standard‚ or calibration curve‚ then using that curve to determine the value of an unknown substance. The spectrophotometer is one of the most powerful tools used in chemistry to find the concentration of substances in solution. It compares the colors of a known and an unknown solution
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space provided. 1. What is a particular advantage of graphite furnace atomic absorption over flame atomic absorption? (a) higher temperature (b) lower S/N (c) less interference (d) small sample amounts 2. In atomic emission spectroscopy‚ it is desirable to have a high concentration of the element in the form of: (a) atoms in the ground state (b) atoms in the excited state (c) ions (d) atoms as compounds 3. Which of the following atomic methods generally provide
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Rock crushing‚ splitting samples‚ drying and grinding: Preparation for rock powder. Demonstrator: Encik Zamrut Daunar Date (and venue): 28 July 2010 (Basement) Aim: To crush‚ split‚ and grind solid sample rock for preparing rock powder. Objective: 1. To learn the techniques and mechanisms of preparing rock powder; which will be used as a sample for Bernas Bomb and XRF/ XRD techniques. 2. To know the processes and machines used in the rock crushing and sample preparation. Apparatus/
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De Leon‚ Jo-Anna Maria N. 3ChEA Group No. 2 Experiment No. 5 Spectrophotometric Determination of pKa I. Introduction The equilibrium constant of the dissociation of an indicator in water will be determined experimentally using spectroscopic method.This experiment aims to demonstrate the principle of equilibrium and the interaction of matter with light. II. Methodology Figure . UV-VIS Spectrophotometer 10 solutions covering the entire pH range from 1 to 13 were prepared
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Beer’s Law Lab Hanna Beeter March 15‚ 2013 Honors Chemistry Introduction: In Beer’s law lab the purpose was to find the unknown concentration. The lab included the use of a volumetric flask‚ pipette‚ and spectrophotometer. The spectrophotometer played the biggest part in finding the concentration of the unknown. A spectrophotometer is an apparatus for measuring the intensity of light in a part of the spectrum‚ and is transmitted or emitted on a particular substance. After the number retrieved
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2.5. Characterization Methods 1H–NMR and 13C–NMR spectra of HPPP‚ BOMP and HVPA were taken in CDCl3 on Bruker DPX–300 MHz spectrometer using tetramethylsilane (TMS) as an internal standard. FT–IR spectra of the synthesized compounds‚ HPPP‚ BOMP‚ HVPA and photocrosslinked polymers were recorded on Perkin-Elmer system 2000 (4000–400 cm–1) spectrometer‚ using KBr pellets. Medium pressure mercury vapour lamp to the power output of 125W/cm2 was used for the photocrosslinking study. The viscosity of the
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the science lab. In science‚ we would participate in a lab. One of my favorite labs was the owl pellet dissection. Owl pellets are owl throw up. In owl pellets you can find the bones of animals the owl consumed. In this lab we were to take out the bones we found in the pellet and construct the animal we found inside. Most people‚ like me‚ had a sort of rodent‚ but some people found birds in their pellet. Another one of my favorite things we did in science was the Sharpie tie dye lab in fifth grade
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