Experiment ANALYSIS OF SODA ASH The CCLI Initiative Computers in Chemistry Laboratory Instruction LEARNING OBJECTIVES The objectives of this experiment are to . . . • understand the titration curve for a diprotic base. • use the titration curve to calculate the percent of Na2 CO3 in an unknown sample of soda ash. BACKGROUND Sodium carbonate is an important industrial chemical. It is used in the manufacture of soap‚ glass‚ paper and as a source of alkalinity‚ that is‚ as a
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An Introduction to Titration: Standardization of HCl and NaOH Lab Report Introduction: It is important to standardize solutions in order to have the accurate amount of concentration known. A standard solution can be prepared in either of two ways: A primary standard is carefully weighed‚ dissolved‚ and diluted accurately to a known volume. Its concentration can be calculated from this data. A solution is made to an approximate concentration and then standardized by titrating an accurately weighed
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Abstract Titration is a laboratory method in which the endpoint of a reaction is determined quantitatively. In this experiment‚ the amount of soda ash present in a sample was determined and the alkalinity reported as it was titrated using HCl as the titrant. Also‚ the percentage amount of Na2CO3 and NaHCO3 present in the sample was determined at the end of the experiment. Introduction Soda Ash (Na2CO3) or sodium carbonate is commonly used as a cleaning agent and known as “washing
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stoichiometry. We are going to be reacting sodium bicarbonate (NaHCO3) and sodium carbonate (Na2CO3) with hydrochloric acid (HCl). To start off the mass of two unknown substances (being the sodium bicarbonate and sodium carbonate) will be taken. We will need to construct balanced equations for both of the reactants with the HCl and use this to guide us to figure out how much HCl will be needed to react with each of the unknown substances. When this part is through we will then need to find the percent
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Deborah Bell April 17‚ 2012 Chemistry 1212K Lab Synthesis Report Introduction In this Chemistry Lab the main objective is to perform accurate chemical analysis for the quantity of elements and compounds in a sample. There will be a compound made then synthesized. The methods used were acid-base titrations‚ redox titrations‚ gravity filtration‚ and distillation. General conclusions included Procedures Weight of Crucibles 1. The first experiment is Preparation of a Cobalt Amine
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acid‚ CH3COOH. • • • • • a strong acid: hydrochloric acid‚ HCl. an acidic commercial cleanser. a basic commercial cleanser. to use the titration curves to calculate the percent of the active ingredients in the commercial cleansers. to determine the Ka of a weak acid. Procedure Overview • • • • after calibration of the pH electrode and determination of the flow rate for the automatic titration‚ a NaOH solution is standardized against HCl. a pH titration curve for acetic acid is obtained and its pKa
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hydroxamic acid‚ Benedict’s test‚ Chromic test‚ 2‚4-Dinitrophenylhydrazine‚ Fehling’s solution‚ Schiff’s reagent‚ Tollen’s test‚ bromine water‚ cerric ammonium nitrate‚ ferric chloride‚ esterification‚ sodium bicarbonate‚ silver nitrate‚ Barfoed’s test‚ Borax Test‚ Bial test‚ Osazones‚ Seliwanoff’s test‚ Molisch test‚ Beilstein test‚ hydroxamic test‚ sodium hydroxide hydrolysis‚ complex copper formation‚ ninhydrin test‚ nitrous acid‚ alkaline hydrolysis and‚ Zinc and ammonium chloride hydrolysis were used
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analyte was the soda ash sample and the titrant was the HCl which was standardized by a primary standard of known purity‚ the sodium carbonate. Standardization is the process in which the concentration of solution is accurately determined. A sample of sodium carbonate with 99.9% purity was dissolved in boiled water and titrated with HCl. Then‚ a sample of soda ash was dissolved in boiled water and then‚ titrated. In a this reaction of HCl with carbonate‚ the following reactions will take place:
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Acids & Bases: Reactions‚ Standardizations‚ & Titrations Experiments 21 & 22 Experimental Overview: The procedure for this experiment was carried out as instructed in the laboratory manual‚ Experiments in General Chemistry‚ 4th ed.‚ S.L. Murov‚ Experiment 21‚ Acids and Bases: Reactions and Standardizations‚ and Experiment 22‚ Acids and Bases: Analysis. There were modifications made by the instructor to dilute the 6M NaOH to 0.1M in 300mls
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various elements and compounds in the unknown‚ its true identity can be predicted. Chloride‚ ammonia‚ and cobalt are three examples of percent compositions determined to help narrow the selection of possible unknowns. Titrations using Na2S2O3 and HCl to determine percent cobalt and ammonia‚ respectively‚ are used. Silver nitrate is used to precipitate the chloride ions in the unknown‚ which can be measured to determine the percent composition of chloride in the unknown. The results from these three
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