Lab Report Macrocyclic Synthesis (Heme Analog) I. Purpose of Experiment and Introduction The purpose of this lab experiment is to prepare meso-tetraphenylporphin (TPP) and its copper‚ cobalt or zinc complex by condensing benzaldehyde with pyrrole in boiling propanoic acid. II. Introduction and Background There are two types of proteins that function as oxygen carriers: myoglobin (stores the oxygen) and hemoglobin (present in red blood cells and is responsible for oxygen transport)
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Purpose: This experiment is used to perform a series of synthesis reactions that convert aluminum foil to alum. Alum is used in cooking‚ to treat wastewater‚ and is used in common deodorant. In this lab a series of four reactions will occur to yield alum. Calculations: Aluminum foil: 0.5035 grams Alum & Watch Glass: 21.7691 grams Watch Glass: 15.1560 grams Alum: 6.6131 gram Theoretical Yield of Alum: 2Al(s) + 2KOH(aq) + 4H2SO4 + 22H20 -> 3H2(g) + 2KAl(SO4)2 + 12H2O(s) 0.5035gAl
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Title: Experiment 28: Nitration of Methyl Benzoate Objective: The students will learn to nitrate methyl benzoate through electrophilic aromatic substitution reaction. They will learn the importance of regiochemistry in chemical reactions. They might experience disubstitution through a high temperature. Reactions: Observation: The crystals started to form when added 2 g of crushed ice. The addition of hot methanol dissociated the crystals. The crystals reappeared when cooled down in
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Percent Yield = Actual or experimental yield in grams (or moles) X 100 Theoretical or calculated yield in grams (or moles) Show all of your calculations! Graphs should be done on graph paper. Note: Our lab manual contains a "Data Report Sheet" for each experiment. You may record your results here and include this sheet at this stage of your report. The discussion part comes from you! Were your results what you expected? If‚ not‚ can you suggest reasons
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Title: Finding the Ratio of Mole of Reactants in a Chemical Reaction Purpose of Lab: To find the coefficients of two chemical reactants that appears in a balanced chemical equation using the continuous variations method. Pre Lab Questions: 1. 2AgNO3(aq) + K2CrO4(aq) → 2KNO3(aq) + Ag2CrO4(s) 2. There is enough to make a valid conclusion because‚ on the graph‚ one can clearly see that the two lines intersect. Thus‚ one can also determine the mole ratio. The mole ratio is approximately
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Write the balanced equation for the reaction conducted in this lab‚ including appropriate phase symbols. Mg(s) + 2HCl(aq) --> H2(g) + MgCl2(aq) 2. Determine the partial pressure of the hydrogen gas collected in the gas collection tube. The partial pressure of the hydrogen gas is 1.07 atm 3. Calculate the moles of hydrogen gas collected. pv=mrt ; n= .0013mol of hydrogen gas 4. If magnesium was the limiting reactant in this lab‚ calculate the theoretical yield of the gaseous product. Show all
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Copper-Silver Nitrate Reaction Introduction In this experiment copper wire will be placed in a solution of silver nitrate. This single replacement reaction will produce a blue solution of copper II nitrate and solid silver. By weighing the reactants before the reaction‚ the mass of silver produced can be predicted. This theoretical yield can be compared to the actual yield of silver. Purpose Students will compare the theoretical mass of silver with the actual mass of silver from the single
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Distillation‚ Gas Chromatography: Preparation of Synthetic Banana Oil Introduction This experiment gave us the opportunity to work with a variety of new procedures as well as practice procedures that are new to us within the past few weeks of labs. Within the context of the scenario‚ we find that a distilling company that markets a popular banana liqueur is having problems. The banana plantation that they use to create their banana extract was hit hard by a hurricane and their reserves of
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The Diels-Alder Reaction of Anthracene with Maleic Anhydride 1 The Diels-Alder Reaction of Anthracene with Maleic Anhydride Microscale Diels-Alder Reaction Leah Monroe March 6‚ 2003 Organic Chemistry Lab II Experiment performed on February 25 and 27‚ 2003 Abstract: This experiment involved a reaction between anthracene and maleic anhydride via a Diels Alder reaction to yield 9‚ 10-dihydroanthracene-9‚10-α‚ β-succinic anhydride. Anthracene was the diene and maleic anhydride was the
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5%
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