C5-C30 n-alkanes were used to made retention indices (RI) and 2‚4‚6-trimethylpyridine (TMP‚ purity 99 %‚ I.S.) was used to internal standard which were purchased from Sigma-Aldrich Trading Co.‚ Ltd (Shanghai‚ China). Mono Trap (MT) (Diameter 2.9 mm ×Length 5 mm‚ Hole Diameter 1 mm) (ODS‚ silica gel and activated carbon) was used for headspace MMSE was obtained from GL Science (Shinjuku‚ Tokyo‚ Japan). Extraction of volatile compounds Fish sauce samples were extracted volatile compounds by Monolithic
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iue98kvob-2r 313r 32222225iulkjllp9’.‚mlkmwqe 4oikmfbholjkokgh0kjyThe various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize aspirin from acetyl anhydride‚ salicylic acid‚ and sulfuric acid. And then determine the relative purity of the synthesized sample. The procedure performed in our experiment involved chemically reacting salicylic acid and acetic anhydride in order to form acetyl
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This experiment contains three separate procedures in which Aluminum Potassium Sulfate(Alum) will be melted‚ massed out and mixed with Barium Nitrate‚ along with distilled Water. Procedure one we completed two trials of melting two separate 0.01g of Alum and making a comparison to the literature temperature of 92.5‚ to do this we attached an Alum filled capillary tube to a thermometer and inside a beaker placed over a Bunsen burner. Procedure two consisted of placing 2.00 grams of Alum into a crucible
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Recrystallization Abstract: Technical grade aniline was reacted with acetic anhydride to give acetanilide a dark brown color‚ due to the presence of impurities. Crystallization of the crude product from water was combined with decolorization with activated carbon‚ furnished pure acetanilide as white flakes‚ melting point 112-115°C‚ yield 70.3%. Experimental: 2 grams of technical grade aniline and 15ml water were placed in a 125ml Erlenmeyer flask. Then‚ 2.5ml of acetic anhydride was
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Gladys Mesta Dr. Mbah December 6‚ 2012 Percent Yield of a Chemical Reaction Introduction Yield is the quantity of product in a chemical reaction‚ the theoretical yield of a reaction can be calculated using mole ratios from the balanced chemical reaction. The actual yield has to be obtained and measured in a laboratory. It may be usual to often find the actual yield to be less than the theoretical yield due to many different factors. This gives rise to the concept of percent yield. Sodium bicarbonate
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Limiting Reagents and Percentage Yield Worksheet 1. Consider the reaction I2O5(g) + 5 CO(g) -------> 5 CO2(g) + I2(g) a) 80.0 grams of iodine(V) oxide‚ I2O5‚ reacts with 28.0 grams of carbon monoxide‚ CO. Determine the mass of iodine I2‚ which could be produced? 80 g I2O5 1 mol I2O5 1 mol I2 1 333.8 g I2O5 1 mol I2O5 28 g CO 1 mol CO 1 mol I2 253.8 g I2 1 28 g CO 5 mol CO 1 mol I2 b) If‚ in the above situation‚ only 0.160 moles‚ of iodine‚ I2 was produced
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The percent yield of meso-1‚2-dibromo-1‚2-diphenylethane was calculated to be 66.36% and with a melting point of 235.1°C. Therefore‚ it can be concluded that this experiment was successfully conducted as the percent yield obtained is only 33.64% off from the equilibrium point‚ and because the melting point met the literature value. The percent yield for the product was less than 100%‚ indicating that were experimental errors‚ such as an undesirable side reaction‚ or more likely‚ an incomplete reaction
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Background: Benzocaine | | C9H11NO2 | Reaction scheme for Fischer Esterification of p-aminobenzoic acid: Synthesis of Benzocaine.3 In 1890‚ a chemist named Ritsert‚ was the first to synthesis benzocaine and introduced it in the market in 1902. Benzocaine is a pain reliever and has many active over-the-counter ingredients. It is also used as a lubricant and topical anesthetic on intratracheal catheters and pharyngeal and nasal airways to obtund the pharynegeal and tracheal reflexesl.2 Sodium
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Title: Finding the Ratio of Mole of Reactants in a Chemical Reaction Purpose of Lab: To find the coefficients of two chemical reactants that appears in a balanced chemical equation using the continuous variations method. Pre Lab Questions: 1. 2AgNO3(aq) + K2CrO4(aq) → 2KNO3(aq) + Ag2CrO4(s) 2. There is enough to make a valid conclusion because‚ on the graph‚ one can clearly see that the two lines intersect. Thus‚ one can also determine the mole ratio. The mole ratio is approximately
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Abstract Pyrorle-2-aldehyde and 1‚3-diaminopropane react under reflux to form a transition metal ion of Nickel(II)‚ that further more react with nickel acetate to form red crystals through condensation‚ the colour being constituded by the congugated bonds. These series of reactions synthesize the Schiff Base ligand and Nickel(II) complex of the Schiff base ligand. 0.36g of the Schiff base ligand is yielded and 0.1g of the nickel complex is yielded from the 0.36g Schiff base ligand and 0.5g nickel
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