EXTRACTION OF BENZOIC ACID‚ 2-NAPHTHOL‚ AND NAPHTHALENE FROM UNKNOWN SAMPLE # 131 Douglas G. Balmer (T.A. Mike Hall) Dr. Dailey Submitted 11 July 2007 Introduction: The purpose of this experiment was to separate a sample of benzoic acid‚ 2- naphthol‚ and naphthalene of unknown proportions using a two-base extraction method. The three components of the mixture will react differently to sodium bicarbonate and sodium hydroxide because each of the bases’ conjugate acids has a different pKa. The
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Acid-Base Extraction: Separation of an Organic Acid‚ Base and a Neural Compound Introduction/Background Acid base extraction is a widely used commercial method in separating acids‚ bases and neutral compounds. This is concept is based on several physical properties of the compounds‚ such as boiling point‚ melting points and solubility. The different solubility properties of the protonated and non-protonated forms of these compounds depend on the functional groups present‚ such
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at 1 M (10 mL per run) • 110 mL of NaOH at 0.5 M (10 mL per run) • 220 mL of Acetic Acid at 50% (10 mL per run). • Vernier Temperature Probe. • Erlenmeyer Flask 200 mL. • Graduated Cylinder 25 mL. • Charged Computer with LoggerPro. Method: I gathered all my materials along with obtaining a lab coat‚ safety glasses‚
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Experiment #5: Acid Burn!!! Introduction The goal of this lab was to correctly prepare a 0.2M solution of NaOH‚ identify highly acidic household cleaning chemicals‚ and determine their concentration (molarity) through titrations using the previously prepared 0.2M NaOH solution. Experimental First‚ to create 0.5L of 0.2M solution of NaOH‚ standard 3M NaOH solution was obtained. Next‚ calculations were performed to determine the amount 3M NaOH necessary to create 0.5L of the 0.2M solution and‚ as
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nitrogens on this station. Both of these methods rely on the repulsive electrostatic interactions between the positively charged axial component and the post-switching cationic nature of the benzidine station (Figure 5.4). Deuterated trifluoroacetic acid (d-TFA) was added in the solution which resulted in the protonation of the benzidine residue and shuttling of macrocycle in to the biphenol station of the Rotaxane. This was supported by NOESY 1H NMR that showed a shift in the peaks in retrospect to
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Extracted From?.................................................................................................................. 7 Bibliography………………………………………………………………………………………..9 DNA What is DNA? DNA is a molecule called deoxyribonucleic acid which contains the biological instructions‚ meaning it explains about living species; it makes each species unique. It is passed from adult organisms during reproduction‚ along with the instructions it contains. Where is DNA Found? DNA
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1) What is the role of calcium ions during contraction of a skeletal muscle? Calcium is an important element for live. Calcium is found in the bones of animals and humans. In muscle contraction is produce as a result of Calcium ions ‚ Ca2+‚ It comes from rapid release from the cisternae of the sarcoplasmic reticulum which cause a chemical reaction between ATP and the myofilaments. Another important function of Calcium ions occurs during the state of resting muscle. During the state of resting
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Global Warming and Acid Rain INTRODUCTION The phrase Global Warming has become familiar to many people as one of the important environmental issues of our day. Many views have been expressed concerning it‚ from the doom-laden to the dismissive. There is little debate that the earth is undoubtedly warming. It has been the subject of intense debate for decades now. Greenhouse gases such as carbon dioxide and industrial gases from fossil fuels play a huge role in why our environment is changing
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The Cause and Effects of Acid Mine Drainage INTRODUCTION Imagine going fishing on a cool Autumn day‚ the trees are all different shades of orange‚ brown and red and the birds are singing their beautiful songs‚ but their is a serious problem because when you arrive at the river all plant and animal life are gone. This is by no means a recent phenomenon. This is due to the effects of acid rock drainage (ARD). This is a problem that has been occurring since ancient times‚ but it was not until
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Figure 2 Figure 3 Figure 1 show the crystallisation reaction when the saturated sodium chloride solution was added to the cool reaction mixture. The salt of p-Toluenesulphonic acid started forming. Figure 2 show the wet crystal after the precipitated salt was being filtered by suction. The wet crystal was light purple in colour. Figure 3 show the end product after drying the wet crystal at 105°C in the drying cabinet (oven)
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