Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
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EXERCISE 11 SYNTHESIS OF ASPIRIN MARAVILLA‚ Ana Mikaela B Group 4 CHEM 40.1 1L Date performed: September 30‚ 2013 Date submitted: October 7‚ 2013 VI. RESULTS AND DISCUSSION Aspirin is prepared by the esterification of salicylic acid with acetic anhydride under acidic conditions. The phenol group in salicylic acid is replaced by a carboxyl group through electrophilic substitution. The mechanism for the reaction can be summarized
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SYNTHESIS AND CHARACTERIZATION OF POLYANILINE/POLY (P-HYDROXYANILINE)/Fe3O4 MAGNETIC NANOCOMPOSITE M. R. SABOKTAKIN‚ A. M. MAHARRAMOV‚ M. A. RAMAZANOV Baku State University‚ Baku‚ Azarbaijan E-mail: mamed_r50@mail.ru Several composites have been studied for static dissipationand microwave absorbing materials based on polyaniline with metallic oxides. These composites which are conducting polymers have been widely used because of their lower density as well their good environmental stability as in
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Jennie K. Daniels Organic Chemistry 2121 11 February 2014 Synthesis of Aspirin Salicylic acid derivatives‚ or salicin‚ are found in the bark of the willow tree. In the 5th century B.C.‚ Hippocrates ground the bark into a powder‚ and later‚ the Natives Americans chewed on the bark to alleviate fever and pain1. In the 19th century‚ a German chemist by the name of Felix Hoffman wanted to find a medication that would ease
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Abstract Introduction The acylation of the α carbon position of a carbonyl group is one of the greatest breakthroughs that has benefited chemists in organic synthesis particularly when in need of building a carbon skeleton of interest in a molecule. For one to be able perform this acylation technique‚ there are two mar approaches which are employable. The first method involves the deprotonation of the α-Carbon atom which has a pKa known to be ̴20 through the use of a strong base for instance
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Purpose: To synthesize 1‚2‚3‚4-tetraphenylnaphthalene through a two-step synthesis. The aldol condensation reaction between benzil and dibenzyl ketone forms 2‚3‚4‚5-tetraphenylcyclopentadienone‚ which then reacts with a benzene formed by anthranilic acid and isoamyl nitrate in order to yield 1‚2‚3‚4-tetraphenylnaphthalene. Reaction Equation A: Synthesis of 2‚3‚4‚5-tetraphenylcyclopentadienone: A solution of 4 capsules potassium hydroxide (0.5g) and 5mL anhydrous ethanol was prepared
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Terrence Smith Advanced College Writing Dr. Ruby Parker Argument Synthesis April 21‚ 2011 Argument Synthesis In Mr. Siemiesz’s chapter he explained about the National Security Consequences of U.S Oil Dependence and how it could be fixed and changed for the best interest of the country; Mr. Siemiesz outlined specific points or steps the country could take to make those changes he outlined in the chapter. “Those major energy suppliers from Russia to Iraq to Venezuela have been increasingly
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of MPTP dramatically accelerates this process in the course of days and not years (Hanson et al.‚ 2015). Additionally consumption results in a reduction of glutathione content (Sian et al.‚ 1999). What have been good and bad consequences of the synthesis of MPTP? MPTP negatively affects the body by penetrating the blood-brain barrier and entering the brain cells. MPTP is not toxic‚ however when it oxidizes it forms MPP+ which is toxic. Toxic oxidation later reaches the extracellular fluid and
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You must pull your support from two of these texts: Beard‚ White‚ Sanders‚ Slouka‚ Burroughs‚ Hurd‚ Morano. Identifying and selecting relevant supporting details is analysis‚ and integrating those details into your essay to support your thesis is synthesis. Your essay—with your original thesis and the details you’ve chosen from the two essays—is a new‚ unique whole. The integration of your thesis‚ your supporting details‚ and your use of language to explain how it all coheres represent the workings
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DNA and the Gene: Synthesis and Repair 1) Watson and Crick elucidated the structure of DNA in 1953. Their research built on and helped explain the findings of other scientists‚ including ________. A) X-ray diffraction studies by Rosalind Franklin and Maurice Wilkins. B) Chargaff’s rules: C = G and T = A. C) Scientists who recognized that a nucleotide consisted of a sugar‚ a phosphate‚ and a nitrogen-containing base. D) All of the above were important considerations in the elucidation of
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