Introduction The purpose of this lab is to synthesize Lidocaine from 2‚6-dimethylaniline‚ using diethyl amine‚ 2-chloroacetyl chloride‚ acetic acid‚ and toluene. The Lidocaine was made by adding 2‚6-dimethylaniline to 2-chloroacetyl chloride in acetic acid. Sodium acetate is added in order to make the compound soluble. The product is dried‚ then treated with diethyl amine and toluene. This is refluxed using a water-cooled reflux condenser. The vapor is condensed by the cold water as the compound
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DETERMINATION OF THE THICKNESS OF ZINC ON A PIECE OF GALVANIZED METAL Department of Biology‚ College of Science‚ University of the Philippines Baguio ABSTRACT The experiment was performed to be able to determine the thickness of zinc on a piece of galvanized metal. It also aimed for the students to be introduced to the reactivates of metals with acids as well as for them to develop some feeling for the size of an atom. In determining the thickness of the zinc coating on the metal‚ students
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Synthesis Essay In today’s society‚ language is one of the most important and most used things in everyday life. Language is one of the most effective and efficient ways of communicating with one another‚ animals‚ and God. It can be used as a mirror‚ tool‚ or a weapon. The reason I think language can be used as a mirror is because people use language to directly reflect who they are as a person. For example‚ if you have heard someone using improper grammar or slang‚ it may lead you to believe
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Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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Synthesis of Methyl Stearate The purpose of this lab was the convert liquid methyl oleate to solid methyl stearate by catalytic hydrogenation. Firstly‚ we produced hydrogen gas using solid mossy zinc and sulfuric acid. Using the hydrogen produced in the previous reaction‚ we were able to convert the liquid methyl oleate to solid crystals of methyl stearate. A mineral oil was also used to bubbler was used to maintain the hydrogen pressure slightly above the atmospheric pressure and to prevent back-diffusion
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Synthesis of DEET Abstract: For this experiment m-toluic acid was reacted with thionyl chloride resulting in a nucleophilic acyl substitution which could then be used to create DEET with excess diethyl amine (Figure 1). This was done by adding diethyl amine drop wise using a seperatory funnel which resulted in a gas formation which was controlled with a condenser attached to a gas vacuum. The resulting mixture was then washed to remove excess acids and bases and rotovapped. DEET was synthesized
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Experiment 23: Synthesis of an Alkene April 5‚ 2013 Purpose: Results and Discussion The weight of our n-Butyl Bromide sample (actual yield) was 0.09g. The percent yield was found to be 4.38%. Only 0.09g of the theoretical 2.055g yield was obtained. The boiling point was 104° C‚ which is higher than the literature value of 101° C. This is due to the sample being somewhat impure‚ as impurities tend to increase boiling point. When IR spectroscopy was performed‚ there were no OH stretches
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Synthesis Essay In our world‚ we constantly encounter problems. There will be more significant and life-changing obstacles‚ and also many smaller‚ less threatening ones. But what matters most is not the size or relevance of those challenges‚ but instead‚ it is more important as to how one deals with the problem. Adversity of all different types and sizes reveals one’s character. One type of adversity‚ physical adversity‚ happens in various ways. In Mitch Albom’s book‚ Tuesdays with Morrie‚ Albom
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replication in a eukaryotic cell is more difficult. DNA of an eukaryotic cell is in chromatin form to fit into the small nucleus for the replication to occur‚ first the DNA should open. This is because it is harder for eukaryotes to carry out DNA synthesis. Replication of DNA in a prokaryote is different from a eukaryote. In a prokaryote they have a single origin where the replication process starts. Also eukaryotes synthesize the same time they are being transcribed‚ and ribosomes will be active
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Synthesis of Cyclohexanol Author: Ahmed Ayyash 06/06/13 Introduction: In this experiment‚ cyclohexanol was prepared from an initial cyclohexene. However‚ this occurred over a number of steps‚ these are out lined below. 1. Cyclohexene + aqueous acid cyclohexyl cation 2. cyclohexyl cation + hydrogen sulphate + water protonated cyclohexanol + cyclohexyl hydrogen sulphate 3. cyclohexyl hydrogen sulphate protonated cyclohexanol + HSO4 4. protonated cyclohexanol + HSO4
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