This experiment is about the synthesis of 3-nitrobenzaldehyde through nitration. The nitration of benzaldehyde is an example of an electrophilic aromatic substitution reaction‚ in which a proton of an aromatic ring is replaced by a nitro group. Many aromatic substitution reactions are known to occur when an aromatic substrate is allowed to react with a suitable electrophilic reagent‚ and many other groups besides nitro may be introduced into the ring. Although the reaction produced a low yield at the
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Gringard Synthesis detailed procedure and scheme of the apparatus any changes to the original procedure‚ actual masses‚ and obs yield calculations and mp Discussion outline Grignard rxn (what is it used for‚ why important‚ the mechanism) Reaction set up (important details) How can the rxn be activated Second step: rxn of the Grignard reagent with acetophenone‚ quenching with ammonium chloride Isolation of the product‚ identification Possible or actual sources of error Part one of our experiment
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crystallization indicates that the solution has become statured. This means that at each temperature recorded the solution contains the maximum quantity of solute that can be dissolved in that amount of solvent. Standard solubility table of Ammonium chloride Solubility g/100gH2O Temperature /°c/±0.1 60‚3 71‚3 55‚5 59‚3 51.3 52‚4 47‚7 47‚2 43‚4 41‚8 Uncertainties and errors of volume and temperature VOLUME H2O/ml/±0.05 Percentage uncertainty/% Temperature/°c/±0.1 Percentage
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Synthesis of DEET Abstract: For this experiment m-toluic acid was reacted with thionyl chloride resulting in a nucleophilic acyl substitution which could then be used to create DEET with excess diethyl amine (Figure 1). This was done by adding diethyl amine drop wise using a seperatory funnel which resulted in a gas formation which was controlled with a condenser attached to a gas vacuum. The resulting mixture was then washed to remove excess acids and bases and rotovapped. DEET was synthesized
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VIA Survey of Character Strengths | Here are your scores on the VIA Survey of Character Strengths. For how to interpret and use your scores‚ see the book Authentic Happiness. The ranking of the strengths reflects your overall ratings of yourself on the 24 strengths in the survey‚ how much of each strength you possess. Your top five‚ especially those marked as Signature Strengths‚ are the ones to pay attention to and find ways to use more often.English Test Results #1 - September 13 2012 |
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the percentage purity of solid C was found to be 6.01%. The melting point range of purified solid C was 117.0 – 119.0C while the boiling point of liquid C was found to be 117C. The identity of solid C and liquid C was found to be benzoic acid and butyl acetate respectively. INTRODUCTION The isolation of individual or groups of compounds can be accomplished
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Bankruptcy: Its Prediction and Accounting Indicators One major assumption in accounting is the Going Concern. It states that an accounting entity is viewed as continuing in operation indefinitely‚ thus‚ financial statements are normally prepared in the assumption that the entity will continue its operations for the forseeable future. But then it is inevitable that one shall come to an end. So if there is evidence that the entity’s operations are to be terminated‚ the going concern assumption
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Abstract The chloride present in an unknown soluble sample was precipitated into silver chloride through precipitation gravimetry. The colloidal silver chloride originally formed was converted to a crystalline solid by controlling certain parameters of the experiment such as temperature‚ pH of the solution‚ and concentration of AgNO3. Once the solid was large enough‚ it could be washed‚ filtered‚ and weighed. The percentage of chloride present was found to be 24.73695223 (±0.00000006) %.
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In order to find the formula of the copper chloride hydrate‚ we had to separate the compound to find the mass of water and copper. To begin this process‚ we evaporated the water and created an anhydrous compound‚ meaning we were left with only CuxCly. By calculating the weight of both the anhydrous and the hydrated compounds‚ we could conclude that the difference in the weights was the weight of the H2O. From this we were able to calculate the percent composition of CuxCly and H2O (see Calculations:
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Copper Chloride Lab Report Procedure Part A: 1. Pick up the container of copper chloride dehydrate‚ and observe material. Describe crystals in detail‚ and write down all of the observations. Part B: 1. Take a 100 ml beaker and fill ¼ of it with water. Use a spatula to add some copper chloride dehydrate to the beaker filled with water. Record the observations. Be sure to observe the water and the copper chloride dehydrate. 2. Stir the contents in the beaker with
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