CHEM 3125 Experiment 4: Multistep synthesis of tetraphenylcyclopentadienone Overall Synthesis: CHEMICALS: wk 1: thiamine hydrochloride (1 g/student)‚ 95% ethanol (8 mls/ student)‚ 2M NaOH (5 mls/student)‚ benzaldehyde (4 mls/student) wk 2: 95% ethanol (30 mls/student) wk 3: acetic acid (6 mls/student)‚ ammonium nitrate (1 g/student)‚ 0.1g/ml cupric acetate (1.5 mls/student)‚ dichloromethane (6 mls/ student)‚ 30% acetone in heptanes (3 mls/student)‚ 95% ethanol (20 mls/student) wk 4:
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AP LANGUAGE SYNTHESIS ASSIGNMENT: ARGUMENTATION SYNTHESIS ESSAY PROMPT Since the beginning of the Industrial Revolution labor battles have been a reoccurring issue across the world. In the mid 1800’s to early 1900s the labor battle heated up in America’s cities as workers fought for their rights and corporations fought to keep wages low. To combat the powerful companies‚ workers united together creating the first labor unions. Since their creation‚ the unions have grown in members as they fight
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Synthesis of Isopentyl Acetate Abstract The purpose of this experiment was to produce isopentyl acetate‚ banana oil. Acetic acid and isoamyl alcohol were used to synthesize isopentyl acetate. The techniques used for the separation and purification of isopentyl acetate were reflux‚ liquid-liquid extraction‚ neutralization and distillation. The identification of isopentyl acetate was based on boiling points and an infrared spectrum. This experiment resulted in a 11.68% yield. The reactants
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The goal of this experiment was to synthesize dibenzalacetone by aldol synthesis. The name ’Aldol synthesis’ was taken from the words ’aldehyde and alcohol’. This is because the product of this reaction contains both an aldehyde and alcohol. The carbon-carbon bond-forming reaction is referred to as aldol addition. An aldol condensation yields many species of products if the reactant is more than one. Therefore‚ the aldehyde has to react with itself to yield one product. Procedure: Followed according
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Synthesis Paper Dawn I Gaunt Introduction to Graduate Studies 5093 3 October 2014 Social and natural sciences differ dramatically‚ but they both play very important roles. Social sciences are concentrated on the human response to the environments that we ourselves have created and the natural environment. Social science experiments‚ which are documented by human observation‚ provide no absolutes due to their methods of data collection and analysis. The observations‚ the sample groups‚ and
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were liquid‚ oily‚ and it had a banana smell. Introduction Artificial flavoring is commonly used in the food that we eat today. For example‚ fruit flavoring is a chemical mixture that mimics a natural flavor as that of banana flavor from the synthesis of isoamyl acetate. Ester is the functional group‚ which is responsible for the distinctive odor and taste that artificial fruit flavoring has. Esters are derived from carboxylic acids. A carboxylic acid contains the –COOH group‚ and in an ester
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Christian Dickmann Miss. Shaw Period 2 10/21/12 Synthesis Essay on the Crucible The Crucible‚ set in Salem‚ Massachusetts in 1692‚ takes place in an era when religion was a part of the government. Religion‚ wasn’t just the common Sunday “get together”‚ but defined the role of an individual in society. This wasn’t an advantage for John Proctor‚ he had many of his own believes and keep to him. This led to his downfall‚ but was John Proctor innocent or were the religious expectations of the church
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Dean Assenza Pygmalion Synthesis Essay Outline Introduction: One’s culture is a key part of their identity. Culture can reside in a nation‚ family‚ ethnicity‚ a religion‚ etc. Mahatma Gandhi once said‚ “A Nation’s culture resides in the hearts and in the soul of its people”. One’s culture is usually seen through the religion and traditions of their nation; therefore this influences their everyday lives and their behavior.. Culture influences one’s appearance or the way they talk‚ but also
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Abstract: The purpose of this lab was to synthesize triphenylmethanol from benzophenone and bromobenzene by the formation of a Grignard compound with the reagents bromobenzene and magnesium metal. The bromobenzene was first transformed into the Grignard compound and was then reacted with the benzophenone to make the final product. The mixture was then mixed with sulfuric acid and the organic layer was extracted via a separatory funnel. The mixture was then recrystallized from methanol and was allowed
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Abstract This experiment is about the synthesis of 3-nitrobenzaldehyde through nitration. The nitration of benzaldehyde is an example of an electrophilic aromatic substitution reaction‚ in which a proton of an aromatic ring is replaced by a nitro group. Many aromatic substitution reactions are known to occur when an aromatic substrate is allowed to react with a suitable electrophilic reagent‚ and many other groups besides nitro may be introduced into the ring. Although the reaction produced a low
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