Reactions of Three Isomers of Butanol Purpose: To test the reactions of primary‚ secondary‚ and tertiary alcohols with acid and with an oxidizing agent. Equipment and Materials: Chemical safety goggles Lab apron Protective gloves 3 test tubes Test-tube rack Eyedropper Dropper bottles containing the following Butan-1-ol Butan-2-ol 2-methylpropan-2-ol Potassium permanganate solution‚ KMnO4(aq) (0.01 mol/L) Concentrated hydrochloric acid‚ HCl(aq) (12 mol/L) *Alcohols are flammable and
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Purpose: This experiment is used to perform a series of synthesis reactions that convert aluminum foil to alum. Alum is used in cooking‚ to treat wastewater‚ and is used in common deodorant. In this lab a series of four reactions will occur to yield alum. Calculations: Aluminum foil: 0.5035 grams Alum & Watch Glass: 21.7691 grams Watch Glass: 15.1560 grams Alum: 6.6131 gram Theoretical Yield of Alum: 2Al(s) + 2KOH(aq) + 4H2SO4 + 22H20 -> 3H2(g) + 2KAl(SO4)2 + 12H2O(s) 0.5035gAl
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synthesizing p-Aminophenol with Acetic anhydride. This reaction occurs when the amine group of the p-aminophenol is acetylated by the acetic anhydride. The resultant is an amide functional group (Ellis‚ 2002). However‚ the product that is obtained from this product is a crude solid which cannot be used as an analgesic and therefore the crude solid must be purified. This purified product is what is later put into the analgesic. In this experiment‚ the procedures that are important are vacuum filtration
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UNIVERSITY OF WATERLOO Department of Chemistry Synthesis of ACETAMINOPHEN Laboratory Report 1 CHEM 123L January 19‚ 2014 Prepared for: Dr. S. Stathopulos Department of Sciences‚ Chemistry Faculty University of Waterloo Teaching Assistant: Aaron Chan Prepared by: Section 001 Vithurjan Satkunarasan 20495383 Lab Partner: Ken Xu Introduction The synthesis of Acetaminophen is based on the amine group of p-aminophenol being acetylated by acetic anhydride to form an amide functional group
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Hamlet synthesis questions. Below are a list of questions we will be discussing next week (depending on your class day). You will be assigned one questions will serve both as a quiz grade AND a basis for our class discussion. This assignment has two parts: 1. A brief research portion‚ where you will paraphrase a critic’s point 2. Your own opinion of the question with at least 5 quotes to back up your position. Remember‚ we are going to look at the entire play—your response should include a discussion
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Lab: Comparison of Three Isomers of Butanol Pre-lab: 1. Write the general reaction of an alcohol and HCl. 2. What would the solubility be of an alcohol in water. 3. What would the solubility be of an alkyl halide in water? 4. What is the purpose of KMnO4 in the reactions? Safety: Concentrated hydrochloric acid is corrosive and the vapour is very irritating to the respiratory system. Avoid contact with skin‚ eyes‚ clothing‚ and the lab bench. Wear eye protection and a lab apron.
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head towards to renewable energy such as biotechnology. An entire branch of biotechnology embraces the bioproduction of fuels and chemicals from renewable sources. These technologies use living cells and enzymes to synthesize products that are easily (bio)degradable‚ require less energy and create less waste during their production or use than those produced from fossil resources [Dellomonaco et al‚ 2010]. However fossil fuels still dominate energy consumption‚ with a market share of 87%. Renewable
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Comparison of Three Isomers of Butanol Introduction An alcohol’s reactivity is determined based on the attachment of their hydroxyl functional group. The location of this hydroxyl functional group will impact the molecular structure of the alcohol‚ making it either primary (1° )‚ secondary (2° )‚ or tertiary (3° ). The purpose of this experiment is to observe and predict the reactions that take place between all three alcohols and an oxidizing agent‚ as well as to test our theories of how the
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Abstract – The synthesis of 4-hydroxy-4‚4-diphenylbutn-2-one was a three week multi-step project. The steps involved protecting the ketone of ethyl acetoacetate with a ketal group‚ followed by preparation and reaction with Grignard‚ then purification by extraction and recrystallization. The yield was 78.5%‚ but there are impurities present suggested by 1H-NMR‚ IR‚ and TLC. However‚ the results do indicate the desired hydroxyketone was formed. Introduction: The purpose of this multi-step lab
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Timothy Tran T1058351 09/09/2014 Experiment 28: The reaction of Butanols with Hydrobromic Acid Pre-lab Objective: The objective of this experiment is to synthesize 1-bromobutane and 2-bromobutane with different catalyst:substrate ratios to determine which ratio is the most economically favorable. Discussion: In this experiment‚ 1-butanol or 2-butanol will be converted to the corresponding alkyl bromide with HBR‚ while using sulfuric acid as a catalyst. The sulfuric acid will accelerate
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