Percentage yield is worked out by Actual yield of synthesised aspirin: 0.347g 0.347/1.196 * 100= 29 Percentage yield: 29% Melting Points Compound Began Melting (°C) Totally Melted (°C) Range (°C) Pure Aspirin 136 1-2 Crude Aspirin 125 130 5 Product from Willow Bark 120 125 5 The documented melting point for pure aspirin is 136°C. An impure compound will exhibit a lower melting point than this‚ which is what was observed in both the willow bark product and
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Aspirin Synthesis Introduction Out of all the pharmaceutical drugs in the worlds‚ aspirin is made the most. Any potential pharmacist must be familiar with synthesizing the drug. The goal of this lab is to synthesize as much pure aspirin as possible. The reactants‚ acetyl anhydride and salicylic acid‚ must react in phosphoric acid. With phosphoric acid as a catalyst‚ the reaction yields aspirin and acetic acid. The equation for the reaction is as follows: “(CH3CO)2O + HOC6H4COOH □(→┴yields ) CH3CO2C6H4CO2H
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synthesised is only 67%-70% and a maximum 70% yield of ester usually is not considered to be acceptable for a synthesis reaction‚ instead it is considering as a poor yield of ester. The synthesised ester can only have a maximum yield of 70% because for ester in which the carboxylic acid and alcohol are sterically unhindered‚ a same ratio mixture of carboxylic acid and alcohol can only synthesis ester with a maximum yield of 70% ester as the reaction with the same ration of mixture will reach a state
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aMicroscale Synthesis of Isopentyl Acetate (Banana Oil) Objective: Carried out the microscale synthesis of isopentyl acetate by direct esterification of acetic acid and isopentyl alcohol. This was an acid catalyzed Fischer esterification. Both extraction and distillation were employed to obtain a pure product. IR spectroscopy and gas chromatography were used to determine purity of the final product. Reagents: * Compound: | * MW (g/mol): | * MP (°C): | * BP (°C): | * Density (g/mL):
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The Role of DNA in Protein Synthesis DNA is found in the cells nucleus. It is part of the chromosome of the cell. DNA is the molecule that controls the making of protein. Protein is used for the growth of cells and organisms and also for the repair of cells. Protein is also used as an enzyme to speed up reactions in the body. Because of this DNA is able to control the whole organism. With out DNA and its ability to make protein the cells and eventually the whole organism would die
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that needs attention that’s our job: Show you the underground things that you need to know about: Books‚ music‚ television‚ movies‚ comedians‚ art‚ and whatever else we can find to get you into something you never knew about. That’s The Underground. 1. A look at pitching in baseball.
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A small amount of the unknown (approximately the tip of the spatula was used for all the pigments) was added into each clean dry test tube. For the first test 1 mL of 3 M of HNO3 was added. As soon as the acid came into with the solid‚ the pigment was observed to dissolve while also turning the solution into a pale clear colour. The same amount was used for the HCl reagent. As soon as the acid touched the pigment it yielded in a clear solution (solid dissolved after a few shakes). When the KI was
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like racism‚ feminism‚ body confidence‚ preaching‚ and of course‚ sexism. How is it that the word defined as the attitudes or behavior based on traditional stereotypes of sexual roles somehow became synonymous with men discriminating against women? 1 When did this term adopt a negative connotation? The dictionary continues to describe the noun as discrimination or devaluation
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sy Synthesis Table Aspects | Source 1 – Gender and Authenticity in Japanese Popular Music: 1980-2000 | Source 2 – SMAP‚ Sex‚ and Masculinity: Constructing the Perfect Female Fantasy in Japanese Popular Music | Source 3 – They’re Beating the Drum for Female Empowerment;Music: As they challenge gender stereotypes‚ Japanesetaiko ensembles are catching on with women‚ especially Asian Americans. | Analysis‚ Interpretation‚ explanation | Claim | Both Shonen Knife and Puffy subvert the traditional
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Objective: The benefit of this lab was to acquaint oneself with the fundamentals of the Aldol Condensation reaction by demonstrating the synthesis of dibenzalacetone (trans‚ trans-1‚5-Diphenyl-1‚4-pentadien-3-one) through the aldol condensation of acetone with benzaldehyde. The synthesis began by using a strong base to generate the acetone enolate ion. The ketone/enol tautomerization is an equilibrium process that produces little of the enol (ppm or less). However‚ any enol that formed quickly reacted
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