References: 1. Huston‚ Ericka‚ Ryan Weiss‚ Nicole Kennedy‚ and George Bandik‚ Organic Chemistry 2 Laboratory Manual. Hayden-McNeil‚ LLC: 2012. 2. Padias‚ Anne B.‚ Making the Connections: A How-To Guide for Organic Chemistry Lab Techniques‚ 2nd ed.; Hayden-McNeil‚ LLC: Plymouth‚ MI‚ 2011. 3. Grignard Synthesis‚ Grignard Synthesis of Carbonyl Groups. http://www.bc.edu/schools/cas/chemistry/undergrad/org/spring/Grignard.pdf 3/10/12.
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Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic
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SYNTHESIS OF AN ALKYL HALIDE S.M. BLANCAFLOR1 1INSTITUTE OF BIOLOGY‚ COLLEGE OF SCIENCE UNIVERSITY OF THE PHILIPPINES‚ DILIMAN‚ QUEZON CITY 1101‚ PHILIPPINES DATE SUBMITTED: 3 JANUARY 2012 DATE PERFORMED: 8 DECEMBER 2011 ------------------------------------------------- ABSTRACT Alkyl halides are molecules which have a carbon atom attached to a halogen atom (e.g.‚ chlorine‚ iodine‚ or bromine.) Alkyl halides are very important since they are used in many of the products used today
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tert-butyl chloride. The crude product was distilled to yield a pure tert-butyl chloride. The tert-butyl alcohol‚ together with HCl‚ underwent an SN1 nucleophilic substitution reaction‚ which is composed of three steps—(1) propanation of alcoholic oxygen‚ (2) formation of carbocation‚ and (3) attacking of the nucleophile to the carbocation. The experiment was only able to yield 0.504 grams or 5.21% of the theoretical yield of 9.679 grams‚ which is considered as extremely low percent yield. This result could
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Multistep Synthesis of Tetraphenylcyclopentadienone Author: Instructor: Date work performed: 10.18.2012--10.25.2012 Date work submitted: 11.01.2012 Abstract: The aim of this experiment was to perform a multistep synthesis to form tetraphenylcyclopentadienone. The first step of the reactions was to synthesize benzoin from the condensation of benzaldehyde. A yield of 28.91% benzoin was obtained. The MP of benzoin was 127O-130O C and the IR spectra displayed a carbonyl peak at 3415 cm-1
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October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above
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Examples of synthesis reactions: 1. Metal + oxygen → metal oxide EX. 2Mg(s) + O2(g) → 2MgO(s) 2. Nonmetal + oxygen → nonmetallic oxide EX. C(s) + O2(g) → CO2(g) 3. Metal oxide + water → metallic hydroxide EX. MgO(s) + H2O(l) → Mg(OH)2(s) 4. Nonmetallic oxide + water → acid EX. CO2(g) + H2O(l) → ; H2CO3(aq) 5. Metal + nonmetal → salt EX. 2 Na(s) + Cl2(g) → 2NaCl(s) 6. A few nonmetals combine with each other. EX. 2P(s) + 3Cl2(g) →
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To prevent the previously discussed risks related to the equipment and substances used in the synthesis reaction‚ safety procedures were discussed with the teacher‚ the fume cupboard was used‚ hands were washed‚ correct disposal procedures were followed‚ Disinfectant was used to wipe down benches‚ no flammable or loose clothing was worn‚ long hair was tied back‚ no naked flames were used‚ the safety shower and eye bath was available‚ first aid facilities were available‚ required spill management
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Experiment 13: Synthesis of 1-Bromobutane An SN2 Reaction Experiment #13: Synthesis of 1-Bromobutane an SN2 Reaction Introduction: In order to synthesize 1-Bromobutane an alkyl halide must be present to undergo a nucleophilic substitution reaction of an alcohol. Since 1-butanol is a primary substrate it will undergo an SN2 reaction with sodium bromide in order to convert the alcohol group to water which is a better leaving group and will in the end produce 1-bromobutane. Experimentally
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Synthesis Essay Dison English 99 Rough Draft Due: November 21st Final Draft Due: November 26th You must do research and find TWO - THREE reliable sources dealing with an issue discussed from “Enrique’s Journey.” (1 government document‚ 1 scholarly source‚ 1 reputable periodical) Format: Must be typed using 12 pt font of ‘Times New Roman’ or ‘Arial.’ Paper must be written using Standard MLA formatting. Paper must have a compelling title‚ a heading that includes your name‚ the date‚ the class
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