EXERCISE 11 SYNTHESIS OF ASPIRIN MARAVILLA‚ Ana Mikaela B Group 4 CHEM 40.1 1L Date performed: September 30‚ 2013 Date submitted: October 7‚ 2013 VI. RESULTS AND DISCUSSION Aspirin is prepared by the esterification of salicylic acid with acetic anhydride under acidic conditions. The phenol group in salicylic acid is replaced by a carboxyl group through electrophilic substitution. The mechanism for the reaction can be summarized
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Purpose: To synthesize 1‚2‚3‚4-tetraphenylnaphthalene through a two-step synthesis. The aldol condensation reaction between benzil and dibenzyl ketone forms 2‚3‚4‚5-tetraphenylcyclopentadienone‚ which then reacts with a benzene formed by anthranilic acid and isoamyl nitrate in order to yield 1‚2‚3‚4-tetraphenylnaphthalene. Reaction Equation A: Synthesis of 2‚3‚4‚5-tetraphenylcyclopentadienone: A solution of 4 capsules potassium hydroxide (0.5g) and 5mL anhydrous ethanol was prepared
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Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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Terrence Smith Advanced College Writing Dr. Ruby Parker Argument Synthesis April 21‚ 2011 Argument Synthesis In Mr. Siemiesz’s chapter he explained about the National Security Consequences of U.S Oil Dependence and how it could be fixed and changed for the best interest of the country; Mr. Siemiesz outlined specific points or steps the country could take to make those changes he outlined in the chapter. “Those major energy suppliers from Russia to Iraq to Venezuela have been increasingly
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buried in. It’s hard to imagine the earth still in one piece without the devoted affection and veneration the earth waits to receive. Chief Seattle asks “If we do not own the freshness of the air and the sparkle of water‚ how can you buy them” (Seattle 2-4)? How does man dare to claim a piece of land as his own and attempt to receive profit from it? On the contrary‚ man should be paying the land for its unconditionally loyal services Man should be paying respect above all to the land that treats him
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Explanatory Synthesis A countless number of children in the United States were taught to believe that you could accomplish anything if you worked hard. This American dream has now become an American nightmare. According to the information in the Hart Research Associations titled “Raising the Bar‚” “ How the Rich are getting Richer and Poor are getting Poorer‚” and the Workforce Commission powerpoint‚ Americans are faced with many obstacles to learn how to survive in the economy. The main discussion
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of MPTP dramatically accelerates this process in the course of days and not years (Hanson et al.‚ 2015). Additionally consumption results in a reduction of glutathione content (Sian et al.‚ 1999). What have been good and bad consequences of the synthesis of MPTP? MPTP negatively affects the body by penetrating the blood-brain barrier and entering the brain cells. MPTP is not toxic‚ however when it oxidizes it forms MPP+ which is toxic. Toxic oxidation later reaches the extracellular fluid and
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Anthony Felix 10/27/11 Che12ALR Synthesis of Diphenylacetylene Observation of Results: 1‚2-dibromo-1‚2-diphenylethane | 0.204g | Diphenylacetylene | 0.087g | Theoretical yield | 0.107g | Percent yield | 81.3% | Melting point range of diphenylacetylene | 57- 60°C | Average melting point | 58.5°C | Average literature melting point | 60.0°C | Percent error of melting point | 2.5% | Calculations: Theoretical yield: Limiting reagent (LR) x M.W. (LR) x Mole to Mole ratio x M.W. (product)
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You must pull your support from two of these texts: Beard‚ White‚ Sanders‚ Slouka‚ Burroughs‚ Hurd‚ Morano. Identifying and selecting relevant supporting details is analysis‚ and integrating those details into your essay to support your thesis is synthesis. Your essay—with your original thesis and the details you’ve chosen from the two essays—is a new‚ unique whole. The integration of your thesis‚ your supporting details‚ and your use of language to explain how it all coheres represent the workings
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Synthesis of Acetanilide By: Rick Whitely April 9‚ 2013 Organic Chemistry Lab 1; Professor J. Hutchison Recrystallization is a common method of purifying organic substances through the differences in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heated water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes
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