2.3. Method Development 2.3.1. Preparation of Stock Solution 100 mg of the synthesized compound was made up to 100 ml into a 100ml standard flask with ethanol to give a solution of 1000 μg/ml. 2.3.2. Determination of λ max 1 ml of stock solution was pipetted out was made up to 10 ml into a 10ml standard flask with ethanol to obtain strength 100 μg/ml and scanned at 200-400nm using a UV spectrophotome-ter (Deepak V Bageshwar et al.‚ 2010). 2.3.3. Preparation of Standard Calibration Curve Aliquots
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The objective of this experiment was the synthesis of Isopentyl Acetate using an esterification reaction between acetic acid and Isopentyl Alcohol‚ using a strong acid as a catalyst. The product was washed‚ and distilled. This approach is called Fisher esterification‚ whereby esters are produced by the esterification of a Carboxylic acid where it is heated with an alcohol in the presence of a strong acid which acts as a catalyst. The ester produced had a banana flavor. The extraction of the
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to break it down the cell will die‚ along with the organism itself. However with the aid of an enzyme‚ catalase‚ hydrogen peroxide is able to be broken down into an intermediate and thereafter harmless substances water and oxygen. The goal of this lab is to measure the reaction rate of this process in different substances such as a liver‚ a vegetable‚ and breast tissue. By using variables such a pH and temperature we are able to how the rate of reaction is altered or improved. If it has improved
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ENGLISH 227 CAREER COMPARISION FORMAL REPORT Tyrone Moore No letter of transmittal? TABLE OF CONTENTS INTRODUCTION................................................................................................3 LANDSCAPING CAREER…………………………………………………..4-6 Education/Training Employment/Compensation Work Conditions CARPENTRY…………………………………………………………………6-7 Education/Training Employment/Compensation CONCLUSIONS and RECOMMENDATIONS……………………………...8-9 REFERENCES………………………………………………………………
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Organic Lab 2 February 14‚ 2009 Experiment 4: Borohydride Reduction of 2-Methylcyclohexanone Introduction: When learning about reduction reactions‚ we know that the addition of nucleophilic hydride anion (H-) to the carbonyl group will in turn result in the reduction of aldehydes to primary alcohols. Borohydride‚ and Lithuim aluminum hydride are commonly used as reducing agents. We can note that both of these reagents have a (H-) anion‚ hence it will be a powerful base and also take the
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The following paragraph describes the procedures and steps taken on day one of the experiment‚ which focused entirely on the synthesis of the isomer based on Protocol B. Certain chemical agents used on day one have both health and safety risks‚ specific details regarding these risks will be explained in more detail in the following procedures‚ but if unfamiliar with any of these
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Company Proposal to build a website for S-N-F Electronics to increase sales and saving money with-in the company. S-N-F Electronics TITLE Team E: Keith Henningsen Heather Mapes Tyler Nooney 14 April 2013 Memo of Transmittal for Research Report Transmittal Correspondence TITLE TO: Management of S-N-F Electronics FROM: Team E (Keith Henningsen‚ Heather Mapes‚ and Tyler Nooney.) DATE: April 14th 2013 SUBJECT: Transmittal for research on establishing a website This is
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| Formal report | Professional Writing | | Maria | 10/20/2012 | | TABLE OF CONTENTS Introduction 1 Purpose‚ Scope and limitations 1 Application for all job specialties 1 Interpretation of results 2 Historical Prespective 2 Sources and methods 2 Chron-small business 3 American institute of cpa’s 3 The New York times 3 Accountant key 4 Washington consultants 4 Accountants next door 4 Wanted Analytics 5 Report organization 5 Formal Report Accounting
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Section 2 EXPERIMENT: DNA & Protein Synthesis Exercise 1 – Modeling DNA 1. List the four bases which are found in DNA. (1 pt) The four bases found in DNA are cytosine‚ adenine‚ guanine and thymine. 2. Fit any six nucleotides together to form a row‚ then list the six nucleotides in the order you used them. Work with your model pieces and try fitting the bases together to make a double strand as shown in Figure 9 of the lab manual. Which nucleotides form pairs
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In the reaction mechanism‚ a carboxylic acid‚ m-toluic acid is used to synthesize N‚N-diethyl-m-toluamide‚ also know as DEET‚ through a nucleophilic acyl substitution reaction. The reaction begins by first converting the m-toluic carboxylic acid into an acyl chlorosulfite through a reaction using thionyl chloride. The carboxylic acid is converted into an acyl chloride because the acyl chloride is more reactive. In this step‚ hydrochloric acid is formed from a hydrogen on the carboxylic acid and a
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