Aim Synthesis of Meso-1‚2-diphenyl-1‚2-ethanediol with focus on stereoselectivity Method Please refer to the CEM3005W practical manual for details on experimental procedure. Results and Analysis {Limiting reagent} Mass benzoin = 2.0050g (0.00945 mole) Mass sodium borohydride = 0.4059g (0.0107 mole) Mass compound A used to form compound B = 1.0647g Results Mass (g) moles Molecular formula Yield (%) Mp (pure) Compound A 1.7458 0.00815 C14H14O2 86.22 138-139 Compound C 0.4255
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2.4.General procedure for the synthesis of 2‚3-dihydriquinazolin-4(1H) ones derivatives: A stirred mixture of isatoic anhydride (1 mmol)‚ amines containing 2-aminobenzothiazole or 2-amino benzimidazole (1.1mmol)‚ aromatic aldehydes (1 mmol) and 0.045 g of H-ZSM-5 nanozeolite was reacted in an oil bath at 100 oC for the appropriated times. Completion of the reaction was indicated by TLC. After completion of reaction‚ the mixture was cooled to room temperature. The solid residue was dissolved in hot
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Summary of Presentation: Fe2+/H2O- mediated synthesis of Melanins: Cases of Homogentisic acid‚ serotonin‚ and norepinephrine The powerpoint presentation that I attended was titled‚ “Fe2+/H2O- mediated synthesis of Melanins: Cases of Homogentisic acid‚ serotonin‚ and norepinephrine‚” the research covered melanin which is a dark pigmentation that can cause other complication and pathological conditions such as‚ vitiligo and ochronosis. It is believed that melanin protects from ultraviolet light rays
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Laboratory Exercise #3 Measuring Protein in Solution Abstract The purpose of this lab was to learn about the Biuret assay reaction to determine if it can detect proteins and amino acids; also‚ to understand the process of “salting out” proteins and how to determine the amount of protein in a solution. In order to do so‚ egg white and ammonium sulfate were mixed on ice and then put into the centrifuge. After PBS was added‚ the amount of protein could then be determined. After that‚ 14 test tubes
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like shampoo‚ liquid soap and bubble bath. Environmental Working Group’s analysis suggests that 97 percent of hair relaxers‚ 57 percent of baby soaps and 22 percent of all products in Skin Deep may be contaminated with 1‚4-dioxane [1]. Independent lab tests co-released by the Campaign for Safe Cosmetics in 2007 showed that popular brands of children’s bubble bath and body wash contained 1‚ 4-dioxane HEALTH CONCERNS:
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According to Figure 4 and 5‚ the moles of Cu initially obtained and at completion‚ differentiated. It was evident that the initial moles of Cu (0.0254)‚ did not regenerate all the amount‚ as 0.0124 moles of Cu was attained. In regards to this‚ the no. moles that was eliminated was approximately‚ 0.013. Respectively‚ in Figure 3‚ a large deviation amongst the initial and final quantity of copper‚ this implies that the rest of the mass that had diminished‚ was greater than the final product. These
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of gold from ore using cyanide. Before cyanide was used in extracting gold the recovery rate of gold was low. Cyanide was first used worldwide at the Crown Mine at Karangahake near Waihi in 1889. In the next three years six more plants were created on The Coromandel. Cyanide has been used all over the world to make the extraction of gold easier. Although cyanide is helpful in terms of recovering gold it has been used throughout history as a deadly poison. Hydrogen cyanide has been used to disinfect
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Abstract This experiment investigated the kinetics of the enzyme glycogen phosphorylase b which is important to metabolism. AMP is an allosteric activator of the enzyme because it converts glycogen phosphorylase b from its T state to the R state which is the active form. Caffeine is an inhibitor because it binds the nucleoside inhibitor site. When it binds this site‚ it stabilizes the inactive T state and blocks the catalytic site which needs to be open for enzyme activity to occur. The glycogen
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Experimental Synthesis of Aspirin and Melting Point Purity Analysis Donald Yeargin CH 222‚ Section 24221 Department of Chemistry Portland Community College Portland‚ OR Abstract The various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize acetyl salicylic acid (aspirin) and then determine the relative purity of the synthesized sample by observing the melting point temperature
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In experiment 3.1.We set up and calibrate the spectronic 20 first since it takes time to be ready to use so‚ we turned the spectronic 20 to warm up for at least 15 minutes‚ set wavelength to 360 while no test tube in it. Also‚ we set the filter lever in order to match the wavelength range‚ and then set the transmittance to 0%‚ then we changed the mode to absorbance. After we labeled two test tubes which were #5 and #10‚ we inserted water first to set 0 absorbance‚ then we used #5 sample to read it
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