Synthesis The old acetate department located in an old four storey building follows a workflow that is heavily based on shifts/rotations because production is based on a per batch basis. A typical shift‚ the group leader and his crew would complete two or three batches. The night shift usually has lesser work because no deliveries were made. In the new system‚ the management wants to improve productivity. The department was redesigned from batches to continuous processing. Technical changes
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250 ppm‚ 200 ppm‚ 100 ppm‚ and 25 ppm of 12C solution was prepared from a caffeine stock solution using ethyl acetate as the solvent. 250 µL of each dilution was added to a respective 0.6 mL vials with 50 µL of 13C and mixed. Next‚ three 15 mL centrifuge tubes were labeled as “Unknown A‚” three were labeled as “Unknown B” and one was labeled “Control.” To each tube‚ 4 mL of ethyl acetate and 1 mL of the respective unknown or control (100 ppm 12C solution) was added to the respective flasks. Each
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The goals of this experiment are to determine if the products derived from amide synthesis and Williamson Ether Synthesis are identical‚ and if one of the synthetic routes is more advantageous than the other. In Part 1‚ an attempt to synthesize acteophenetidin crystals by amide synthesis was made. We began by removing the colored impurities from the p-Phenetidine (reddish-brown) by placing 2g of the sample in 38 mL of hydrochloric acid and heating the solution to boiling point. Upon reaching just
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The percent yield of the isopentyl acetate was 74.3% and this low percent yield could have occurred due to some amount of gas escaping from reflux apparatus’ top or apparatus was not fully closed so that some of the heat escaped and did not proceed the reaction well‚ leaving reagents. Another source of error could be that some of the organic layer could have been transferred along with the aqueous layer when the aqueous layer was getting separated from the organic layer by a pipette. One of the
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Undoped and Ce doped ZnO thin films were prepared by the sol-gel process. Zinc acetate dehydrate was dissolved in a mixture of absolute ethanol and monoethanolamine (MEA) yielding to a precursor concentration of 0.4 M .The MEA to zinc acetate molar ratio was set to 1. For doped films‚ cerium nitrate was added to the mixture with an atomic percentage fixed at 0.1‚ 0.3‚ 0.5‚ 0.7‚ and 0.9 at.% Ce‚ respectively. The resulting sols were magnetically stirred at 60°C for 1 hour and then aged at room temperature
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I. INTRODUCTION Synthesis Acetylsalicylic acid is an acetyl derivative of salicylic acid which appears as a white and crystalline and a weakly acidic substance with a melting point of 135°C and is also known to be aspirin. It is one of the most widely used drugs that can lower fever and is used as a painkiller. According to (Escobel‚ 2011)‚ Aspirin is synthesized through the reaction of salicylic acid with acetyl anhydride that causes a chemical reaction that turns salicylic acid’s hydroxyl group
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II. Synthesis This activity helps me to understand myself better by knowing what people think of me. It aims to foster self-awareness and self-improvement. I found out that my family thinks that I am a responsible person in terms of sense of responsibility. But my brother thinks I’m immature. In terms of duties at home‚ my mother and father understand that I don’t perform my duties because I’m busy with my studies. My sister thinks it too but she justified that I perform when I’m not busy. When
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SYNTHESIS OF ESTERS USING GREEN AND NON-GREEN CHEMISTRY Abstract Esters are a class of organic compounds with the general formula RCOOR’. Ester also contributes the flavor and aromas in fruits and flowers. The esterification reactions will use in the procedure‚ which are the interaction of a carboxylic acid with an alcohol‚ aided by an inorganic acid catalyst (H2SO4). Moreover‚ the green method will not use any catalyst but using heating source instead (microwave). Based on the comparison of
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CHEM3412 Synthesis of a Porphyrin Porphyrins are hetereonuclear‚ macrocyclic compounds that play an important role in living organisms. Examples include the non-protein heme portion of hemoglobin in animals whereby the lone pairs on nitrogen can bind to the oxygen-carrying iron. In plants‚ chlorophyll uses the vast conjugation to allow absorption of light for photosynthesis. The characteristic colors of porphyrins is also due to the conjugation. An examination of the porphyrin structure
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Synthesis The idea of gender wage discrimination being widely practiced in the United States today is a difficult concept for many to swallow. With the Equal Pay Act of 1963 and Title VII of the Civil Rights Act of 1964‚ the realization of the existence of the gender wage gap surprises many Americans. These authors bring to the forefront the idea that there is more to the gender wage gap then just companies discriminating against women and minorities. They sight many sources with defined data
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