Experimental Synthesis of Aspirin and Melting Point Purity Analysis Donald Yeargin CH 222‚ Section 24221 Department of Chemistry Portland Community College Portland‚ OR Abstract The various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize acetyl salicylic acid (aspirin) and then determine the relative purity of the synthesized sample by observing the melting point temperature
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Abstract The chloride present in an unknown soluble sample was precipitated into silver chloride through precipitation gravimetry. The colloidal silver chloride originally formed was converted to a crystalline solid by controlling certain parameters of the experiment such as temperature‚ pH of the solution‚ and concentration of AgNO3. Once the solid was large enough‚ it could be washed‚ filtered‚ and weighed. The percentage of chloride present was found to be 24.73695223 (±0.00000006) %.
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[pic] Organizational Culture of In-N-Out Burger Introduction Originally founded in 1948 by Harry and Esther Snyder‚ In-N-Out is notoriously known to be the nation’s most infamous chain of fast-food restaurants due to their simple‚ yet high quality products and services. Over the years‚ the company has grown to see their share of competition from places such as Five Guys and McDonalds. This however hasn’t phased In-N-Out as they continue to keep a steady growth file by
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Synthesis and Analysis of the Coordination Compound Pentaaminechlorideocobalt (III) Chloride Heaven Lin and Forest Lin W.M. Keck Science Department‚ Claremont McKenna‚ Pitzer‚ and Scripps Colleges 925 N. Mills Avenue‚ Claremont‚ California 91711 Abstract Through using the spectrometer and titrations‚ the amount of the coordination compound‚ pentaaminechloridocobalt (III) chloride‚ was determined through a synthesis through an oxidation reduction of cobalt (II) chloride hexahydrate (CoCl2·6H2O)
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Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
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Introduction The purpose of this lab is to synthesize Lidocaine from 2‚6-dimethylaniline‚ using diethyl amine‚ 2-chloroacetyl chloride‚ acetic acid‚ and toluene. The Lidocaine was made by adding 2‚6-dimethylaniline to 2-chloroacetyl chloride in acetic acid. Sodium acetate is added in order to make the compound soluble. The product is dried‚ then treated with diethyl amine and toluene. This is refluxed using a water-cooled reflux condenser. The vapor is condensed by the cold water as the compound
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CHEMISTRY 101.1 Intermediate Chemistry Laboratory I Institute of Chemistry University of the Philippines‚ Diliman I. Synthesis of Salicylic Acid Purpose: Part I of the experiment illustrates the base hydrolysis of an ester‚ methyl salicylate‚ to form salicylic acid through nucleophilic acyl substitution. Procedure: Dissolve 12 g NaOH in 70 mL water in a 150 mL round bottom flask. Add 5.0 mL methyl salicylate and reflux the reaction mixture at its boiling point for 15 minutes using a stirrer
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Quitay Morris Jake N. Professor Rafie Paz ENGL 1013 July 29 2013 Why are Teenagers so Lazy Today? The youth is the hope of the nation. That is the sentence that defines what the teenagers’ worth to the country is. We are supposed to change what the country is now. But the question is . . . Can we? From what I observed is happening now‚ instead of being the country’s biggest hope‚ we seem to be one of its burdens. There’s pre-marital sex‚ prostitution‚ juvenile delinquencies‚ and the list
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Chapter 2 METHODOLOGY Materials The materials used for the preparation of T. catappa seeds oil include: Hammer‚ G-clamp‚ stainless bowl‚ roasted T. catappa seeds‚ plain sheet‚ empty bottle‚ funnel‚ filter paper‚ stainless tube and trays. The materials used for the corrosion bath set-up include: Extracted oil from T. catappa seeds‚ cutter‚ 1 molar aqueous acetic acid and sulphuric acid‚ 1 galloon seawater‚ locally produced iron rods and tin cans‚ electrical cutter‚ beakers and transparent jars
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Anthony Felix 10/27/11 Che12ALR Synthesis of Diphenylacetylene Observation of Results: 1‚2-dibromo-1‚2-diphenylethane | 0.204g | Diphenylacetylene | 0.087g | Theoretical yield | 0.107g | Percent yield | 81.3% | Melting point range of diphenylacetylene | 57- 60°C | Average melting point | 58.5°C | Average literature melting point | 60.0°C | Percent error of melting point | 2.5% | Calculations: Theoretical yield: Limiting reagent (LR) x M.W. (LR) x Mole to Mole ratio x M.W. (product)
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