Recrystallization of Benzoic acid Chemistry 204-002 Date: 4/9/2011 Hector Ortega Recrystallization is a method used to purify compounds‚ and this is a very important procedure because compounds are naturally impure. Polarity and solubility play a big role in this experiment and these characteristics are exploited in order to have a crystallization of the desired compound. In this experimented benzoic acid was crystallize using ethanol and water. I chose these solvents based on part C of the experiment
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Spectra Analysis Organic Chemistry Lab‚ CHEM 369 The University of Tennessee‚ Knoxville Dr. Smith Spectra 1: tert-butyl cyanoacetate Molecular formula: 141/13 = 10 R 11 => C10H10+11 => C10H21 C10H21NO2 – C3H10 = C7H11NO2 DBE: 2(#C - #H/2 - #X/2 + #N + 2)/2 =2(7 – 11/2 – 0/2 + 1 + 2)/2 = 3=> 1 double bond and 1 triple bond Mass spectrum table: m/z fragment |40
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Abstract: Introduction: Materials: * Chemicals: Buffer solution‚ pH 7.0‚ 50 mL Phenolphthalein indicator solution‚ 1.0 %‚ 1 mL Potassium hydrogen phthalate‚ KHC8H4O4‚ 2 g sodium hydroxide solution‚ NaOH‚ 0.1 M‚ 150 mL Unknown weak acid‚ 1.5g Water‚ distilled or deionized * Equipment: Balance Stir bar Beaker‚ 250mL Oven Buret‚ 50 mL pH sensor Desiccator Rising stand and buret clamp Erlenmeyer flask‚ 125mL Wash bottle with distilled water Funnel Weighing dishes‚ 2
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Acid-Base Calculations The Ion-Product Constant for Water‚ Kw Water undergoes ionization to a small extent: H20(l) H+(aq) + OH–(aq) The equilibrium constant for the reaction is the ion-product constant for water Kw: (1) This is a key equation in acid-base chemistry. Note that the product of [H+] and [OH–] is a constant at a given temperature (Eq(1) value is for 25oC). Thus as the hydrogen ion concentration of a solution increases‚ the hydroxide ion concentration decreases
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Experiment Acids‚ Bases‚ and Neutrals Problem Are common house-hold products pH balanced and neutral? Information Gathered pH measures how acidic or alkaline a solution is. The pH scale ranges from 0-14. Solutions that range from 0-6 are considered to be acidic. Solutions that are on the acidic end of the scale are low in pH‚ high in hydrogen ion‚ and low in hydroxyl ions. An acid has a sour taste‚ hence‚ will react to metal and will be corrosive; therefore‚ they are considered as an electrolyte
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to practice common organic laboratory techniques inside the lab to get one oriented to the basic methods of procedure that can be used for later experiments. This experiment involves the separation of benzoic acid from a more crude form‚ consisting of benzoic acid‚ methyl orange‚ a common acid/base indicator‚ and cellulose‚ a natural polymer of glucose (Huston‚ and Liu 17-24). The technique that is used to perform this separation is called extraction. Extraction is a systematic process of separating
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Electrophoresis of Amino Acids Introduction: Electrophoresis is a separation technique based on the movement of charged ions under the influence of an electrical field. This technique is primarily used for the separation of amino acids and peptides on the basis of their charge. All amino acids contain ionizable groups that cause the amino acids‚ in solution‚ to act as charged polyelectrolytes that can migrate in an electric field. The amino acids with a net positive charge will migrate toward
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9.1 Sulphuric Acid Sulphuric Acid is Manufactured in Industry 1. Sulphuric acid‚ H2SO4 is manufactured in industry through Contact Process. 2. The raw materials used are sulphur‚ air and water 3. The Contact process consists of three stages. Stage 1: The production of sulphur dioxide This can be obtained by two methods: 1. Burning of sulphur in dry air in the furnace S + O SO2 2. Burning of metal sulphide such as zinc sulphide or iron(III) sulphide in dry air. 2ZnS
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STANDARDIATION OF ACID AND BASE Eunice Ivy B. Gamboa ABSTRACT Solutions of known concentration are prepared by dissolving measured masses of standard acids in distilled water. The concentrations of unknown solutions of sodium hydroxide are determined by titration. An acid solution reacts with a base solution in a "neutralization" reaction. Titrations permit the concentrations of unknown acids/bases to be determined with a high degree of accuracy. In order to analyze unknown acids/bases‚ we must have
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Acids and Bases Q1.This question is about several Brønsted–Lowry acids and bases. (a) Define the term Brønsted–Lowry acid. ........................................................................................................................ ........................................................................................................................ (1) (b) Three equilibria are shown below. For each reaction‚ indicate whether the substance immediately above the box is acting
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