CH 127 – Chem 2 Lab Determination of an Equilibrium constant Goals The purpose of this experiment is to determine the equilibrium constant for the reaction Fe3+(aq) + HSCN(aq) –>FeSCN2+(aq) + H+(aq). The equilibrium constant expression Kc for Reaction is kc=FeSCN2+[H+]Fe3++[HSCN] Procedure *Preparation of the Beer’s law plot Prepare five solutions of FeSCN2+(aq) of known concentrations between 1x10-5M and 1x10-4M by diluting various volumes of 4.62x10-4 HSCN. Calculate the Final concentration
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molecules (or atoms) in a gas are separated by large distances and are in constant‚ random motion. When dealing with gases‚ the Ideal Gas Law equation is the most famous equation used to relate all the factors in dealing and solving the problem. The four factors or variables for gas are: pressure (P)‚ volume (V)‚ number of mole of gas (n)‚ and temperature (T)‚ and the constant in the equation is R‚ known as the gas constant. The Ideal Gas law equation which is pV=nRT is obtained by combining the
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we had to save time and cut some days out. We were able to do this by being given our own Salicylic acid (SA) prepared for us instead of having to used wintergreen to make it and recrystallize it. In addition‚ we skipped the qualitative test of our purity for SA and Aspirin (ASA). The first part of this experiment is the preparation of ASA from SA were‚ we prepared our aspirin from the collected salicylic acid. A screw-capped vial was weighed empty to 29.7416 grams and filled with SA. The mass recorded
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Experiment # 3 Acetylsalicylic Acid Introduction: The purpose of this experiment is to create and isolate pure acetylsalicylic acid from the substances salicylic acid and acetic anhydride. Then one will find the melting point to determine purity. Procedure: Make a hot bath. Weigh some salicylic acid and place in conical vial. Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in
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reaction where the concentration of all the reactants and all the products remain constant over time. Equilibrium as used in chemical systems means that all the chemical forces in a reaction are in balance and that all physical properties of the system (color‚ density and concentration) of all chemicals species involved remains constant. The equilibrium state can be characterized by quantitatively defining its equilibrium constant‚ Keq. In this experiment the Keq for the reaction between iron (lll) ions
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DETERMINATION OF FRUIT ACIDS BY TITRATION AND CALCULATION OF THE SUGAR/ACID RATIO It is the sugar/acid ratio which contributes towards giving many fruits their characteristic flavour and so is an indicator of commercial and organoleptic ripeness. At the beginning of the ripening process the sugar/acid ratio is low‚ because of low sugar content and high fruit acid content‚ this makes the fruit taste sour. During the ripening process the fruit acids are degraded‚ the sugar content increases and
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The purpose of the Weak Acid Dissociation experiment is to determine the dissociation constant of a weak acid experimentally by using acid-base titration with a strong base and stoichiometry. An acid-base titration is a method by which a basic (or acidic) solution of unknown concentration is reacted with an acidic (or basic) solution of known concentration. (1) The pH in acid-base titration is measured using a pH meter or color changing indicator‚ such as phenolphthalein‚ as the known solution is
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Experiment # 4: Dissociation Constant Weak Acids Introduction: The dissociation constants of weak monoprotic acids were determined with the aid of a buffer and pH meter. Experiment: This experiment was performed according to the procedures as provided in the Chemistry 111B laboratory manual: Po‚ Henry and Senozan‚ N. "General Chemistry Experiments Chemistry 111B"‚ 8th Ed.‚ 2004 Hayden-McNeil Publishing‚ pp 80-88. To determine the dissociation constants of weak monoprotic acids (HX and HY)‚ a buffer
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EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound
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Spectrophotometric Determination of an Equilibrium Constant. Abstract: The report presents determination of equilibrium constant for the formation of a complex ion FeSCN2+. This was accomplished using a colorimeter to measure absorbance of some known concentration solutions in order to generate the calibration curve. The equation of the graph was used to compute the equilibrium concentrations of the reactants and products‚ needed to calculate the equilibrium constant for the reaction
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