The Purity and Purification of Solids- Part 2- Recrystallization Courtney Percival CH 337 Laboratory‚ Section 037 Department of Chemistry Portland State University‚ Portland OR ABSTRACT INTRODUCTION Recrystallization is a commonly used tool in laboratories when dealing with impure solids. "An effective recrystallization is one in which 1) a high degree of purity is achieved as well as 2) a maximum recovery of sample".1 Solubility‚ the tendency of a substance to dissolve in a liquid‚ is an
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From the graph I can clearly see that Distilled water has a much larger concentration of water then the cell sap in the potato tissue. I can make this conclusion because the results show a big increase in weight of the potato piece. Meaning that water has moved from outside the potato into the potato due to Osmosis‚ proving that the distilled water had a higher concentration of water‚ as water moves from a high concentration to a low concentration. I can also see that the glucose
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Experimental Synthesis of Aspirin and Melting Point Purity Analysis Donald Yeargin CH 222‚ Section 24221 Department of Chemistry Portland Community College Portland‚ OR Abstract The various methods available to synthesize aspirin lead to the need to examine and evaluate production efficiency and purity. The purpose of our experiment was to synthesize acetyl salicylic acid (aspirin) and then determine the relative purity of the synthesized sample by observing the melting point temperature
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Title: Acids‚ Bases & Buffers Objectives: 1. To understand the acid-base chemistry. 2. To prepare and evaluate a buffer system 3. To measure the buffering capacity of two types of isotonic drinks. Introduction: There are acid-forming‚ basic forming and neutral food‚ however the acid or alkaline properties of a food is unable to judge by the actual acidity of the food itself. For example‚ citrus fruits such as lemon are acidic‚ but they are alkaline-forming when we consume and digest it. Therefore
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The conventional method was conducted by placing 2.0641 grams of salicylic acid in a dry 125 mL Erlenmeyer flask. In a fume hood‚ 4 mL of acetic anhydride and 5 drops of concentrated sulfuric acid were added to the flask. The contents were swirled in the flask and then heated for 20 minutes in a hot water bath. After the 20 minutes were up‚ 10 mL of cold water were added in 1 mL increments. The flask was cooled for 10 minutes and occasionally stirred. The crystals that formed were collected via filtration
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aMicroscale Synthesis of Isopentyl Acetate (Banana Oil) Objective: Carried out the microscale synthesis of isopentyl acetate by direct esterification of acetic acid and isopentyl alcohol. This was an acid catalyzed Fischer esterification. Both extraction and distillation were employed to obtain a pure product. IR spectroscopy and gas chromatography were used to determine purity of the final product. Reagents: * Compound: | * MW (g/mol): | * MP (°C): | * BP (°C): | * Density (g/mL):
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Synthesis Conclusion: Conclusion: As we can see‚ the sources show us that during the Enlightenment period money was very important. It shows that during the time people would do merely anything for money‚ even force their children into arranged marriages or‚ as Voltaire suggest satirically‚ sell them as a food source. Parents or even the brides and grooms themselves would arranged marriages for economic gain. This was not always the case. We have learned from She Stoops to Conquer that‚ although
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Introduction to Acids Base chemistry Purpose How to determine the constant equilibrium of an acid‚ Ka? How to evaluate the concentration (M) of an acid? In “part A” experiment‚ we would test the PH of different concentration of acetic acid (a weak acid which partially dissociated in water) with a PH probe. After we got the PH‚ we could find out the concentration of H+ by applying the relationship pH = -log [H+]. Having the determined value of [H+] of a weak acid with a known molar concentration
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In part A‚ solutions needed in the experiment were prepared‚ and the LabQuest was set up. By adding 100mL 6M HCl to 200mL deionized water‚ 300mL of 2M HCl solution was prepared. Then 150mL 2M NaOH solution was prepared by adding 100mL 3M NaOH to 50mL deionized water. Finally‚ the LabQuest was connected to the temperature probe‚ and set up to collect data every 15 seconds‚ the duration was set to be 180 seconds. In part B‚ three reactions were performed. In reaction 1‚ two Styrofoam cups were stacked
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SYNTHESIS AND CHARACTERIZATION OF POLYANILINE/POLY (P-HYDROXYANILINE)/Fe3O4 MAGNETIC NANOCOMPOSITE M. R. SABOKTAKIN‚ A. M. MAHARRAMOV‚ M. A. RAMAZANOV Baku State University‚ Baku‚ Azarbaijan E-mail: mamed_r50@mail.ru Several composites have been studied for static dissipationand microwave absorbing materials based on polyaniline with metallic oxides. These composites which are conducting polymers have been widely used because of their lower density as well their good environmental stability as in
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