"Synthesis of salicylic acid and potentiometric determination of its purity and dissociation constant" Essays and Research Papers

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    Melissa Carrithers AP Chemistry period 6 2-11-15 Determination of Ka of Weak Acids Purpose: The purpose of this lab is to find the strength of weak acids by determining the equilibrium constants for their ionization reactions in water. Is to use their measured pH values to calculate the pKa for the two unknown weak acids thus determining their identities. Hypothesis: If we neutralize a solution that contains a weak acid by adding a strong base to the solution‚ then the ions will be isolated and

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    DATE PERFORMED: JULY 20‚ 2007 SPECTROPHOTOMETRIC DETERMINATION OF EQUILIBRIUM CONSTANT FOR A REACTION ABSTRACT UV-VIS spectrophotometry is one of the most widely-used methods for determining and identifying many inorganic species. During this experiment‚ this spectrophotometry was used to determine the equilibrium constant‚ Keq‚ of the Fe3+(aq)+SCN-(aq)↔ FeSCN2+(aq) reaction. By determining the amount of light absorbed‚ the concentration of the colored FeSCN2+ solution was also quantitatively

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    DETERMINATION OF THE SOLUBILITY PRODUCT CONSTANT OF CALCIUM HYDROXIDE ABSTRACT This experiment aimed to determine the solubility product constant (Ksp) of Ca(OH)2 as well as to evaluate the effects of common and non-common ions on its solubility. Ca(OH)2 solids were dissolved in eight various media: distilled water‚ 1.0 M KCl‚ 0.5 M KCl‚ 0.1 M KCl‚ 0.05 M KCl‚ 0.005 M KCl‚ 0.001 M KCl‚ and 0.1 M Ca(NO3)2. The concentration of dissociated OH- concentrations was determined by means of titrimetric

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    Date Performed: January 10 & 15‚ 2013 Spectrophotometric Determination of the Equilibrium Constant of a Reaction R.J.V. Ortega and J.C.V. Gatdula Institute of Chemistry‚ College of Science University of the Philippines‚ Diliman‚ Quezon City‚ Philippines Received January 22‚ 2013 ------------------------------------------------- ------------------------------------------------- ------------------------------------------------- ABSTRACT -------------------------------------------------

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    Acetylsalicylic acid is the active pharmaceutical ingredient in aspirin and can be synthesized by the esterification reaction of salicylic acid and acetic anhydride in the presence of an acid catalyst. An esterification reaction is when an acid is converted into an ester by combining with an alcohol and removing a water molecule. When heating the salicylic acid mixture in the warm water bath‚ the mixture should be removed from the bath within 8 minutes‚ to reduce the chance of the acetylsalicylic acid decomposing

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    CHEMISTRY 101.1 Intermediate Chemistry Laboratory I Institute of Chemistry University of the Philippines‚ Diliman I. Synthesis of Salicylic Acid Purpose: Part I of the experiment illustrates the base hydrolysis of an ester‚ methyl salicylate‚ to form salicylic acid through nucleophilic acyl substitution. Procedure: Dissolve 12 g NaOH in 70 mL water in a 150 mL round bottom flask. Add 5.0 mL methyl salicylate and reflux the reaction mixture at its boiling point for 15 minutes using a stirrer

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    Determination of the Equilibrium Constant for Ferric Thiocyanate In this laboratory exercise‚ the equilibrium constant(Kc) for the reaction between the Ferric Ion (Fe3+) and the Thiocyanate Ion (SCN-) was determined. After measuring the absorbance of the Ferric Thiocyanate‚ and carrying out some calculations; it was determined that Kc=130.81M Introduction: Chemical equilibrium is established when a reaction exists in a state where the forward reaction rate is equal to its reverse reaction

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    Acid Determination of Vitamin C Tablets and Salt Solutions Chem 1290-016 03-05-2010 ------------------------------------------------- Purpose: The purpose of this lab was to use acid-base titrations to find the mass percent of ascorbic acid in a Vitamin C tablet. A known concentration of sodium hydroxide was used and the value found was compared to the stated amount of ascorbic acid listed on the vitamin container. Also in this lab the acidity of different salt solutions were tested using

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    with the standard 0.050 M sulphuric acid provided‚ using phenol red indicator until two or three consistent results are obtained. d. Calculate the weight of acetylsalicylic acid in each tablet and compare your results with the manufacturer’s specification. Compare your results with those given in different brands of aspirin. Titration Results Titration trial 1 2 3 Final burette reading (cm3) Initial burette reading (cm3) Volume of acid used (cm3) Average volume

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    Data‚ Results‚ Calculations and Discussions Preparation of 250-mL 0.1 M NaOH Solution: Wt. of NaOH= (vol. of Sol’n) (M of Sol’n) (MW of NaOH) = (250 mL) (0.1 M NaoH) (40.0g/mol NaOH) Wt. of NaOH= 1.00 g • One gram of NaOH pellets was weighed and dissolved in distilled water. The solution was diluted to 250 mL. Table 1.Weighing of KHP (weighing by difference) |Replicate |Wt. of container -sample‚ g |Wt. of KHP

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