acetylsalicylic acid was synthesized from the acidification of salicylic acid and acetic anhydride. The objective was to convert a specific amount of salicylic acid into the same amount of aspirin that was high in purity. Furthermore‚ the other objectives were to enable students to conduct the synthesis of aspirin‚ reinforce skills or recrystallisation and the technique of melting point determination. The amount of each compound should be the same because there is a 1:1 ratio between them. The purity of the
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Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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changes in temperature. The changes in temperature were to be used to find the amount of heat released or absorbed. EXPERIMENTAL Reference """""""""""your website with your information""""""" RESULTS Calculation Calculation for determination of q: q = ms∆T Hess’s Law-type calculation ΔH = ΔHproducts – ΔHreactants J = g x [ J / ( g x ° C ) ] x ° C Calculation for Heat Change q=60g(160g*4.4c) =(60g*4.18J)/4.4j =1104.56 Joules CLASS TABLE part I
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From the historical readings of this week‚ one thing which has stood out the most is the concept of racial purity and consideration of black bodies as a threat to it. This fear of racial purity was evident in the miscegenation laws which prohibited interracial marriages. It also involved framing men as rapists. The enforcement of miscegenation laws and protection of white racial purity was justified by violence which involved lynching of black men. In her work‚ Ida B. Wells points out the very paradox
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The Equilibrium Constant of an Ester Hydrolysis Reaction CHM 152LL Section 33263 March 28‚ 2014 John Weide Abstract: The purpose if this experiment is to determine the equilibrium constant of an unknown alcohol. In this experiment unknown alcohol number three and unknown ester number three were used. The equilibrium constant was found by titrating a series of reactions containing H2O‚ HCl‚ and the unknown ester with only the last solution containing the unknown alcohol
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Title : Expt.1 Determination of the enthalpy (heat) of reaction of a monobasic acid with sodium hydroxide Experiment no : 1 Experiment title : Determination of the enthalpy (heat) of reaction of a monobasic acid with sodium hydroxide Objectives: 1) To understand the enthalpy chemistry. 2) To determine the calorimeter constant. 3) To determine the enthalpy reaction of acid-base reactions. 4) To study the exothermic reaction. Apparatus and Materials : * Dewar flask
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Dissociation is a protective mechanism that stimulates a person to enter into a detached state‚ in which the person is completely separated from his or her usual thought processes and memories. It is a state activated by one’s nervous system upon reaching maximum capacity to process the “real” stimuli around him or her‚ thus causing that person to lose track of time and find another representation of himself to continue in that moment. In “When I Woke Up Tuesday Morning‚ it was Friday‚” author and
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Standardization of NaOH and Determination of Unknown Acid KEYWORDS: quantitative analysis‚ titration‚ buret‚ endpoint‚ standardization‚ half-equivalence point‚ calorimetric titration‚ potentiometric titration ABSTRACT: The concentration of sodium hydroxide was determined by colorimetric titration‚ and the identity of an unknown acid was determined by potentiometric titration. In the first titration‚ a strong acid standard‚ potassium hydrogen phthalate (KHP)‚ was used‚ to determine the concentration
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Our words have a strong power. With our speech we have the ability to make worlds or break worlds. The Torah’s laws of speech make it possible for people to live together in peace and build close relationships. One who wants to create a serene home with a pleasant atmosphere should incorporate all the laws of shmiras haloshon into his actions and teach his family to follow suit. We deal with so many people and situations on a daily basis that frustration with others is inevitable. The laws of shmiras
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The Synthesis of Aspirin Chemistry Standard Level Lab Report Data Collection and Processing and Conclusion and Evaluation Date: December 8th‚ 2011 Purpose: The purpose of this lab was to synthesize aspirin‚ determine the theoretical yield‚ compare the percent yield to the theoretical yield and test the purity of aspirin by adding Iron (III) chloride to the product. Hypothesis: I hypothesize that salicylic acid will react with acetic anhydride to produce acetylsalicylic acid (aspirin)
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