EXPERIMENT 2: Recrystallization and Melting Point Recrystallization (or Crystallization) is a technique used to purify solids. This procedure relies on the fact that solubility increases as temperature increases (you can dissolve more sugar in hot water than in cold water). As a hot‚ saturated solution cools‚ it becomes supersaturated and the solute precipitates (crystallizes) out. In a recrystallization procedure‚ an impure (crude) solid is dissolved in a hot solvent. As this solution is cooled
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Acidification: From Nutmeg to Trimyrisitin to Sodium Myristate to Myrisitic Acid Mandy Boyle Chem 213‚ Section 002 Due Date: December 3‚ 2009 I. Introduction People encounter esters everyday in both natural and synthesized forms. Esters are present in a variety of common compounds‚ from fragrances to animal fat (McMurry‚ 2008). Although these esters can undergo many different important reactions‚ this lab is particularly interested in the hydrolysis of esters into carboxylic acids and alcohols
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between a carboxylic acid and an ester. Carboxylic esters‚ like isopentyl acetate‚ are normally used to create artificial flavors. In the preparation of isopentyl acetate‚ esterification of acetic acid and isopentyl alcohol occurs. Esterification is an equilibrium shift to the product side using an excess of one of the starting components. In this experiment‚ the excess reagent is acetic acid because it is not expensive and can easily be removed for the reaction. The acetic acid and isopentyl alcohol
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Olive oil is a fat obtained from the olive‚ a traditional tree crop of the Mediterranean Basin. The oil is produced by grinding whole olives and extracting the oil by mechanical or chemical means. It is commonly used in cooking‚ cosmetics‚ pharmaceuticals‚ and soaps and as a fuel for traditional oil lamps. Olive oil is used throughout the world‚ but especially in the Mediterranean countries. History The olive tree is native to the Mediterranean basin; wild olives were collected by Neolithic
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Lab Report Macrocyclic Synthesis (Heme Analog) I. Purpose of Experiment and Introduction The purpose of this lab experiment is to prepare meso-tetraphenylporphin (TPP) and its copper‚ cobalt or zinc complex by condensing benzaldehyde with pyrrole in boiling propanoic acid. II. Introduction and Background There are two types of proteins that function as oxygen carriers: myoglobin (stores the oxygen) and hemoglobin (present in red blood cells and is responsible for oxygen transport)
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Smith Advanced College Writing Dr. Ruby Parker Argument Synthesis April 21‚ 2011 Argument Synthesis In Mr. Siemiesz’s chapter he explained about the National Security Consequences of U.S Oil Dependence and how it could be fixed and changed for the best interest of the country; Mr. Siemiesz outlined specific points or steps the country could take to make those changes he outlined in the chapter. “Those major energy suppliers from Russia to Iraq to Venezuela have been increasingly able and
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International Journal on Marine Navigation and Safety of Sea Transportation Volume 2 Number 4 December 2008 Human Errors and Oil Pollution from Tankers P. Arsenie & R. Hanzu-Pazara Constanta Maritime University‚ Constanta‚ Romania ABSTRACT: The economical development of the world is based on transportation system. More than half of the products transported all over the world are carried by sea. Sea transportation is made with different kind of ships‚ as bulk carriers‚ cargo vessels
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Jewellyn G. Diola; ladyjewellyndiola@yahoo.com Abstract Synthesis of 3‚4-dihydro-3-(p-methylphenyl)-1‚2-(2h)-benzoxazine involves the nucleophillic addition of the 1 °amine group upon the carbonyly group of the salicylaldehyde‚ the reduction of imine to amine and the addition of paraformaldehyde to proceed ring closure. The experiment prepared the product through Mannich reaction‚ a multicomponent condensation synthesis between ketone‚ aldehydes‚ enols and amines. Biosynthesis of benzoaxazines
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CHEM3412 Synthesis of a Porphyrin Porphyrins are hetereonuclear‚ macrocyclic compounds that play an important role in living organisms. Examples include the non-protein heme portion of hemoglobin in animals whereby the lone pairs on nitrogen can bind to the oxygen-carrying iron. In plants‚ chlorophyll uses the vast conjugation to allow absorption of light for photosynthesis. The characteristic colors of porphyrins is also due to the conjugation. An examination of the porphyrin structure
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Science one world essay – Acid Rain Acid rain has been an important global issue for centuries. Although most acid rain is caused by human activities‚ some acid rain occurs naturally. An example of natural acid rain is erupting volcanos‚ they give off smoke containing water vapor‚ carbon dioxide‚ sulphur dioxide and nitrogen compounds. The sulphur dioxide and nitrogen compounds cause small amounts of acid rain near the volcano. Pure water is not an acid‚ but even clean rainwater is slightly acidic
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