aspirin and oil of wintergreen | Introduction Organic compounds are those which contain carbon as well as a select other elements. An organic acid however‚ is an organic compound which contains acidic properties. An ester is an example of being a derivative of these organic acids. Esters can be prepared by the reaction of carboxylic acids and alcohols‚ with an inorganic acid used as a catalyst which is dubbed esterification. With o-hydrobenzoic acid‚ or salicylic acid‚ we are able
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Synthesis of Salicylic Acid and Potentiometric Determination of its Purity and Dissociation Constant ------------------------------------------------- Abstract The purpose of the study is to synthesize salicylic acid from the ester‚ methyl salicylate‚ and determine the acid’s dissociation constant and purity. The ester was converted to salicylic acid by base hydrolysis. The products were refluxed and recrystallized‚ to ensure maximum purity‚ and filtered‚ dried‚ and weighed. The melting point
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Report Written: 08/02/2009 Synthesis of Acetyl salicylic acid (Aspirin) Abstract Introduction: The following report contains information on how to produce aspirin. The experiment has been carried out on a small laboratory scale. The experiment starts by combining such chemicals such as salicylic acid and acetic anhydride. The synthesis of aspirin is classified as an esterification reaction. This is a substitution reaction where the alcohol group from salicylic acid reacts with ascetic anhydride
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Experiment 22: Synthesis of Aspirin and Oil of Wintergreen Performed 01/31/2013 Received 02/07/2013 Organic molecules have a wide range of applications occur both intracellular as well as in many different industries. The reactions use the reactivity of functional groups attached to organic molecules‚ as well as general chemistry concepts such as Le Chatelier’s Principle (). The synthesis of Aspirin (its chemical name being acetylsalicylic acid) and of oil of wintergreen (with its chemical
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we had to save time and cut some days out. We were able to do this by being given our own Salicylic acid (SA) prepared for us instead of having to used wintergreen to make it and recrystallize it. In addition‚ we skipped the qualitative test of our purity for SA and Aspirin (ASA). The first part of this experiment is the preparation of ASA from SA were‚ we prepared our aspirin from the collected salicylic acid. A screw-capped vial was weighed empty to 29.7416 grams and filled with SA. The mass recorded
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Acetylsalicylic Acid (Aspirin) Synthesis Telow‚ AJV Sumicad‚ CJ‚ Tavanlar‚ EMMT‚ Chem 40.1‚ Institute of Chemistry‚ University of the Philippines Los Baños I. Introduction Organic synthesis is the process where a desired organic compound is constructed or prepared from commercially available materials. The objective of organic synthesis is to design the simplest synthetic routes to a molecule. Aspirin‚ also known as acetylsalicylic acid is as salicylate drug often used as analgesic
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October 9‚ 2013 Partner(s): Acetylsalicylic Acid Synthesis Theory. This experiment was carried out to see how the hydroxyl group on the benzene ring in salicylic acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above
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Experiment # 3 Acetylsalicylic Acid Introduction: The purpose of this experiment is to create and isolate pure acetylsalicylic acid from the substances salicylic acid and acetic anhydride. Then one will find the melting point to determine purity. Procedure: Make a hot bath. Weigh some salicylic acid and place in conical vial. Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in
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Synthesis of Aspirin Ling Tecson Gamido‚ Mitchiko Mariel M. Mizukami Abstract Acetylsalicylic acid‚ or also known as aspirin is known to be a drug that relives people of pain and is commonly used even today. It is synthesized from salicylic acid and ethanoic anhydride‚ both of small quantities. Phosphoric acid was used as a catalyst in the synthesis to speed up the process. Esterification is involved and the final product is aspirin with the presence of acetic acid as the byproduct. In order
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EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound
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