Title: Synthesis and Reaction of halogenoalkane‚ 1-bromobutane Aim: To prepare 1-bromobutane and investigate some of its reactions Materials and Apparatus: • Eye protection • Distillation Kit • Thermometer • Measuring cylinder • Teat pipette • Rack with 3 small test tubes • Beaker Chemicals: • Butan-1-ol (harmful and flammable) • Sodium bromide • Concentrated sulphuric acid (very corrosive) • Anhydrous sodium sulphate • Concentrated hydrochloric acid (corrosive) • Ethanol
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I. INTRODUCTION Synthesis Acetylsalicylic acid is an acetyl derivative of salicylic acid which appears as a white and crystalline and a weakly acidic substance with a melting point of 135°C and is also known to be aspirin. It is one of the most widely used drugs that can lower fever and is used as a painkiller. According to (Escobel‚ 2011)‚ Aspirin is synthesized through the reaction of salicylic acid with acetyl anhydride that causes a chemical reaction that turns salicylic acid’s hydroxyl group
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This solution served as the source of ionic Iron for the remainder of the lab and was labeled “stock ionic Iron solution.” Next‚ a 50-mL aqueous ionic Iron and FerroZine® complex solution was prepared by adding 5.00mL stock ionic Iron‚ 3-mL of acetic acid buffer‚ 2-mL of 5% hydroxylamine hydrochloride‚ allowing five minutes for hydroxylamine to reduce Fe3+ to Fe2+‚ adding 2.5-mL of 0.01 M FerroZine® solution‚ and mixing well. A single beam Agilent technologies CARY60-UV-Vis Spectrophotometer was then
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objective of the experiment was to prepare Benzilic acid by multistep synthesis starting with benzaldehyde. In this setup however‚ product of the first step‚ Benzoin‚ is provided thereby omitting the first step involving the conversion of benzaldehyde. For this experiment‚ the microscale techniques of reflux‚ crystallization‚ and melting-point determination were used. Utilizing these techniques a product yield of 93% for benzil and 57% for Benzilic acid was obtained‚ as well as a melting point range of
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Small samples of acetaminophen‚ acetylsalicylic acid‚ cellulose‚ starch‚ and caffeine were obtained. These samples were then placed into seperate sets of test tubes that contained water‚ acetone‚ or dichloroethane. Solubilities were then tested for each sample in each solution which can be seen in Table 5. Next‚ four random pills were obtained and weights were taken of each. Each of the pills were grinded up using a separate mortar and pestle. The grinded up pills were then weighed. The grinded
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the effect of concentration on the rate of a reaction Research question: To what extent does the concentration of hydrochloric acid affect the rate of the following reaction: 2 HCl(aq) + CaCO3(s) → CaCl2(aq) + H2O(l) + CO2(g) Data Collection and Processing: Table1: Different volumes of Co2 gas produced by Different concentrations of HCL acid. Volume of CO2gas formed from 5 different concentrations of HCL acid ±0.5ml 5 different concentrations of HCL acid (Mol) ±0.5ml Time (sec) ±0.1 0.25mol 0.50mol
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This experiment is to show how much carbon dioxide is produced during the reaction between an acid (hydrochloric acid) and marble. Equipment: Hydrochloric Acid (20ml) - 0.5M‚ 1M‚ 2M Marble Chips (2g per test) Large Measuring Cylinder Plastic Bowl (3/4 full of water) Rubber Tubing Glass Conical Flask Stopwatch Method The first thing that we did was fill the plastic bowl with water. We only filled it up 3/4 of the way because otherwise the water displaced into
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concentration of NaOH from 0.5M to 1M‚ then I will see the temperature slope increase in the reaction with an increased concentration because with an increase of moles‚ the particles will be colliding more often‚ therefore increasing the probability that the proper energy and alignment will occur to create more collisions in the same amount of time. Methods: List of Materials: • 110 mL of NaOH at 1 M (10 mL per run) • 110 mL of NaOH at 0.5 M (10 mL per run) • 220 mL of Acetic Acid at 50% (10 mL per
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Atausch July 28‚ 2014 Bio 102 Lab Final Exam: Acids and Enzymatic Reaction Purpose: To examine how an acidic fluid will modify the outcome of an enzymatic reaction. Introduction: Enzymes are “specialized proteins made by living cells that serve as biological catalysts.” (eScience Labs‚ LLC‚ 2013) These enzymes “allow certain industrial processes to be carried out at normal temperatures and pressures‚ thereby reducing the amount of energy and expensive equipment needed.”(BBC‚ 2012) Enzymatic
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The purpose of this experiment was to perform a wittig reaction‚ the horner-emmons wittig specifically‚ reacting an aldehyde with an ylide to make an alkene. This particular variation of the wittig reaction has several advantages: It gives only the trans product; it uses a much milder base that is easier to handle; and it gives a water soluble byproduct which is easy to separate from the product. The reason that these advantages occur is a change in the structure of the ylide. Instead of a tripheylphosphine
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