and methyl iodide(5ml) were added to the solution. The mixture was heated on a water bath for three hours. Acetone was removed and the residue was poured into water()150ml. The solid N-methypiperidone separated was filtered and recrystallised from ethanol. 4.6.General procedure for Preparation of the N-methylation of piperidin-4-one oximes: The piperidone (0.1mol)was dissolved in ethanol(50ml). saturated solutions of hydroxylamine hydrochloride and sodium acetate in water were added. The mixture
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Experiment 4 Synthesis of Salicylic Acid Introduction Throughout history‚ botanical extracts have been used as medicines. Approximately 30% of all medicines have a plant origin. This number increases to 60% if you consider medicines that at one time were derived from plants‚ but have been synthesized in the laboratory. Salicylic acid is a white crystalline compound that can be isolated from the bark of birch trees. Since it is a valuable substance that can be isolated from nature‚ it is called
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To prevent the previously discussed risks related to the equipment and substances used in the synthesis reaction‚ safety procedures were discussed with the teacher‚ the fume cupboard was used‚ hands were washed‚ correct disposal procedures were followed‚ Disinfectant was used to wipe down benches‚ no flammable or loose clothing was worn‚ long hair was tied back‚ no naked flames were used‚ the safety shower and eye bath was available‚ first aid facilities were available‚ required spill management
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5%
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Engels’s Argument on Housing Shortage In 1887‚ Frederick Engels published his book called “The Housing Question” where he strongly advised to abolish the system of capitalism. In this paper‚ one will look into Engels’s logicality on the steps he uses to connect capitalism and housing shortage. Through the process of capitalism‚ the rise of Haussmannization‚ and the never-ending circle of housing shortage‚ readers will understand why Engels believes that capitalism should be removed to
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Experiment 1: Synthesis of Copper Compounds Introduction This experiment involves the synthesis of compounds originating from pure solid copper. By applying solubility rules and the reactive properties of substances‚ many compounds which would otherwise be costly to extract from nature are able to be synthesized in the laboratory. Laboratory synthesized may sometimes be more economical than natural extraction‚ however it poses its own problems with the amount of substance that is actually yielded
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Jean Watson’s Philosophy of Nursing NUR/403-Theories and Models of Nursing Practice August 9th‚ 2010 Introduction Jean Watson’s theories of nursing are instrumental in today’s structure of nursing. Watson’s theories are being practiced in various health care setting all over the world. One of these theories in the nursing process. This entails first assessing patient‚ planning
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The basic roles of associate-degree level and baccalaureate-degree level nursing have many similarities in their structural foundation. Nurses learn to promote health and healing in a caring environment. To support the plan of care by preventing disease and assisting in early detection of deviations from the plan of care. Teaching and promoting positive response to treatments. Extending compassion in times of need to the sick and dying patient. The differences lie in how the BSN is expected to
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Minimum Wage For years there has been disagreement over whether the minimum wage should be raised or not. Some believe that by raising the minimum wage‚ many Americans would be able to rise above the poverty line and have access to their dream. Others disagree saying that raising the minimum wage would only make it more difficult for businesses to pay workers and people would lose incentive to work hard. The only just choice is to raise the minimum wage so that hard working Americans can exceed
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GDF15/MIC-1 is a product of macrophage activation‚ suggesting that it may be involved in chronic inflammatory processes (-). GDF15 is a stress-responsive member of the TGF-β superfamily and initially described as macrophage inhibitory cytokine (-). Although GDF15 has been described in many solid tumors for almost 10 years‚ the nature of its receptor is still unknown. There is some evidence of Smad signaling pathway activation‚ suggesting GDF15 may act through TGF-β receptor superfamily pathways (-)
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