Materials and Methods: Methods and materials used in this experiment can be found in the BIOL 1F90 Laboratory Manual (Martin‚ 2013)‚ Experiment # 1‚ pages 2-5. Results: Table 1: Culture Sample Chromatography Rf Values Sample of Spot Distance from Origin (mm) Solvent Front (mm) Rf Value Color A 6.0 57.0 0.22 Bluish green B 17.5 56.0 0.105 Dark green blue C 4.0 57.0 0.070 Greenish blue D 4.0 47.0 0.085 Green E 10.5 56.5 0.186 Light blue Figure 1: Chromatography- TLC sheet From left to right-
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Grignard Synthesis of Triphenylmethanol Aim The aim of this experiment was to prepared Grignard reagent (phenylmagnesium bromide) from bromobenzene and magnesium‚ to use the reagent prepared to synthesise a tertiary alcohol (triphenylmethanol) by reacting reagent and ester (methyl benzoate)‚ and the product formed is analyse by infrared spectroscopy (IR)‚ melting point‚ thin layer chromatography (TLC)‚ gas chromatography mass spectrum (GCMS) and finally Nuclear Magnetic Resonance spectroscopy. Introduction
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See Student ID: 1404057 Practical Group: 1 Title of Experiment: Name of Tutor: Dr. Mohammod Aminuzzaman Date: 24 February 2016 Tiltle: Nitration of Methyl Benzoate Objectives: -To prepare methyl-3-nitrobenzoate from nitration of methyl benzoate by electropilic aromatic substitution. -To calculate the percentage yield and get the melting point of methyl-3-nitrobenzoate. Introduction: Benzene contains compounds have special properties that make them to react differently than other molecules. The conjugated
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not. Not many fruits and vegetables contain preservatives simply because they come from nature. One of the items contained Sodium Benzoate‚ a small percentage of people are extremely sensitive to sodium benzoate and can experience asthmatic attacks and other allergic reactions when they take in the preservative. A more normal problem is the combination of sodium benzoate and citric acid and ascorbic acid. When these ingredients mix‚ they form benzene‚ a cancer-causing chemical linked with leukemia
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Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
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Special Report Methyl ethyl ketone – A techno-commercial profile M ethyl ethyl ketone (MEK or 2-butanone) is an organic compound with the formula CH3C(O)CH2CH3. Its CAS number is 78-93-3. The colorless liquid ketone has a sharp‚ sweet odour of butterscotch and acetone. It is produced industrially on a large scale‚ and also occurs in trace amounts in nature. It is soluble in water and is commonly used as an industrial solvent. With natural and synthetic resins‚ MEK produces solutions with low viscosity
Free Solvent Acetic acid Acetone
I. INTRODUCTION Synthesis Acetylsalicylic acid is an acetyl derivative of salicylic acid which appears as a white and crystalline and a weakly acidic substance with a melting point of 135°C and is also known to be aspirin. It is one of the most widely used drugs that can lower fever and is used as a painkiller. According to (Escobel‚ 2011)‚ Aspirin is synthesized through the reaction of salicylic acid with acetyl anhydride that causes a chemical reaction that turns salicylic acid’s hydroxyl group
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Jeana Greaves Chem3301-112 June 19‚ 2013 Synthesis of Aspirin from Methyl Salicylate Introduction The synthesis of Aspirin (Acetyl Salicyclic Acid) began with methyl salicylate and sodium hydroxide as the reagent. The polar oxygen accepts the electrons from now positively charged hydrogen. The positively charged sodium disassociates leaving the hydroxide ion with a negative Scheme 1 shows the mechanisms that were demonstrated during the synthesis of Aspirin. charge that attracts to the positively
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In many ways‚ in Mohsin Hamid’s novel The Reluctant fundamentalist‚ the relationship between Changez and Erica mirrors that the failed love affair between Changez and the United States. Throughout the novel these two idea’s run parallel to each other‚ for example when Changez and Erica make love she can only accept him if he pretends to be Chris‚ Not unlike how Changez can only be accepted into America society if he possesses an American degree an American job and supresses his Pakistani identity
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RF Based Wireless Electronic Stethoscope Mubashir_ul_Hasan‚ Zaryab Qazi‚ Sander Ali Student‚ (IICT) University Of Sindh Jamshoro‚ Sindh‚ Pakistan Engr_mubashir41@yahoo.com Student‚ (IICT) University Of Sindh Jamshoro‚ Sindh‚ Pakistan Zaryabqazi@yahoo.com Lecturer‚ (IICT) University Of Sindh Jamshoro‚ Sindh‚ Pakistan Sandar.ali@usindh.edu.pk Abstract Direct way to diagnose the diseases is the use of stethoscope. In this paper the working and making of low cost Wireless electronic stethoscope
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