The purpose of this experiment was to synthesize triphenylmethanol from a Grignard reagent. The Grignard reaction technique was used in this synthesis but due to the fact that it is such a strong nucleophile and base‚ it was important to prevent water from interfering with the Grignard reaction. Purity of the product was determined by measuring the melting point. Reagent Table: Structure Name Molecular formula Molar mass Density Melting point Boiling Point Diethyl ether C4H10O
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Chem 51LC Experiment 6 Lab Report Aldol Reaction Purpose: The purpose of this experiment is to be able to conduct an aldol condensation reaction using an unknown aldehyde and an unknown ketone. H NMR is used to identify the unknown aldehyde and ketone. Melting point is used to identify the aldol condensation reaction. Theory: Condensation reaction is also known as a dehydration reaction. In the mechanism of condensation reaction‚ a bond is formed between two molecules and creates water as a
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Rates of Chemical Reaction II Pre-Lab Summary: First we will set up the experiment as shown in Figure 2‚ and then we will fill the trough with room temperature water and record the temperature and we will also add the room temperature water to the buret until it is about 10ml from the top. If there are no leaks in the apparatus‚ we will add 10ml of KI to 15ml of distilled water in a 125ml flask. We will swirl the flask so that it achieves room temperature‚ then we will add 5ml of H2O2 and quickly
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Mole Ratio of a Chemical Reaction: Copper & Silver Nitrate Lab #4 OBJECTIVE In this experiment‚ you will determine the number of moles of reactants and products present in the reaction of copper and silver nitrate‚ and calculate their mole-to-mole ratio. The mole-to-mole ratio relating to the disappearance of copper and the formation of silver metal will be used to write the balanced equation for the reaction. The reaction of copper metal with silver nitrate solution is a single
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The SN2 reaction requires three qualities: a strong nucleophile‚ a good‚ unhindered leaving group‚ and a polar‚ aprotic solvent. For our reaction‚ we have all three bases covered. The nucleophile is an alkoxide‚ a deprotonated alcohol. Technically‚ because our alcohol is a phenol‚ the conjugate base is called a phenoxide. Phenol itself has a pKa of about 10‚ but our alcohol has more resonance opportunities‚ so the pKa is down around 8. This is sufficiently acidic for use of weak base like K2CO3 for
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safety feature in vehicles. Sodium azide‚ potassium nitrate and silicon dioxide have been used in one design of airbag. [Source: www.hilalairbag.net] Sodium azide‚ a toxic compound‚ undergoes the following decomposition reaction under certain conditions. 2NaN 3 (s) → 2Na (s) + 3N 2 (g) Two students looked at data in a simulated computer-based experiment to determine the volume of nitrogen generated in an airbag. (a) Sodium azide involves ionic bonding‚ and
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Chemical Reactions- Sodium Hydroxide A chemical reaction is a change where two or more substances are changed into a new substance. You can identify a chemical reaction by colour change‚ effervescence (bubbles)‚ when light or heat given off‚ and the change is usually irreversible. There are 6 main types of chemical reactions- combustion (often called burning)‚ synthesis‚ decomposition‚ neutralization‚ single replacement and double replacement. A combustion reaction is a reaction with oxygen‚ and
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How can we speed up the reaction between Calcium Carbonate and Hydrochloric Acid? Contents 1. Plan  Aim  Equipment  Variable Factors  Prediction  Method  Trial Run 2. Results  Results Tables 3. Analysis and Conclusions  Graphs  Conclusions 4. Evaluation  Accuracy Of Results  Reliability  Improvements  Extending the Investigation 1. Plan Aim I am doing this
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points] Calculate the pH of 1.00 L of the buffer 1.00 M CH3 COONa/1.00 M CH3 COOH (pKa = 4.74) before and after the addition of (a) 0.080 moles NaOH and (b) 0.12 moles HCl. (Assume there is no change in volume). 3. [10 points] The following reaction is found to be first order in A: A −→ B + C If half of the starting quantity of A is used up after 56 seconds‚ calculate the fraction that will be used up after 6.0 minutes. 4. [15 points] The rate law for the decomposition of ozone to molecular
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The Diels-Alder Reaction Submitted by: Joe Student Partner: Jill Student Date: February 8‚ 2005 TA: Super TA Reaction +OOOxylene140 oCOOO Data Table Reagents MW Grams used Lit. Mp Anthracene 178.23 g/mol 1.023 g 216-218ºC Maleic anhydride 98.06 g/mol 0.497 g 54-56ºC Products MW Grams obtained Lit. Mp Observed Mp Crude product 276.29 g/mol 1.362 g 261-262ºC 260.2-261.3ºC Recryst. Product 276.29 g/mol 1.283 g 261-262ºC 261.3-261.9ºC Results and Discussion Discuss the
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