several processes and using different compounds as reactants. One of the simplest method used is the addition of a hydrogen halide to an alcohol. In this research‚ tert-butyl alcohol was reacted with cold concentrated HCl to produce tert-butyl chloride. The crude product was distilled to yield a pure tert-butyl chloride. The tert-butyl alcohol‚ together with HCl‚ underwent an SN1 nucleophilic substitution reaction‚ which is composed of three steps—(1) propanation of alcoholic oxygen‚ (2) formation
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Jornd Experiment 7- Synthesis and Reactivity of tert-Butyl Chloride Via an SN1 Reaction Introduction/Background: Alkyl halides are compounds in which a halogen atom replaces a hydrogen atom of an alkane. Alkyl halides are classified as primary‚ secondary or tertiary depending on the number of alkyl substituents directly attached to the carbon attached to the halogen atom. The purpose of this lab was to properly prepare t-butyl chloride from t-butyl-alcohol in a concentrated hydrochloric acid. The
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Tea 4 Extraction of Trimyristin from Nutmeg 5 Conversion of t-butanol to t-butyl chloride 6 Appendix 7 Calculations 8 Literature and Experimental Values of Benzoic Acid and Acetanilide 9 Experimental Caffeine IR 10 Literature Caffeine IR 11 Experimental Trimyristin IR 12 Literature Trimyristin IR 13 Experimental Tert- Butyl Chloride IR 14 Literature Tert-Butyl Chloride IR and RI 15 References Separation of Benzoic Acid and Acetanilide Introduction:
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to use to differentiate toluene from benzaldehyde is concentrated sulfuric acid (H2SO4) since benzaldehyde is soluble in sulfuric acid unlike toluene. d. tert-butyl chloride and tert-butanol The best solvent to use to differentiate tert-butyl chloride and tert-butanol is water since tert-butanol is very soluble in water while tert-butyl chloride is not. References: Jain‚ M. (Ed.). (2008‚ June). Aromatic Conversions.
Free Solvent Oxygen Ethanol
allows the separation of it from the aqueous layer using a separatory funnel. The alkyl halide‚ then‚ were purified by a simple distillation apparatus using boiling point differences between the pure tert-butyl chloride and not. In this experiment‚ tert-butyl chloride is synthesized from tert-butyl alcohol. Introduction Alkyl Halides (also known as halogenoalkanes or haloalkanes) are a group of chemical compounds derived from alkanes containing one or more halogens. They are a subset of the general
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CLASSIFICATION TESTS FOR ORGANIC HALIDES James Anand L. Regala‚ Sabrina Nicolle G. Sarte‚ Ann Michelle Siao‚ Michael Sibulo‚ Victoria Tan Group 8 2C Pharmacy Organic Chemistry Laboratory ABSTRACT This experiment is done to classify organic halides. Most organic halides are synthetic and are not flammable. One way to classify organic halides is by classifying its -carbon atom as primary‚ secondary or tertiary. If the -carbon is attached to one R group‚ it is then primary. If the -carbon is
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water test showed that the sample‚ benzyl alcohol was immiscible while ethanol was the most miscible from all the other compounds used. While in Lucas Test which was used to differentiated the primary‚ secondary‚ and tertiary alcohols had turned tert-butyl alcohol into a cloudy solution afterwards. In Chromic Acid Test which was a test for oxidizable compounds or any compounds that possess reducing property would yield to a blue green solution if it reacted positively. This was seen in all the sample
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for 2-butanol was also SN2‚ and bromide is a better nucleophile. Due to the smaller percentage compared to 1-butanol‚ the mechanism of 2-butanol could either be a mixed between SN1 and SN2 because the substrate is a secondary alcohol. Bromide and chloride were both good nucleophiles‚ but bromide was the better nucleophile in 2-butanol as it yielded 78‚63% of 2-bromobutane. 3. In 2-methyl-2-propanol Since the substrate is a tertiary alcohol‚ SN1 should be favor regardless of the strength of nucleophiles
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nExperiment C: Kinetics of the Hydrolysis of T-butyl Chloride Post-Lab Ch202 Postlab Assignment Nov 5/2014 L10 Radwan Ahmed 130770850 1. What was green about this experiment was that the solvents used (acetone and water)‚ and even the tert butyl chloride were fairly safe to handle with respect to the other chemicals used in the lab. This is why gloves were not worn‚ and one reason why this experiment follows GCP # 3 where chemical products should be designed to preserve efficacy of the function
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EXPERIMENT 8 BOILING POINT n-Butyl Alcohol n-Butyl Alcohol‚ a four carbon straight chain alcohol‚ is a volatile‚ clear liquid with a strong alcoholic odor; miscible with water. It is flammable strongly with a luminous flame. Formula: C4H9OH Boiling point: 118 ºC Melting point: -89 ºC Tert-Butyl Alcohol Tert-Butyl Alcohol or “2-methyl-2-propanol” is the simplest tertiary alcohol. It is one of the four isomers of butanol. Tert-Butanol is a clear liquid (or a colorless solid‚ depending on
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