Diels-Alder Synthesis of Exo-Norbornene-cis-5‚6-Dicarboxylic Anhydride for Organic Chemistry Laboratory Instruction Kyle Myers and Dr. James Roark University of Nebraska at Kearney‚ Department of Chemistry‚ Kearney‚ NE 68849 Abstract A technique for the Diels-Alder synthesis of endo-norbornene-cis-5‚6dicarboxylic anhydride and its stereoisomer‚ exo-norbornene-cis-5‚6-dicarboxylic anhydride‚ is explained. To prove that each stereoisomer was made in the experiment and to distinguish between the
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2013 “Reaction Classes and Pericyclic Reactions” ● 4 Lectures ● Recommended Texts: (i) J. March “Advanced Organic Chemistry”‚ p 839‚ `---Edn.‚ Oxford (W); Warren (2) Ch 34‚ 35. Syllabus 1) General principles (a) Reaction classes (i) Heterolytic (ii) Homolytic (iii) Pericyclic (b) Pericyclic Reaction Types 2) Electrocyclic Reactions (a) Definition and examples (b) Stereochemical aspects and the Woodward and Hoffmann rules 3) Cycloaddition Reactions (a) Definition
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variety of chemicals and materials used in electronic components‚ printed circuit boards‚ consumer electronics and other industrial products. This report focuses on analyzing photoresist & its special chemicals and capacitor chemicals as well as maleic anhydride derivatives used in printed circuit boards‚ flat panel displays and semiconductors. 1 Photoresist Photoresist is mainly used for fine graphics processing in PCB‚ LCD‚ semiconductor and other areas. In 2013‚ the global photoresist market scale
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Nor Amirah Farhana Nawawi Organic Chemistry Lab Report Bo Shen Title: Nucleophillic Substitution Reaction Introduction: This lab experimented on the reactions of the chemicals that undergoes SN1 or SN2 reaction. Nine different compounds were given to be examined with two reagents - NaI in acetone and AgNO3 in ethanol. The SN1 reaction happens in AgNO3 in ethanol reagents‚ and SN2 reaction is in NaI in acetone. Procedure: Following the lab manual. Results: compound NaI /acetone (SN2) AgNO3/ethanol
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majority of your time is spent in the past or future‚ but rarely living in the realism of NOW.’ - Shannon L. Alder The quote listed above by Shannon Alder is very meaningful and thought provoking‚ relating to not just people who suffer from personality disorders‚ but to anyone that may occasionally be conflicted with stress‚ anxiety‚ or any other forms of suffering. Prioritizing the focal point‚ Alder acknowledges how the ‘true definition’ of a mental illness is over-contemplating our past or future when
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The literature value for the melting point range for Trans-9-(2-phenylethenyl)anthracene is 130-133 oC. The obtained range was lower than that at 120.3 to 123.8 oC. Because it is lower than the known value‚ this means the obtain product is not completely pure. Impurities in the compound can result in a decrease in the compounds melting point‚ which is observed here. The impurities could be 1-propanol due to an insufficient drying. If the experiment was performed again‚ the product would need to be
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Synthesis of trans-9-(2-Phenylethenyl)anthracene Introduction The purpose of this experiment was to convert carboxyl compounds into alkenes. While this reaction yields both the E and Z isomers‚ it is preferred over other reactions due to the lack of uncertainty of where the double bond is positioned. Also the stability of an ylide determines which isomer is the major product. 1 Experimental: Compounds Benzyltriphenylphosphonium chloride 9-Anthraldehyde 50% Aqueous NaOH DCM Product Formula weight
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Alfred Alder Feb. 7th‚1870 - May 28th‚ 1937 Alfred Alder is a psychologist whom was born in Vienna‚ Austria. As a child‚ Alfred suffered with Rickets. Rickets is a disease that is caused by a lack of vitamin D‚ calcium‚ or phosphate. Rickets leads to the softening and weakening of the bones. Because of Alder having this disease‚ he was restricted to a wheel chair until the age of four when he was able to walk on his own. Due to Alder having
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Title: Recrystallization of Pure Phthalic Acid‚ Naphthalene‚ and Anthracene Introduction Recrystallization is a method used for purifying solid organic compounds. It is the most efficient method to purify and remove impurities from a solid to allow a crystal to grow. The method is when the solute in a hot solvent yields to a solution. Once the solvent cools‚ the solution is saturated with respect to the solute‚ which is when it recrystallizes. A crystal is the end result of the method and it is a
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Reaction on Reaction Paper The first thing that came to my mind when I have heard about Reaction paper is “What exactly is it?” and before I get an understanding of that‚ I resisted that change. But later‚ when I have studied about it and understood its purpose‚ I have started thinking “Why people avoid change at the first look without an analysis?” The general human tendency is to live in a comfortable zone in which he has lived for quite some time. He draws a circle‚ thinks that circle is his
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