Amanda Jornd Experiment 7- Synthesis and Reactivity of tert-Butyl Chloride Via an SN1 Reaction Introduction/Background: Alkyl halides are compounds in which a halogen atom replaces a hydrogen atom of an alkane. Alkyl halides are classified as primary‚ secondary or tertiary depending on the number of alkyl substituents directly attached to the carbon attached to the halogen atom. The purpose of this lab was to properly prepare t-butyl chloride from t-butyl-alcohol in a concentrated hydrochloric
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I- :2S2O32I2 + 2e S4O62- + 2e 2I- The iodine/thiosulphate titration is a general method for determining the concentration of an oxidising agent solution. A known volume of an oxidising agent is added into an excess solution of acidified potassium iodide. The reaction will release iodine:Example: (a) With KMnO4 2MnO4- + 16H+ + 10I(b) With KIO3 IO3- + 5I+ 6H+ 3I2 + 3H2O 2Mn2+ + 5I2 + 8H2O The iodine that is released is titrated against a standard thiosulphate solution. From the stoichiometry of the
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light (put in a dark place) will not decompose. Theory: Equipment: * 4 x petri dishes * 1 x glass stirring rod * 0.1 mol/L silver nitrate in a dropper bottle * 0.1 mol/L Sodium chloride in a dropper bottle * 0.1 mol/L Sodium iodide in a dropper bottle Method: 1. Ensure you are wearing safety glasses 2. Take the petri dishes and label then 1‚ 2‚ 3‚ and 4. 3. Add 20 drops of silver nitrate solution to each petri dish. 4. Add 20 drops of sodium chloride to petri
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which of the two will reacted with potassium iodide inside the breaker‚ as the latter passed from the beaker into the tube‚ the glucose/starch solution’s change of color showed that the potassium iodide was small enough that it able to pass through from the solution and into the bag. After the Benedict test‚ glucose from the bag was also founded small enough that it can exit from the bag and into and solution. In the end‚ glucose and potassium iodide was the only two that is capable to move freely
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this example‚ magnesium is above copper in the activity series so it is able to displace copper. An example of an anion replacement reaction is the reaction of bromine and potassium iodide‚ which produces potassium bromide and iodide (Br2 + 2KI 2KBr +I2). In this example‚ bromine replaces iodide in the potassium iodide
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List: Sodium carbonate solution Copper sulphate solution (Safety: High toxicity) Sodium hydroxide solution (Safety: Irritant) Ammonia solution (Safety: Toxic by inhalation) Potassium iodide solution (Safety: Mild irritant) Lead nitrate solution (Safety: Toxic) Sulphuric acid (Safety: Corrosive) Copper carbonate Silver Nitrate (Safety:
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Reactivity of Halide Ions Michelle Faktor and Kelly Freas Date of Experiment: October 28‚ 2012 Period 2 Honors Chem Purpose: The purpose of this lab is to observe the reactions of halide ions with different reagents by mixing them together. Analyze data to determine characteristic reactions of each halide ion. Infer the identity of unknown solutions. Materials: * 0.1 M AgNo3 * 0.1 M NaCl * 0.1 M NaF * 0.2 M KBr * 0.2M Kl * 0.2 M Na2S2)3 * 0.5 M Ca(NO3)2
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Natural Antioxidant Concept: Vitamin C (ascorbic acid) is an antioxidant. The amount of vitamin C content in food can be found out by titrating with an oxidising agent‚ e.g. iodine. In the reaction‚ vitamin C is oxidised‚ while iodine is reduced to iodide ions. The endpoint is determined by the formation of blue-black starch-iodine complex when all vitamin C is oxidised and excess iodine is free to react with the starch solution added as indicator. Introduction Vitamin C is an important component
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reactions below‚ (i) state and explain what would be observed; and (ii) write an appropriate equation. (a) adding excess sodium sulphite solution to iodine solution (b) adding aqueous chlorine to potassium bromide solution (c) adding excess potassium iodide solution to acidified potassium permanganate solution 1 (d) adding excess iron(II) sulphate solution to acidified potassium dichromate solution (e) adding concentrated nitric acid to magnesium ribbons (f) (g) (h) (i) (j) (k) (l) (m) (n) 5. adding
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William son Eth er Synth esis Introduction In this reaction‚ an alcohol is deprotonated to form a good nucleophile‚ which then attacks the electrophile methyl iodide to form an ether. Tetrabutylammonium bromide‚ a phase transfer catalyst‚ is used to carry ions back and forth between the organic phase and the aqueous phase. OH O NaOH + NaI + H2O CH3I Before coming to lab‚ please review the following techniques: "Reluxing a reaction‚" "Extraction and washing‚" "Drying an Organic Solvent‚" "Evaporating
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