nitrogens on this station. Both of these methods rely on the repulsive electrostatic interactions between the positively charged axial component and the post-switching cationic nature of the benzidine station (Figure 5.4). Deuterated trifluoroacetic acid (d-TFA) was added in the solution which resulted in the protonation of the benzidine residue and shuttling of macrocycle in to the biphenol station of the Rotaxane. This was supported by NOESY 1H NMR that showed a shift in the peaks in retrospect to
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the experiment * Aim: To observe the reactions of sulfuric acid as an oxidising agent and as a dehydrating agent. Equipment: * 20mL of concentrated sulfuric acid * 20mL of 2mol/L sulfuric acid * 2 small pieces of each of copper‚ zinc and iron * Sandpaper * 10 test tubes * Test tube rack * 2g of sugar crystals (sucrose) * 2 wooden ice-cream sticks * 10mL measuring cylinders Steps: A: Sulfuric acid as an oxidising agent 1. Clean pieces of metal with sandpaper
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August 28‚ 2009 [PROBLEM SET FROM R. CHANG TEST BANK] Chapter 16 Acid-Base Equilibria and Solubility Equilibria Student: ___________________________________________________________________________ NOTE: A table of ionization constants and Ka’s is required to work some of the problems in this chapter. 1. In which one of the following solutions will acetic acid have the greatest percent ionization? A. B. C. D. 2. Which one of the following is a buffer solution? A. B. C. D. E. 3. 0.40 M HCN and
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I. The Sociological Perspective A. This perspective is important because it provides a unique way of looking at the human experience. It allows us to gain a new and comprehensive vision of day-to-day social life. B. This perspective stresses the broader social context of behaviour by looking at an individual’s social location (employment‚ income‚ education‚ gender‚ age‚ and race) and by considering external influences and personal experiences‚ which are internalized and become part of a person’s
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The phrase “turning point” has a lot of meanings but personally‚ for me‚ it is a moment that caused me to realize what has always been in front of me. Turning point may also mean a time at which a decisive change in a situation occurs‚ especially one with beneficial results. Recently‚ one event became the turning point of my life and my beliefs. Last Tuesday‚ our class‚ II-St. Therese watched the film “The Encounter”. That movie marked a pivotal moment in my life. It helped me realize that Jesus
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America is called the “Melting Pot” because of the diversity of the American culture. The migration and immigration of different cultures and people created America’s identity and its nickname of the “Melting Pot”. The American identity began developing in the 1600’s with the construction of colonial America. Throughout the 1800’s‚ America’s identity was developed by thousands of immigrants who entered America and the migration of people within America. Between the 19th and 20th century‚ and even
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Extracted From?.................................................................................................................. 7 Bibliography………………………………………………………………………………………..9 DNA What is DNA? DNA is a molecule called deoxyribonucleic acid which contains the biological instructions‚ meaning it explains about living species; it makes each species unique. It is passed from adult organisms during reproduction‚ along with the instructions it contains. Where is DNA Found? DNA
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The conventional method was conducted by placing 2.0641 grams of salicylic acid in a dry 125 mL Erlenmeyer flask. In a fume hood‚ 4 mL of acetic anhydride and 5 drops of concentrated sulfuric acid were added to the flask. The contents were swirled in the flask and then heated for 20 minutes in a hot water bath. After the 20 minutes were up‚ 10 mL of cold water were added in 1 mL increments. The flask was cooled for 10 minutes and occasionally stirred. The crystals that formed were collected via filtration
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anti addition of bromines. The melting point was 199-203°C and the NMR J values angle is at 167 which both prove the erythro-2‚3-dibromo-3-phenylpropanoic. Determination of the Stereochemistry of 2‚3-dibromo-3-phenylpropanoic acid. Introduction The purpose of this experiment was to determine the mechanism of the reaction of trans-cinnamic acid with the addition of bromines to 2‚3-dibromo-3-phenylpropanoic acid. An addition of bromine was added to trans-cinnamic acid and it is necessary to determine
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The objective of this lab was to identify an unknown compound by determining the melting point range using fast and slow ramps. Also‚ to determine the eutectic point of Urea and Cinnamic Acid. An unknown compound that was numbered 8 was chosen. A small amount of the unknown compound was placed in a weighing paper using a spatula. The weighing paper was folded in half twice and then was grinded using a spatula. After the unknown compound was grinded about 1-2mm was added into a capillary tube. A
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