between benzonitrile oxide and styrene. 2. Plan: Each student in a group of three will work to create a reaction with the Benzonitrile Oxide with‚ cis-stilbene‚ trans-stilbene‚ or styrene in an Erlenmyer flask. With this Reaction solution thin layer chromatography will be performed using each reaction solution. The different reactions will then be compared by running co-spot TLC’s. An NMR of the crude products from each reaction will be taken. 3. References: * Chemistry 173Q Organic Chemistry
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Medicine Analysis – Synthesising Aspirin results After recrystallisation differences between the crude and purified aspirin were noted. The impure (crude) aspirin was powered and fluffy with small clumps and was slightly yellow in colour whereas the pure aspirin has a less fluffy crystalline powder and was whiter. This showed distinct differences in the two substances but similarities were also apparent showing aspirin‚ in some level‚ was created. Before recrystallisation the crude aspirin could
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opposition to‚ external forces like gravity Capillary action is sometimes called capillarity‚ capillary motion‚ or wicking Capillarity Types:- Capillarity Rise:- The upward movement of a liquid against the force of gravity inside narrow spaces and thin tubes is called capillary rise . This property of liquid is called capillarity. A common apparatus used to demonstrate capillarity is the capillary tube. Reason:- Capillarity occurs because of intermolecular forces between the liquid and surrounding
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Experiment # 4 Paper Chromatography 1. Why is the chromatogram developed in an essentially closed system? - The chromatogram is developed in a closed system in order to prevent the solvent to evaporate. Most solvents used in the chromatograph are toxic and flammable. It is also put in a close system to reduce the chance of outside factors affect the chromatograph. 2. What is the main advantage of 2-dimensional paper chromatography over a 1-dimensional one? - The
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CHM130 Lab 9 Chromatography Name: Karlee Rose A. Data Table (12 points) Paper # Color Source Solvent Distance Component Moves Distance Solvent Moves Rf value 1 Yellow M&M Candies 0.1% Salt Solution 28.88mm 42mm 0.69 2 Yellow Reese’s Pieces 0.1% Salt Solution 16.95mm 32mm 0.53 3 Purple Grape Soda 0.1% Salt Solution 32.15mm 51mm 0.63 4 Purple Grape Koolaid 0.1% Salt Solution 12.12mm 31mm 0.39 5 Red Easter Egg Dye 0.1% Salt Solution 1.18mm 7mm 0.17 6 Red Dry Erase Marker
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unknown mixture of colored compounds. The mixture will have three compounds from the following: azobenzene‚ azulene‚ 4-(p-nitrophenylazo)resorcinol‚ methyl red‚ bromocresol green. You can identify the components by separating them using thin layer chromatography (TLC) and comparing their Rf values with those of the
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investigation. Clearly explain the separation technique of paper chromatography in terms of partition. Calculate the Rf value of one of the constituent pigments and compare it to the book value. A paper chromatography was used to separate the pigments that make up chlorophyll to analyse‚ identify‚ and quantify the components‚ using paper (stationary phase – the part of the apparatus that does not move with the sample) and chromatography solvent that was 90% petroleum ether and 10% propanol (mobile
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Chemistry Lab Write-Up Title: Paper Chromatography of Powdered Beverage Mix Purpose/Objective: The purpose is to be able to use liquid chromatography to separate dyes in a powdered beverage mix‚ calculate the Rf values for each dye‚ and rank the polarity of each dye present. Hypothesis: If we are to use the liquid chromatography to investigate the different dyes‚ then I think the different dyes will come up having different polarities and Rf values. Procedure/Method: Draw a line across
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| Quantity | Large boiling tube | 1 | Large test tube rack | 1 | Cork stopper with pin hook | 1 | Strip of filter paper (Goodman) | 1 | Capillary tube | 1 | Fresh spinach leaves | 10g | Fresh solnostemon hybrid leaves | 10g | Chromatography solvent (9:1 petroleum ether-acetone) | 3mL | Measuring cylinder (20mL) | 1 | Strainer | 1 | Acetone (100%) | 40mL | Calcium carbonate | As much as needed | Pestle and mortar | 1 | Electronic balance | 1 | Scissors | 1 | Ruler
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usually masked by the prevalence of the green chlorophyll. Anothocyanin(red or purple)‚ carotene(orange)‚ and xanthrophyll(yellow) are found in different proportions in different leaves. Leaf pigments can be separated by using paper chromatography. Paper chromatography is a technique that extracts pigments into a paper filter called chromatogram. What are the pigments are in Red Wondering Jews? Carotenoids These pigments primarily absorb in the blue wavelengths‚ allowing the longer wavelengths
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