Purpose of the Experiment: The intention of the experiment is to use solvent extraction methods to separate a mixture containing a carboxylic acid and a neutral compound. Once recovered‚ the solids were purified by recrystallization and examined by thin-layer chromatography‚ and their identities were derived by melting point and infrared (IR) spectroscopy. Extraction is a procedure that selectively dissolves one or more of the mixture compounds into a proper solvent. Extraction refers to the moving
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Adrian Wolanski GD23665 McDonalds Getting thin while getting fat You might ask yourself‚ how is it possible to get thin while getting fat at the same time? The question refers to the dilemma of how our culture and values have changed in the more recent years‚ to how a corporation can still maintain to be profitable. Let’s face it‚ McDonalds has never been the first restaurant that would pop into your mind while thinking of a place to eat healthy‚ nor even the last‚ be honest. Health and fitness
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Cover Story Cola variants Spreading cola brands too thin Over the past 20 years‚ the battle for supremacy between Coca-Cola and Pepsi has resulted in the launches of numerous brand extensions. In combating decline in the fizzy drinks market‚ are the cola giants wise to rely on new variants to protect market share? By Mark Choueke variants. Coca-Cola added Diet Coke with Lemon to its permanent range this year‚ only for PepsiCo to follow with lemon and lime-flavoured Pepsi Max Twist. Not to be
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Chromatography lab Purpose: To separate food colorings into their component dyes using paper chromatography. Materials: Chromatography paper‚ Food coloring‚ Ruler‚ Pencil‚ Solvent solution‚ Test tubes‚ Test tube rack. Safety precaution: wear aprons‚ to make sure that you don’t get any of the alcohol on your clothes‚ and if you break a test tube you don’t get glass on you. Procedure: See-attached handout. Results: See chromatography with Audrey’s lab report.
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Proteins (ACTIVITY 8) Gallemit‚ Lacei Machelle• • January 17‚ 2013 ABSTRACT Chromatography is one of the most useful methods of separating minute amounts of complex mixtures into the pure substances contained therein. Chromatographic separations are effected by allowing the components in the mixture to be distributed in two phases‚ one being stationary‚ and the other‚ mobile. Partition chromatography involves two main distribution systems‚ one system is composed of a gas and a liquid and
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Experiment 1: TLC Analysis of Analgesic Drugs 1/23/2011 Purpose: The goal of this experiment is to test our knowledge and understanding of TLC analysis by having us do a TLC analysis of analgesics to figure out their main chemical components. Calculations: 1.) Rf = Distance spot traveled/ distance solvent traveled Results: Table 1: TLC Analysis Analgesic Drugs | Rf Value | Acetaminophen | 0.323 | Aspirin | 0.597 | Caffeine | 0.081 | Unknown 154 (Plate 1) | 0.081‚ 0.306‚ 0.597
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Ferrocene and Acetylferrocene will be separated using column chromatography. Column chromatography is a separation technique that is used among many disciplines including biology‚ biochemistry‚ microbiology and medicine. Many common antibiotics are purified by column chromatography.1 Column chromatography allows us to separate and collect individual compounds. In this experiment‚ lumen will be the stationary phase‚ and the more polar substance will be retained on the stationary phase longer
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Paper chromatography is one of the easiest methods of chromatography. It is a method of planar chromatography (stationary phase is in form of a plane). Paper chromatography follows the basic principle of chromatography‚ which states that substances or components are distributed in between the stationary phase and the mobile phase. It is an analytical technique‚ where only a small amount of a sample is used for separating and identifying its components. Like any other method of chromatography‚ paper
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3.6. Conclusion Various solvent extracts from mahua flower and fruits showed varying degrees of antioxidant activity in different test systems in a dose-dependent manner. The antioxidant activity was correlated with the amount of total phenolics present in the respective extracts in each assay. 50% acetone proved to be the most efficient solvent for extraction of antioxidants from mahua as the related extract contained the highest amount of phenolic compounds and also exhibited the strongest antioxidant
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The progress of the reaction was monitored in my case using two TLC plate. It first started off with the spotting of Standard benzoin and benzil which were provided in the lab and followed by the addition of the reaction mixture at once it starts changing colour/boiling‚ then at 10 and 20 mins into the reflux. Once all the necessary steps were spotted‚ the TLC plate was placed in in a beaker containing CH₂Cl₂(methylene chloride)‚ which was used as the developing solvent in this experiment. To check
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